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    REACTION REAGENT FOR TRIFLUOROMETHYLATION
    3.
    发明公开
    REACTION REAGENT FOR TRIFLUOROMETHYLATION 审中-公开
    REAKTIONSREGENZFÜRTRIFLUORMETHYLIERUNG

    公开(公告)号：EP2080744A1

    公开(公告)日：2009-07-22

    申请号：EP07831307.9

    申请日：2007-11-06

    申请人： SAGAMI CHEMICAL RESEARCH CENTER ,  Tosoh F-Tech, Inc.

    发明人： YAMAKAWA, Tetsu ,  YAMAMOTO, Kyoko ,  URAGUCHI, Daisuke ,  TOKUHISA, Kenji

    IPC分类号： C07B39/00 ,  C07C17/32 ,  C07C22/08 ,  C07C209/68 ,  C07C211/52 ,  C07D213/64 ,  C07D231/12 ,  C07D239/54 ,  C07D473/16 ,  C07D473/18

    CPC分类号： C07C209/74 ,  C07C17/32 ,  C07D213/64 ,  C07D231/12 ,  C07D239/54 ,  C07D473/16 ,  C07D473/18 ,  C07C211/52

    摘要： Provided is a reaction reagent for trifluoromethylation with high general versatility and good efficiency.
    The reaction reagent for trifluoromethylation contains an iron compound, trifluoromethyl iodide, a sulfoxide and a peroxide, and may further contain an acid. The iron compound is, for example, iron(II) sulfate, ammonium iron(II) sulfate, iron(II) tetrafluoroborate, ferrocene, bis(η 5 -pentamethylcyclopentadienyl)iron or an iron powder; the sulfoxide is, for example, dimethyl sulfoxide; the peroxide is, for example, hydrogen peroxide or hydrogen peroxide-urea composite; and the acid is, for example, sulfuric acid, tetrafluoroboric acid or trifluoromethanesulfonic acid.

    摘要翻译： 提供具有高通用性和高效率的三氟甲基化反应试剂。 用于三氟甲基化的反应试剂含有铁化合物，三氟甲基碘化物，亚砜和过氧化物，并且还可以含有酸。 铁化合物是例如硫酸铁（II），硫酸铁（II），四氟硼酸铁（II），二茂铁，双（5-五甲基环戊二烯基）铁或铁粉; 亚砜是例如二甲基亚砜; 过氧化物是例如过氧化氢或过氧化氢 - 尿素复合物; 酸是例如硫酸，四氟硼酸或三氟甲磺酸。

    1,3,5-TRIAZINE DERIVATIVE, METHOD FOR PRODUCING SAME, AND ORGANIC ELECTROLUMINESCENT DEVICE CONTAINING SAME AS COMPONENT
    5.
    发明公开
    1,3,5-TRIAZINE DERIVATIVE, METHOD FOR PRODUCING SAME, AND ORGANIC ELECTROLUMINESCENT DEVICE CONTAINING SAME AS COMPONENT 有权
    -1,3,5-三嗪，其制造方法，并且此作为成分含有机电致发光

    公开(公告)号：EP1930329A1

    公开(公告)日：2008-06-11

    申请号：EP06782922.6

    申请日：2006-08-23

    申请人： TOSOH CORPORATION ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： YAMAKAWA, Tetsu ,  AIHARA, Hidenori ,  YANAI, Naoko ,  TANAKA, Tsuyoshi ,  SATO, Masaru

    IPC分类号： C07D401/10 ,  C07D401/14 ,  C09K11/06 ,  H01L51/50

    CPC分类号： C07D401/14 ,  C07D401/10 ,  C09K11/06 ,  C09K2211/1059 ,  H01L51/0065 ,  H01L51/5048 ,  H05B33/14

    摘要： Since the conventional electron transporters have low thermal stability, the organic electroluminescent devices using them are not sufficient in terms of the compatibility of their luminance and luminous efficiency with device lifetime.
    A 1,3,5-triazine derivative of formula (1) is obtained by a metal catalyst-aided coupling reaction of a compound of formula (2) with a compound of formula (3), and this is used as a composing component of an organic electroluminescent device.




    [In the formulae, Ar 1 and Ar 2 represent phenyl group or the like, R 1 and R 2 represent hydrogen atom or the like, R 3 represents methyl or the like, m is an integer of 0 to 2, X represents 2,4-pyridylene or the like, p is 1 or 2, a and b are 1 or 2, a + b is 3, q is 0 or an integer of p or less, M represents -MgR 4 group or the like, R 4 represents chlorine atom or the like, r is p-q, and Y represents a leaving group.]

    摘要翻译： 由于传统的电子转运具有低的热稳定性，使用它们的有机电致发光装置不是在它们的亮度的相容性和发光效率与器件寿命方面足够的。 式（1）的1,3,5-三嗪衍生物是由式（2）的化合物与式（3）的化合物的金属催化剂辅助的偶联反应而得到的，并且这被用作构成的组分 的有机电致发光器件。 [式中，Ar 1和Ar 2表示苯基或类似物，R 1和R 2表示氢原子等，R 3 darstellt甲基等，m为0〜2的整数，X darstellt 2， 4-吡啶基等，p为1或2，a和b是1或2，a + b为3，q为0或在p以下，男darstellt -mgr 4基团等，R 4的整数 darstellt氯原子等，r为PQ，和Y darstellt离去基团。]

    IMIDE COMPLEX, METHOD FOR PRODUCING THE SAME, METAL-CONTAINING THIN FILM AND METHOD FOR PRODUCING THE SAME
    9.
    发明公开
    IMIDE COMPLEX, METHOD FOR PRODUCING THE SAME, METAL-CONTAINING THIN FILM AND METHOD FOR PRODUCING THE SAME 有权
    IMIDKOMPLEX，方法ITS，金属薄膜和方法及其

    公开(公告)号：EP2058295A1

    公开(公告)日：2009-05-13

    申请号：EP07792748.1

    申请日：2007-08-20

    申请人： Tosoh Corporation ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： TADA, Ken-ichi ,  FURUKAWA, Taishi ,  INABA, Koichiro ,  YOTSUYA, Tadahiro ,  CHIBA, Hirokazu ,  YAMAMOTO, Toshiki ,  YAMAKAWA, Tetsu ,  OSHIMA, Noriaki

    IPC分类号： C07C211/65 ,  C01G33/00 ,  C01G35/00 ,  C07C209/00 ,  C23C16/18 ,  C07F9/00

    CPC分类号： C23C16/18 ,  C01G33/00 ,  C01G35/00 ,  C01P2002/88 ,  C07C211/65 ,  C07C251/08 ,  C07F9/005 ,  C23C16/405

    摘要： Objects of the present invention are to provide a novel niobium or tantalum complex having good vapor pressure and becoming a raw material for producing a niobium- or tantalum-containing thin film by a method such as CVD method, ALD method or the like, a method for producing the same, a metal-containing thin film using the same, and a method for producing the same. The present invention relates to producing an imide complex represented by the general formula (1) by, for example, the reaction between M 1 (NR 1 )X 3 (L) r (2) and an alkali metal alkoxide (3):

    (wherein M 1 represents niobium atom or tantalum atom, R 1 represents an alkyl group having from 1 to 12 carbon atoms, R 2 represents an alkyl group having from 2 to 13 carbon atoms, X represents halogen atom, r is 1 when L is 1,2-dimethoxyethane ligand, r is 2 when L is pyridine ligand, and M 2 represents an alkali metal), and producing a niobium- or tantalum-containing thin film by using the imide complex (1) as a raw material.

    摘要翻译： 本发明的目的是提供一种具有良好蒸气压和成为原料用于生产铌或薄膜通过如下方法含钽的新颖铌或钽络合物：如CVD法，ALD法等，一种方法 其制造，含金属的薄膜使用相同的，和用于生产其的方法。 本发明涉及一种在由通式酰亚胺络合物的制造（1）由，例如，（NR 1）X 3（L）M 1之间的反应R（2）和碱金属醇盐（3）组成：（ worin M 1个darstellt铌原子或钽原子，R 1个darstellt烷基具有1至12个碳原子，R 2 darstellt烷基具有2至13个碳原子基团基团，X darstellt卤素原子，r为1时，L是1 1,2-二甲氧基乙烷配位体，配位体r为2时，L是吡啶和M 2 darstellt到碱金属），并且通过使用酰亚胺络合物（1）作为原料的铌或含钽薄膜。

    TITANIUM COMPLEXES, PROCESS FOR PRODUCTION THEREOF, TITANIUM -CONTAINING THIN FILMS, AND METHOD FOR FORMATION THEREOF
    10.
    发明公开
    TITANIUM COMPLEXES, PROCESS FOR PRODUCTION THEREOF, TITANIUM -CONTAINING THIN FILMS, AND METHOD FOR FORMATION THEREOF 有权
    钛络合物，方法教育及其钛，含薄膜的方法

    公开(公告)号：EP1947081A1

    公开(公告)日：2008-07-23

    申请号：EP06822809.7

    申请日：2006-11-01

    申请人： Tosoh Corporation ,  SAGAMI CHEMICAL RESEARCH CENTER

    发明人： TADA, Ken-ichi ,  INABA, Koichiro ,  FURUKAWA, Taishi ,  CHIBA, Hirokazu ,  YAMAKAWA, Tetsu ,  OSHIMA, Noriaki

    IPC分类号： C07C211/65 ,  C23C16/34 ,  C07F7/28

    CPC分类号： C23C16/18 ,  C07C211/65 ,  C07C251/08 ,  C07F7/006 ,  C23C16/34 ,  C23C16/405

    摘要： Objects of the present invention are to provide a novel titanium complex that has good vaporization characteristics and an excellent thermal stability, and becomes a raw material for forming a titanium-containing thin film by methods such as CVD method or ALD method, its production method, a titanium-containing thin film formed using the same, and its formation method. In the invention, a titanium complex represented by the general formula (1) is produced by reacting a diimine represented by the general formula (2) and metallic lithium, and then reacting a tetrakisamide complex represented by the general formula (3).


            [Chem. 2]   Ti (NR 5 R 6 ) 4      (3)



    (In the formulae, R 1 and R 4 represent an alkyl group having from 1 to 6 carbon atoms. R 2 and R 3 each independently represents a hydrogen atom or an alkyl group having from 1 to 3 carbon atoms. R 5 and R 6 each independently represents an alkyl group having from 1 to 4 carbon atoms.).

    摘要翻译： 本发明的目的是提供一种新颖的钛络合物确实具有良好的气化特性和优异的热稳定性，并成为原料用于形成由方法含钛薄膜：如CVD法或ALD法，它的生产方法， 含钛薄膜使用相同的形成，并且它的形成方法。 在本发明中，钛络合物由通式（1）是通过使由通式（2）和金属锂代表二亚胺反应，然后由通式tetrakisamide复杂产生（3）。 €ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒ[化学式 2]€ƒ€ƒ€ƒTi（NR 5 R 6）4€ƒ€ƒ€ƒ€ƒ€ƒ（3）（式中，R 1和R 4表示在具有1至6个碳原子的烷基。 R 2和R 3各自独立地darstellt氢原子或烷基为1至3个碳原子。R 5和R 6具有各自独立地darstellt烷基具有1至4个碳原子具有基团。）。