公开(公告)号：US06429176B1

公开(公告)日：2002-08-06

申请号：US10076408

申请日：2002-02-19

申请人： Hang-Chang Bobby Chen ,  Edward A. Rowe

发明人： Hang-Chang Bobby Chen ,  Edward A. Rowe

IPC分类号： C11D730

CPC分类号： C11D7/5018 ,  C23G5/02803 ,  C23G5/02806

摘要： Disclosed is a composition of about 20 to about 80 wt % benzotrifluoride and about 20 to about 80 wt % trichloroethylene. Up to about 1 wt % of a stabilizer for the trichloroethylene can be included in the composition.

公开(公告)号：US06380148B2

公开(公告)日：2002-04-30

申请号：US09886270

申请日：2001-06-22

申请人： Eiji Seki ,  Tatsuya Otsuka ,  Tatsuya Hirata ,  Yoshinori Tanaka ,  Hirokazu Aoyama

发明人： Eiji Seki ,  Tatsuya Otsuka ,  Tatsuya Hirata ,  Yoshinori Tanaka ,  Hirokazu Aoyama

IPC分类号： C11D730

CPC分类号： C07C19/16 ,  C01B7/195 ,  C01B7/196 ,  C07C17/38

摘要： The present invention provides a method for isolating and purifying 1,1,1,2,2-pentafluoroethyl iodide or hydrogen fluoride from a mixture of 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride, characterized by distilling an azeotropic mixture of 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride from a mixture containing 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride either after liquid—liquid separation when the mixture is heterogeneous or directly when the mixture is homogeneous to obtain 1,1,1,2,2-pentafluoroethyl iodide or hydrogen fluoride from the bottom of the distillation column.

摘要翻译： 本发明提供从1,1,1,2,2-五氟乙基碘和氟化氢的混合物中分离和纯化1,1,1,2,2-五氟乙基碘或氟化氢的方法，其特征在于蒸馏共沸 当混合物是异质的或直接当液体分离时，来自含有1,1,1,2,2-五氟乙基碘和氟化氢的混合物的1,1,1,2,2-五氟乙基碘和氟化氢的混合物 混合物是均匀的，从蒸馏塔的底部得到1,1,1,2,2-五氟乙基碘或氟化氢。

公开(公告)号：US06271189B1

公开(公告)日：2001-08-07

申请号：US09445584

申请日：1999-12-13

申请人： Eiji Seki ,  Tatsuya Otsuka ,  Tatsuya Hirata ,  Yoshinori Tanaka ,  Hirokazu Aoyama

发明人： Eiji Seki ,  Tatsuya Otsuka ,  Tatsuya Hirata ,  Yoshinori Tanaka ,  Hirokazu Aoyama

IPC分类号： C11D730

CPC分类号： C07C19/16 ,  C01B7/195 ,  C01B7/196 ,  C07C17/38

摘要： The present invention provides a method for isolating and purifying 1,1,1,2,2-pentafluoroethyl iodide or hydrogen fluoride from a mixture of 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride, characterized by distilling an azeotropic mixture of 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride from a mixture containing 1,1,1,2,2-pentafluoroethyl iodide and hydrogen fluoride either after liquid-liquid separation when the mixture is heterogeneous or directly when the mixture is homogeneous to obtain 1,1,1,2,2-pentafluoroethyl iodide or hydrogen fluoride from the bottom of the distillation column.

摘要翻译： 本发明提供从1,1,1,2,2-五氟乙基碘和氟化氢的混合物中分离和纯化1,1,1,2,2-五氟乙基碘或氟化氢的方法，其特征在于蒸馏共沸 当混合物是异质的或直接当液体分离时，来自含有1,1,1,2,2-五氟乙基碘和氟化氢的混合物的1,1,1,2,2-五氟乙基碘和氟化氢的混合物 混合物是均匀的，从蒸馏塔的底部得到1,1,1,2,2-五氟乙基碘或氟化氢。

公开(公告)号：US06759381B1

公开(公告)日：2004-07-06

申请号：US10430078

申请日：2003-05-06

申请人： Robert C. Johnson ,  Daniel C. Merkel ,  Hsuehsung Tung

发明人： Robert C. Johnson ,  Daniel C. Merkel ,  Hsuehsung Tung

IPC分类号： C11D730

CPC分类号： C11D7/5045 ,  C07C17/206 ,  C07C19/10 ,  C07C21/18 ,  C11D7/28

摘要： Provided are azeotropic and azeotrope-like mixtures of 1-chloro-1,3,3,3-tetrafluoropropane and 1,2-dichloro-3,3,3-trifluoropropene that are useful as an intermediate in the production of HFC-245fa. HFC-245fa is useful as a nontoxic, zero ozone depleting fluorocarbon useful as solvents, blowing agents, refrigerants, cleaning agents, aerosol propellants, heat transfer media, gaseous dielectrics, fire extinguishing compositions and power cycle working fluids.

摘要翻译： 提供了可用作HFC-245fa生产中间体的1-氯-1,3,3,3-四氟丙烷和1,2-二氯-3,3,3-三氟丙烯的共沸和类共沸混合物。 HFC-245fa可用作无毒，无臭氧消耗的氟烃，可用作溶剂，发泡剂，制冷剂，清洁剂，气溶胶推进剂，传热介质，气体电介质，灭火组合物和动力循环工作流体。

公开(公告)号：US06475971B2

公开(公告)日：2002-11-05

申请号：US09768415

申请日：2001-01-24

申请人： Hang Thanh Pham ,  Rajiv Ratna Singh ,  Hsueh Sung Tung

发明人： Hang Thanh Pham ,  Rajiv Ratna Singh ,  Hsueh Sung Tung

IPC分类号： C11D730

CPC分类号： C11D7/5045 ,  C07C17/386 ,  C07C21/18 ,  C09K5/00 ,  C11D7/08

摘要： The invention relates to azeotropic and azeotrope-like mixtures of 1,2-dichloro-3,3,3-trifluoropropene (HCFC-1223xd) and hydrogen fluoride, which are useful as intermediates in the production of HCFC-1223xd.

摘要翻译： 本发明涉及可用作生产HCFC-1223xd的中间体的1,2-二氯-3,3,3-三氟丙烯（HCFC-1223xd）和氟化氢的共沸和类共沸混合物。

公开(公告)号：US06176942B1

公开(公告)日：2001-01-23

申请号：US09375089

申请日：1999-08-16

申请人： Lawrence A. Clark ,  James L. Priest

发明人： Lawrence A. Clark ,  James L. Priest

IPC分类号： C11D730

CPC分类号： C11D7/261 ,  C11D7/24 ,  C11D7/267 ,  C11D7/28 ,  C11D7/32 ,  C11D7/5013 ,  C11D7/5018 ,  C11D7/5022 ,  C11D11/0023 ,  C11D11/0041 ,  C11D11/0047 ,  C23G5/028 ,  C23G5/02806

摘要： The invention provides a solvent mixture including n-propyl bromide, a mixture of low boiling solvents and, preferably, a defluxing and/or ionics removing additive and/or at least one saturated terpene. The invention also provides a method of cleaning an article (e.g., an electrical, plastic, or metal part) in a vapor degreaser using the solvent mixture. The solvent mixture of the invention is non-flammable, non-corrosive, and non-hazardous. In addition, it has a high solvency and a very low ozone depletion potential. Thus, using the solvent mixture of the invention, oil, grease, rosin flux, and other organic material can be readily removed from the article of interest in an environmentally safe manner.

摘要翻译： 本发明提供了一种溶剂混合物，包括正丙基溴，低沸点溶剂和优选脱溶剂和/或离子去除添加剂和/或至少一种饱和萜烯的混合物。 本发明还提供了一种使用溶剂混合物在蒸气去油器中清洁制品（例如，电，塑料或金属部件）的方法。 本发明的溶剂混合物是不可燃，非腐蚀性和非危险性的。 此外，它具有很高的偿付能力和极低的臭氧消耗潜力。 因此，使用本发明的溶剂混合物可以以环境安全的方式从感兴趣的物品中容易地除去油，油脂，松香助熔剂和其它有机材料。

公开(公告)号：US06548471B2

公开(公告)日：2003-04-15

申请号：US10028026

申请日：2001-12-20

申请人： Richard M. Flynn ,  George G. I. Moore

发明人： Richard M. Flynn ,  George G. I. Moore

IPC分类号： C11D730

CPC分类号： C07C43/12 ,  C07C43/126 ,  C07C2601/14 ,  C07D207/10 ,  C07D211/38 ,  C07D265/30 ,  C11D7/28 ,  C11D7/3281 ,  C11D7/34 ,  C11D7/5009 ,  C11D7/5013 ,  C11D7/5018 ,  C23G5/032 ,  D06L1/02

摘要： A process for removing contaminants from the surface of a substrate comprises contacting the substrate with a cleaning composition comprising at least one mono-, di-, or trialkoxy-substituted perfluoroalkane, perfluorocycloalkane, perfluorocycloalkyl-containing perfluoroalkane, or perfluorocycloalkylene-containing perfluoroalkane compound, the compound optionally containing additional catenary heteroatoms. The compounds exhibit good solvency properties while being environmentally acceptable.

公开(公告)号：US06489277B1

公开(公告)日：2002-12-03

申请号：US09670120

申请日：2000-09-26

申请人： Pascal Michaud

发明人： Pascal Michaud

IPC分类号： C11D730

CPC分类号： F26B5/005 ,  C11D7/5081 ,  C23G5/02803

摘要： In order to replace 1,1,2-trichloro-1,2,2-trifluoroethane and 1,1-dichloro-1-fluoroethane in compositions for treating solid surfaces (in particular defluxing), the invention proposes the use of a quasi-azeotropic mixture containing, by weight, from 75 to 95% of 1,1,1,3,3-pentafluorobutane, from 1 to 15% of methylene chloride and from 1 to 10% of methanol.

摘要翻译： 为了在用于处理固体表面的组合物（特别是去焊剂）中代替1,1,2-三氯-1,2,2-三氟乙烷和1,1-二氯-1-氟乙烷，本发明提出了使用准 - 含有重量百分比为75至95％的1,1,1,3,3-五氟丁烷，1至15％二氯甲烷和1至10％甲醇的共沸混合物。

公开(公告)号：US06402857B2

公开(公告)日：2002-06-11

申请号：US09725796

申请日：2000-11-29

申请人： Lawrence A. Clark ,  James L. Priest

发明人： Lawrence A. Clark ,  James L. Priest

IPC分类号： C11D730

CPC分类号： C11D7/261 ,  C11D7/24 ,  C11D7/267 ,  C11D7/28 ,  C11D7/32 ,  C11D7/5013 ,  C11D7/5018 ,  C11D7/5022 ,  C11D11/0023 ,  C11D11/0041 ,  C11D11/0047 ,  C23G5/028 ,  C23G5/02806

摘要： The invention provides a solvent mixture including n-propyl bromide, a mixture of low boiling solvents and, preferably, a defluxing and/or ionics removing additive and/or at least one saturated terpene. The invention also provides a method of cleaning an article (e.g., an electrical, plastic, or metal part) in a vapor degreaser using the solvent mixture. The solvent mixture of the invention is non-flammable, non-corrosive, and non-hazardous. In addition, it has a high solvency and a very low ozone depletion potential. Thus, using the solvent mixture of the invention, oil, grease, rosin flux, and other organic material can be readily removed from the article of interest in an environmentally safe manner.

摘要翻译： 本发明提供了一种溶剂混合物，包括正丙基溴，低沸点溶剂和优选脱溶剂和/或离子去除添加剂和/或至少一种饱和萜烯的混合物。 本发明还提供了一种使用溶剂混合物在蒸气去油器中清洁制品（例如，电，塑料或金属部件）的方法。 本发明的溶剂混合物是不可燃，非腐蚀性和非危险性的。 此外，它具有很高的偿付能力和极低的臭氧消耗潜力。 因此，使用本发明的溶剂混合物可以以环境安全的方式从感兴趣的物品中容易地除去油，油脂，松香助熔剂和其它有机材料。

公开(公告)号：US06342471B1

公开(公告)日：2002-01-29

申请号：US09491591

申请日：2000-01-25

申请人： Toney M. Jackson

发明人： Toney M. Jackson

IPC分类号： C11D730

CPC分类号： C11D7/261 ,  C09K3/30 ,  C11D7/28 ,  C11D7/5018 ,  C11D17/0043 ,  H05K3/26

摘要： A propellant-rich aerosol cleaner for use with electrical circuit boards and electrical connector components includes a solvent having a low or no ozone depletion potential and a propellant. The solvent is present in a concentration of at most about 50 percent by weight and preferably about 40 percent, and the propellant is present in a concentration of at least about 50 percent by weight and preferably about 60 percent, of the cleaner. The cleaner exhibits a cleaning characteristic of about 0.25 milligrams of soil per gram of cleaner delivered and exhibits low to no residual flammability. In one formulation, the solvent is n-propyl bromide and is present in a concentration of about 40 weight percent. In another formulation, the solvent is trichloroethylene and is present in a concentration of about 20 weight percent. An alternate formulation includes a solvent that is a blend of TCE or trans 1,2-dichloroethylene at a concentration of about 7 to 9 percent by weight and HFE at a concentration of about 21 percent by weight. A preferred propellant is tetrafluoroethane, an HFC liquefied gas, in a concentration of about 60 to 80 weight percent.

摘要翻译： 用于电路板和电连接器部件的富含推进剂的气溶胶清洁剂包括具有低或无臭氧消耗潜能的溶剂和推进剂。 溶剂的浓度最多为约50重量％，优选约40重量％，推进剂的浓度为清洁剂的至少约50重量％，优选约60重量％。 清洁剂表现出每克清洁剂输送约0.25毫克土壤的清洁特性，表现出低至无残留的可燃性。 在一种制剂中，溶剂是正丙基溴，并且以约40重量％的浓度存在。 在另一种制剂中，溶剂是三氯乙烯并且以约20重量％的浓度存在。 另一种制剂包括溶剂，其为浓度为约7至9重量％的TCE或反式1,2-二氯乙烯的混合物，浓度为约21重量％的HFE。 优选的推进剂是浓度为约60至80重量％的四氟乙烷，HFC液化气体。