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    Process for the manufacture of 1,1,1,3,3-pentafluoropropane
    4.
    发明授权
    Process for the manufacture of 1,1,1,3,3-pentafluoropropane 失效
    制备1,1,1,3,3-五氟丙烷的方法

    公开(公告)号：US5574192A

    公开(公告)日：1996-11-12

    申请号：US519857

    申请日：1995-08-25

    Applicant: Michael VanDerPuy ,  Alagappan Thenappan

    Inventor： Michael VanDerPuy ,  Alagappan Thenappan

    IPC: B01J27/10 ,  B01J27/12 ,  C07B61/00 ,  C07C17/20 ,  C07C17/23 ,  C07C17/278 ,  C07C17/35 ,  C07C19/08 ,  C07C17/08

    CPC classification number: C07C19/08 ,  C07C17/206 ,  C07C17/23 ,  C07C17/278

    Abstract: This invention is related to the preparation of hydrofluorocarbons (HFCs). Specifically, it relates to the fluorination of a compound of the formula:CF.sub.y Cl.sub.3-y CH.sub.2 CHF.sub.w Cl.sub.2-wwherein w=0 or 1, and y=0-3, with hydrogen fluoride in the presence of a fluorination catalyst under conditions sufficient to produce a compound of the formula CF.sub.3 CH.sub.2 CF.sub.2 H.CF.sub.3 CH.sub.2 CF.sub.2 H or HFC 245fa may be used as a blowing agent, a propellant, and a heat transfer agent.

    Abstract translation: 本发明涉及氢氟烃（HFCs）的制备。 具体地说，本发明涉及在氟化催化剂存在下，在足以产生化合物的条件下，在氟化氢存在下氟化氟化的下式化合物：CFyCl 3 -yCH 2 CHF 2 Cl 2 -W其中w = 0或1，y = 0-3 式CF3CH2CF2H。 CF 3 CH 2 CF 2 H或HFC 245fa可以用作发泡剂，推进剂和传热剂。

    Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon
    6.
    发明授权
    Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon 有权
    液相催化氟化氟氯烃和氢氯氟烃

    公开(公告)号：US06689924B1

    公开(公告)日：2004-02-10

    申请号：US09467869

    申请日：1999-12-20

    Applicant: Alagappan Thenappan ,  Hsueh S. Tung ,  Robert L. Bell

    Inventor： Alagappan Thenappan ,  Hsueh S. Tung ,  Robert L. Bell

    IPC: C07C1700

    CPC classification number: C07C17/206 ,  C07C17/00 ,  C07C17/087 ,  Y10S526/906 ,  Y10S526/913 ,  C07C19/08

    Abstract: A process for the catalytic fluorination of hydrochlorocarbons and hydrochlorofluorocarbons in the liquid phase. The process is useful for fluorinating hydrochloropropanes, hydrochlorofluoropropanes, hydrochloropropenes and hydrochlorofluoropropenes and most particularly useful for fluorinating 1,1,1,3,3-pentachloropropane to 1,1,1,3,3-pentafloropropane. Suitable catalysts include (i) a pentavalent molybdenum halide; (ii) a tetravalent tin halide; (iii) a tetravalent titanium halide; (iv) a mixture of a pentavalent tantalum halide with a tetravalent tin halide; (v) a mixture of a pentavalent tantalum halide with a tetravalent titanium halide; (vi) a mixture of a pentavalent niobium halide with a tetravalent tin halide; (vii) a mixture of a pentavalent niobium halide with a tetravalent titanium halide; (viii) a mixture of a pentavalent antimony halide with a tetravalent tin halide; (ix) a mixture of a pentavalent antimony halide with a tetravalent titanium halide; (x) a mixture of a pentavalent molybdenum halide with a tetravalent tin halide; (xi) a mixture of a pentavalent molybdenum halide with a tetravalent titanium halide and (xii) a mixture of a pentavalent antimony halide with a trivalent antimony halide. Products of this process are useful in a variety of applications including solvents, blowing agents, and refrigerants.

    Abstract translation: 在液相中氢氯碳氢化合物和氢氯氟烃的催化氟化的方法。 该方法可用于氟化氢氯丙烷，氢氯氟丙烷，氢氯丙烯和氢氯氟丙烯，最特别用于将1,1,1,3,3-五氯丙烷氟化为1,1,1,3,3-五氟丙烷。 合适的催化剂包括（i）五价钼卤化物; （ii）四价卤化锡; （iii）四价钛卤化物; （iv）五价卤化钽与四价卤化锡的混合物; （v）五价钽卤化物与四价钛卤化物的混合物; （vi）五价铌卤化物与四价卤化锡的混合物; （vii）五价铌卤化物与四价钛卤化物的混合物; （viii）五价锑卤化物与四价卤化锡的混合物; （ix）五价锑卤化物与四价钛卤化物的混合物; （x）五价钼卤化物与四价卤化锡的混合物; （xi）五价钼卤化物与四价卤化钛的混合物，（xii）五价锑卤化物与三价卤化锑的混合物。 该方法的产品可用于各种应用，包括溶剂，发泡剂和制冷剂。

    Compositions of 1-bromopropane and an organic solvent
    7.
    发明授权
    Compositions of 1-bromopropane and an organic solvent 失效
    1-溴丙烷和有机溶剂的组成

    公开(公告)号：US06365565B1

    公开(公告)日：2002-04-02

    申请号：US09562153

    申请日：2000-05-01

    Applicant: Alagappan Thenappan ,  Leonard Michael Stachura ,  Martin Richard Paonessa ,  Kane David Cook

    Inventor： Alagappan Thenappan ,  Leonard Michael Stachura ,  Martin Richard Paonessa ,  Kane David Cook

    IPC: C11D730

    CPC classification number: C07C19/075 ,  C11D7/5081 ,  C23G5/028

    Abstract: The invention relates to novel compositions of 1-bromopropane and at least one organic solvent selected from the group consisting of methanol, ethanol, 1-propanol, 2-propanol, 2-methyl-2-propanol, 2,2,2-trifluoroethanol, tetrahydrofiran, nitromethane, ethyl acetate, acetonitrile, hexane, 1,3-dioxolane, 1-chloro-2-methylpropane, 1,1,1,2,3,4,4,5,5,5-decafluoropentane, methyl ethyl ketone and cyclohexane and more particularly to azeotrope-like compositions based on these compounds which are useful as solvents in refrigeration flushing, oxygen system cleaning and vapor degreasing applications.

    Abstract translation: 本发明涉及1-溴丙烷和至少一种有机溶剂的新型组合物，其选自甲醇，乙醇，1-丙醇，2-丙醇，2-甲基-2-丙醇，2,2,2-三氟乙醇， 四氢呋喃，硝基甲烷，乙酸乙酯，乙腈，己烷，1,3-二氧戊环，1-氯-2-甲基丙烷，1,1,1,2,3,4,4,5,5,5-十氟戊烷，甲乙酮 和环己烷，更具体地涉及基于这些化合物的类共沸组合物，其可用作制冷冲洗，氧气系统清洗和蒸汽脱脂应用中的溶剂。

    Compositions of 1-bromopropane and an organic solvent
    9.
    发明授权
    Compositions of 1-bromopropane and an organic solvent 失效
    1-溴丙烷和有机溶剂的组成

    公开(公告)号：US6103684A

    公开(公告)日：2000-08-15

    申请号：US104646

    申请日：1998-06-25

    Applicant: Alagappan Thenappan ,  Leonard Michael Stachura ,  Martin Richard Paonessa ,  Kane David Cook

    Inventor： Alagappan Thenappan ,  Leonard Michael Stachura ,  Martin Richard Paonessa ,  Kane David Cook

    IPC: C07C19/075 ,  C11D7/50 ,  C23G5/028 ,  C11D7/30

    CPC classification number: C07C19/075 ,  C11D7/5081 ,  C23G5/028

    Abstract: The invention relates to novel compositions of 1-bromopropane and at least one organic solvent selected from the group consisting of methanol, ethanol, 1-propanol, 2-propanol, 2-methyl-2-propanol, 2,2,2-trifluoroethanol, tetrahydrofuran, nitromethane, ethyl acetate, acetonitrile, hexane, 1,3-dioxolane, 1-chloro-2-methylpropane, 1,1,1,2,3,4,4,5,5, 5-decafluoropentane, methyl ethyl ketone and cyclohexane and more particularly to azeotrope-like compositions based on these compounds which are useful as solvents in refrigeration flushing, oxygen system cleaning and vapor degreasing applications.

    Abstract translation: 本发明涉及1-溴丙烷和至少一种有机溶剂的新型组合物，其选自甲醇，乙醇，1-丙醇，2-丙醇，2-甲基-2-丙醇，2,2,2-三氟乙醇， 四氢呋喃，硝基甲烷，乙酸乙酯，乙腈，己烷，1,3-二氧戊环，1-氯-2-甲基丙烷，1,1,1,2,3,4,4,5,5,5-十氟戊烷，甲基乙基酮 和环己烷，更具体地涉及基于这些化合物的类共沸组合物，其可用作制冷冲洗，氧气系统清洗和蒸汽脱脂应用中的溶剂。

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