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    Coating method
    1.
    发明授权
    Coating method 失效
    涂布方法

    公开(公告)号：US5691002A

    公开(公告)日：1997-11-25

    申请号：US596094

    申请日：1996-01-31

    申请人： Hiroaki Oda ,  Masaru Mitsuji ,  Yasumasa Okumura ,  Hiroshi Inoue ,  Hisashi Isaka

    发明人： Hiroaki Oda ,  Masaru Mitsuji ,  Yasumasa Okumura ,  Hiroshi Inoue ,  Hisashi Isaka

    IPC分类号： B05D1/00 ,  B05D7/00 ,  B05D1/36

    CPC分类号： B05D7/52 ,  B05D7/542 ,  B05D7/587 ,  B05D1/007

    摘要： The coating method of the present invention comprises sequentially applying an amine-neutralized type aqueous intermediate coating composition and an amine-neutralized type aqueous top coating composition, the method being characterized in that a coating composition mainly comprising (A) an amine-neutralized base resin having a hydroxyl value of 30 to 150 KOH mg/g and an acid value of 15 to 50 KOH mg/g, (B) an amino resin and (C) an organic sulfonic acid amine salt is used as the amine-neutralized type aqueous intermediate coating composition. The method of the present invention can improve the adhesion between layers of a multi-layer coating film formed from aqueous coating compositions and chipping resistance of said coating film.

    摘要翻译： PCT No.PCT / JP95 / 01079 Sec。 371日期1996年1月31日 102（e）日期1996年1月31日PCT归档1995年6月1日PCT公布。 出版物WO95 / 33578 日期1995年12月14日本发明的涂布方法包括依次施加胺中和型水性中间体涂料组合物和胺中和型水性顶涂料组合物，其特征在于，主要包含（A） 使用羟基值为30〜150KOHmg / g，酸值为15〜50KOHmg / g，（B）氨基树脂和（C）有机磺酸胺盐的胺中和基础树脂作为 胺中和型水性中间体涂料组合物。 本发明的方法可以提高由水性涂料组合物形成的多层涂膜和所述涂膜的耐崩裂性之间的粘合力。

    Coating method
    2.
    发明授权
    Coating method 失效
    涂布方法

    公开(公告)号：US5756221A

    公开(公告)日：1998-05-26

    申请号：US785600

    申请日：1997-01-17

    申请人： Kyoichi Horibe ,  Hidehiko Haneishi ,  Masaru Mitsuji ,  Motoshi Yabuta ,  Yasumasa Okumura

    发明人： Kyoichi Horibe ,  Hidehiko Haneishi ,  Masaru Mitsuji ,  Motoshi Yabuta ,  Yasumasa Okumura

    IPC分类号： B05D1/36 ,  B05D3/02 ,  B05D3/10 ,  B05D5/00 ,  B05D7/00 ,  B05D7/24 ,  C08G18/58 ,  C09D5/44 ,  C25D13/06

    CPC分类号： B05D7/576 ,  C08G18/58 ,  C08G18/584 ,  C09D5/4473 ,  Y10T428/12569 ,  Y10T428/31522

    摘要： The present invention provides a coating method which comprises applying, onto a material to be coated, a cationic electrodepositable coating composition comprising (A) a polyurethane-modified epoxy resin-amine adduct obtained by a reaction of (A-1) a polyurethane-compound having one terminal isocyanate group in the molecule, obtained by a reaction of (a) a polyhydroxy compound having a number-average molecular weight of 50-8,000, (b) a polyisocyanate compound, and (c) a compound having one active hydrogen atom in the molecule; (A-2) a bisphenol type epoxy resin having at least two epoxy groups in the molecule; and (A-3) an active-hydrogen-containing amine compound, and (B) a nonionic film-forming resin, the weight ratio of the resin (A)/the resin (B) being 15/85 to 95/5 and the coating composition comprising substantially no pigment, then heat-curing the formed electrocoating film; and thereafter applying, onto the cured electrocoating film, an aqueous coating composition comprising a metallic pigment and/or a coloring pigment and a high-solid-content coating composition comprising (C) a carboxyl group-containing compound, (D) a vinyl type polymer containing, in the molecule, an epoxy group, a hydroxyl group and a hydrolyzable alkoxysilyl group, (E) a reactive organopolysiloxane, and (F) crosslinked polymer fine particles but comprising substantially no pigment, by two-coat two-bake or by two-coat one-bake.

    摘要翻译： 本发明提供一种涂布方法，其包括在待涂覆的材料上涂布阳离子可电沉积涂料组合物，其包含（A）通过（A-1）聚氨酯化合物（A-1）反应获得的聚氨酯改性的环氧树脂 - 胺加合物 通过（a）数均分子量为50-8,000的多羟基化合物（b）多异氰酸酯化合物和（c）具有一个活性氢原子的化合物的反应获得的分子中具有一个末端异氰酸酯基团 在分子中 （A-2）分子中具有至少两个环氧基的双酚型环氧树脂; 和（A-3）含活性氢的胺化合物和（B）非离子成膜树脂，树脂（A）/树脂（B）的重量比为15/85至95/5，和 所述涂料组合物基本上不含颜料，然后热固化所形成的电泳涂膜; 然后在固化的电泳涂膜上涂覆含有金属颜料和/或着色颜料的水性涂料组合物和包含（C）含羧基化合物的高固含量涂料组合物，（D）乙烯基型 在分子中含有环氧基，羟基和可水解的烷氧基甲硅烷基的聚合物，（E）反应性有机聚硅氧烷和（F）交联的聚合物细颗粒，但基本上不含颜料，通过双层二烘烤或通过 双面单烤。

    Aqueous coating composition and coating method using same
    3.
    发明授权
    Aqueous coating composition and coating method using same 失效
    水性涂​​料组合物及其涂布方法

    公开(公告)号：US4948829A

    公开(公告)日：1990-08-14

    申请号：US347645

    申请日：1989-05-05

    申请人： Masaru Mitsuji ,  Mistugu Endo ,  Youji Kawachi ,  Akira Asada

    发明人： Masaru Mitsuji ,  Mistugu Endo ,  Youji Kawachi ,  Akira Asada

    IPC分类号： B05D1/36 ,  B05D5/06 ,  B05D7/02 ,  B05D7/16 ,  B05D7/24 ,  C08G18/08 ,  C08L61/20 ,  C08L75/04 ,  C09D4/02 ,  C09D133/06 ,  C09D175/00 ,  C09D175/04

    CPC分类号： C09D133/06 ,  C08G18/0823 ,  C09D175/04 ,  B05D7/532 ,  C08L61/20 ,  C08L75/04

    摘要： Disclosed are (1) an aqueous coating composition which is characterized in that the composition comprises:(A) an acrylic resin-type emulsion,(B) a urethane resin-type emulsion and(C) a crosslinking agentthe component (B) being a self-emulsifiable urethane emulsion prepard by subjecting a urethane prepolymer to reaction for chain extension by water and to emulsification after or during neutralization of the urethane prepolymer with a tertiary amine, the urethane prepolymer consisting essentially of (i) an aliphatic and/or alicyclic diisocyanate, (ii) a polyether diol and/or polyester diol both having a number-average molecular weight of about 500 to about 5000, (iii) a low-molecular weight polyhydroxyl compound and (iv) a dimethylolalkanoic acid in an NCO/OH ratio by equivalent of 1.1-1.9/1; and (2) a two-coat one-bake coating method characterized by use of said aqueous coating composition as the base-coat composition.

    摘要翻译： 公开了（1）一种水性涂料组合物，其特征在于组合物包含：（A）丙烯酸树脂型乳液，（B）聚氨酯树脂型乳液和（C）交联剂，组分（B）为 一种可自乳化的聚氨酯乳液，其通过在氨基甲酸酯预聚物与叔胺中和之后使氨基甲酸酯预聚物进行水反应扩链和乳化，氨基甲酸酯预聚物基本上由（i）脂族和/或脂环族 二异氰酸酯，（ii）数均分子量为约500至约5000的聚醚二醇和/或聚酯二醇，（iii）低分子量多羟基化合物和（ⅳ）NCO / OH中的二羟甲基链烷酸 比例相当于1.1-1.9 / 1; 和（2）双层单烘烤涂布方法，其特征在于使用所述水性涂料组合物作为底涂层组合物。

    Aqueous coating and method for film formation using the same
    4.
    发明授权
    Aqueous coating and method for film formation using the same 失效
    水性涂​​料及其成膜方法

    公开(公告)号：US06268429B1

    公开(公告)日：2001-07-31

    申请号：US09482001

    申请日：2000-01-13

    申请人： Masaru Mitsuji ,  Nobushige Numa ,  Yugen Kawamoto

    发明人： Masaru Mitsuji ,  Nobushige Numa ,  Yugen Kawamoto

    IPC分类号： C08L6702

    CPC分类号： C09D133/066 ,  C08L33/062 ,  C08L61/20 ,  C08L61/32 ,  C09D167/00 ,  C08L2666/14 ,  C08L2666/28 ,  C08L2666/02

    摘要： The present invention provides an aqueous coating comprising: (A) a resin having hydroxyl group and carboxyl group in the molecule, (B) an alkyl-etherified methylolmelamine resin, and (C) an oxazoline group-containing compound. This aqueous coating can alleviate the problems of conventional aqueous coatings comprising (a) a resin having hydroxyl group and carboxyl group and (b) an alkyl-etherified methylolmelamine resin.

    摘要翻译： 本发明提供一种水性涂料，其包含：（A）分子中具有羟基和羧基的树脂，（B）烷基醚化羟甲基三聚氰胺树脂和（C）含有恶唑啉基的化合物。该水性涂料可以缓解 常规水性涂料的问题包括（a）具有羟基和羧基的树脂和（b）烷基醚化的羟甲基三聚氰胺树脂。

    Water-dispersible resin composition, water-dispersible coating composition and coating method using the coating composition
    5.
    发明授权
    Water-dispersible resin composition, water-dispersible coating composition and coating method using the coating composition 失效
    水分散性树脂组合物，水分散性涂料组合物和使用该涂料组合物的涂布方法

    公开(公告)号：US5332766A

    公开(公告)日：1994-07-26

    申请号：US24083

    申请日：1993-03-01

    申请人： Yasuo Takaya ,  Masaru Mitsuji ,  Mitsugu Endo

    发明人： Yasuo Takaya ,  Masaru Mitsuji ,  Mitsugu Endo

    IPC分类号： C08F8/44 ,  C08F285/00 ,  C09D151/00 ,  C08L83/00 ,  C08F265/04 ,  C08G77/00

    CPC分类号： C08F8/44 ,  C08F285/00 ,  C09D151/003 ,  Y10S525/902

    摘要： Disclosed are (1) a water-dispersible resin composition prepared by a process comprising; (I) reacting a silane monomer (A) having hydrolytic functional group and/or silano group and polymerizable unsaturated bond with a vinyl monomer (B) in an aqueous medium to obtain a three-dimensionally crosslinked particulate polymer, (II) reacting the particulate polymer with the silane monomer (A) and/or an allyl acrylate or allyl methacrylate (C), and (III) copolymerizing the resulting reaction product with a vinyl monomer component comprising a carboxyl-containing vinyl monomer (D), followed by neutralizing the carboxyl group; (2) a water-dispersible coating composition comprising a crosslinking agent and the water-dispersible resin composition prepared using a hydroxyl-containing vinyl monomer and another vinyl monomer as the vinyl monomer (B) in the step (I), and (3) a coating method characterized by using as a base coat composition a water-dispersible coating composition comprising the foregoing water-dispersible coating composition and a coloring pigment and/or metallic pigment in the two-coat method.

    摘要翻译： 公开了（1）通过以下方法制备的水分散性树脂组合物： （I）在水性介质中使具有水解官能团和/或硅烷基的硅烷单体（A）和可聚合不饱和键与乙烯基单体（B）反应，得到三维交联的颗粒聚合物，（II）使颗粒 聚合物与硅烷单体（A）和/或丙烯酸烯丙酯或甲基丙烯酸烯丙酯（C）的共聚物，和（III）使所得反应产物与包含含羧基的乙烯基单体（D）的乙烯基单体组分共聚，然后中和 羧基; （2）包含交联剂的水分散性涂料组合物和在步骤（I）中使用含羟基的乙烯基单体和另一种乙烯基单体作为乙烯基单体（B）制备的水分散性树脂组合物，和（3） 一种涂布方法，其特征在于在双涂层法中使用包含上述水分散性涂料组合物和着色颜料和/或金属颜料的水分散性涂料组合物作为底涂层组合物。

    Two-coat, one-bake coating method using aqueous base coat
    8.
    发明授权
    Two-coat, one-bake coating method using aqueous base coat 失效
    双面包衣，单面包衣方法采用水性底漆

    公开(公告)号：US5130167A

    公开(公告)日：1992-07-14

    申请号：US552388

    申请日：1990-07-13

    申请人： Masaru Mitsuji ,  Akira Kasari ,  Nobuyuki Kawasaki

    发明人： Masaru Mitsuji ,  Akira Kasari ,  Nobuyuki Kawasaki

    IPC分类号： B05D7/14 ,  B05D1/36 ,  C08K5/00 ,  C09D143/04 ,  C09D151/00

    CPC分类号： C09D151/00 ,  B05D7/532 ,  C08K5/0091 ,  C09D143/04

    摘要： Disclosed is a coating method comprising the steps of applying a base coat composition to a substrate, applying a clear coating composition to the coated surface while the applied base coat composition is still uncured and curing the two coating compositions thus applied at the same time, the method being characterized in that the base coat composition is an aqueous one containing a coloring pigment and that the clear coating composition is a curable one containing a basal resin and a curing catalyst as main components, the basal resin being a resin (Y) having in the molecule hydroxyl group and/or hydrolyzable group both directly attached to the silicon atom, and epoxy group or a resin mixture (Z) of a resin or a compound (Z-1) having hydroxyl group and/or hydrolyzable group both directly attached to the silicon atom and a resin (Z-2) having epoxy group.

    摘要翻译： 公开了一种涂布方法，其包括以下步骤：将基底涂料组合物施加到基材上，在涂布的底涂层组合物仍未固化的同时将涂布的涂料组合物施加到涂布表面上并固化由此施加的两种涂料组合物， 方法的特征在于，底涂层组合物是含有着色颜料的水性组合物，透明涂料组合物是含有基础树脂和固化催化剂作为主要成分的可固化组合物，所述基础树脂是树脂（Y），其具有 直接连接到硅原子上的分子羟基和/或可水解基团，和环氧基团或具有羟基和/或可水解基团的树脂或化合物（Z-1）的树脂混合物（Z）直接连接到 硅原子和具有环氧基的树脂（Z-2）。

    Coating method
    9.
    发明授权
    Coating method 失效
    涂布方法

    公开(公告)号：US4981759A

    公开(公告)日：1991-01-01

    申请号：US189167

    申请日：1988-05-02

    申请人： Eisaku Nakatani ,  Masaru Mitsuji ,  Yasuhiro Fujii ,  Katsuya Sera ,  Yuzo Miyamoto ,  Masafumi Kume ,  Tadayoshi Tatsuno ,  Akimasa Nakahata

    发明人： Eisaku Nakatani ,  Masaru Mitsuji ,  Yasuhiro Fujii ,  Katsuya Sera ,  Yuzo Miyamoto ,  Masafumi Kume ,  Tadayoshi Tatsuno ,  Akimasa Nakahata

    IPC分类号： C09D5/44 ,  C09D5/46

    CPC分类号： C09D5/4473 ,  Y10T428/12569 ,  Y10T428/31522

    摘要： A coating method, which comprises(i) applying to a substrate a multilayer film-forming cationic electrodeposition paint composed of(A) a cationic electrodepositable epoxy resin having a surface tension of 40 to 60 dynes/cm and being able to form a cathodically electrodepositable aqueous bath by neutralization with an acid, and(B) a nonionic film-forming resin having a surface tension of 25 to 45 dynes/cm, the weight ratio of resin (A) to resin (B) being from 60:40 to 98:2 and the surface tension of resin (A) being greater than that of resin (B), and curing the coated film by heating,(ii) applying a water-base or organic solvent-base colored paint as a first top coat, and(iii) applying as a second top coat a powder paint capable of forming a transparent film which may be colored.

    摘要翻译： 一种涂布方法，其包括（i）向基材施加多层成膜阳离子电沉积涂料，其由（A）表面张力为40至60达因/厘米的阳离子可电沉积环氧树脂组成，并且能够形成阴极电沉积 （B）表面张力为25〜45达因/厘米的树脂（A）与树脂（B）的重量比为60:40〜98的非离子性成膜树脂 ：2，树脂（A）的表面张力大于树脂（B）的表面张力，并且通过加热固化涂膜，（ii）施加水基或有机溶剂基着色涂料作为第一面漆， 和（iii）作为第二面漆施加能够形成可以着色的透明膜的粉末涂料。

    Aqueous resin dispersion
    10.
    发明授权
    Aqueous resin dispersion 失效
    水性树脂分散体

    公开(公告)号：US5539049A

    公开(公告)日：1996-07-23

    申请号：US247579

    申请日：1994-05-23

    申请人： Junichi Kajima ,  Masaru Mitsuji ,  Mitsugu Endo ,  Yasuo Takaya

    发明人： Junichi Kajima ,  Masaru Mitsuji ,  Mitsugu Endo ,  Yasuo Takaya

    IPC分类号： C08F290/12 ,  C08L51/00 ,  C08L55/00 ,  C08L61/28 ,  C09D161/28 ,  C08L33/02

    CPC分类号： C08L61/28 ,  C08F290/126 ,  C08L55/005 ,  C09D161/28 ,  C08L51/00

    摘要： Disclosed is an aqueous resin dispersion prepared by dispersing in an aqueous medium a graft resin (A) and a hydrophobic melamine resin (B), said graft resin (A) having a weight average molecular weight of 10,000 to 100,000 and an acid value of 5 to 80, and consisting of a hydrophobic main chain moiety and a hydrophilic side chain moiety, said hydrophilic side chain moiety being 5,000 to 50,000 in weight average molecular weight and at least 20 in acid value.

    摘要翻译： 公开了通过在水性介质中分散接枝树脂（A）和疏水性三聚氰胺树脂（B）而制备的水性树脂分散体，所述接枝树脂（A）的重均分子量为10,000〜100,000，酸值为5 80，由疏水性主链部分和亲水性侧链部分组成，所述亲水性侧链部分的重均分子量为5,000〜50,000，酸值为至少20。