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公开(公告)号：US09783681B2
公开(公告)日：2017-10-10
申请号：US13500836
申请日：2010-10-21
申请人： Peter D. Condo , Jung-Sheng Wu , Chad A. Haraldson , William J. Schultz , Emily S. Goenner , James E. Thorson , Wendy L. Thompson
发明人： Peter D. Condo , Jung-Sheng Wu , Chad A. Haraldson , William J. Schultz , Emily S. Goenner , James E. Thorson , Wendy L. Thompson
IPC分类号： C09C1/02 , C09C3/04 , C09C3/08 , C08J3/20 , C08K3/26 , C08K5/42 , C08K5/51 , C08K5/521 , C08K5/5317 , B82Y30/00 , C01F11/18
CPC分类号： C09C1/021 , B82Y30/00 , C01P2004/62 , C01P2004/64 , C08J3/203 , C08J2367/06
摘要： Methods of compounding nanoparticles with a resin, e.g., a curable resin and one or more surface modifying agents are described. The methods use wet milling technology, including both continuous and batch milling processes, and can be used to functionalize the nanoparticles and disperse the functionalized nanoparticles into the resin system in a single process. Methods of compounding curable resin systems containing reactive diluents are also disclosed.
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公开(公告)号：US09512264B2
公开(公告)日：2016-12-06
申请号：US13991634
申请日：2011-12-12
IPC分类号： C08K3/26 , B05D3/02 , C08L63/00 , C08G59/14 , C08K9/08 , C09C1/02 , C08K9/04 , C09C3/04 , C09C3/08 , C09C3/10
CPC分类号： C08G59/1438 , C01P2004/51 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C08K9/04 , C08K9/08 , C08L63/00 , C09C1/02 , C09C1/021 , C09C3/041 , C09C3/08 , C09C3/10
摘要： Nanoparticle compositions including calcite and a surface-modifying agent bonded to the calcite are described. The surface-modifying agent includes a binding group bonded to the calcite and a compatiblizing segment. The compatiblizing segment includes at least one of a polyethylene oxide, a polypropylene oxide, a polyester, a polyamide, or a combination thereof. The composition includes less than 2 wt. % solvents and/or resins. Methods of preparing nanoparticle compositions are also described.
摘要翻译： 描述了包括方解石和与方解石结合的表面改性剂的纳米颗粒组合物。 表面改性剂包括与方解石结合的结合基团和相容化部分。 相容片段包括聚环氧乙烷，聚环氧丙烷，聚酯，聚酰胺或其组合中的至少一种。 组合物包含小于2重量％ ％溶剂和/或树脂。 还描述了制备纳米颗粒组合物的方法。
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公开(公告)号：US20130253139A1
公开(公告)日：2013-09-26
申请号：US13991634
申请日：2011-12-12
CPC分类号： C08G59/1438 , C01P2004/51 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C08K9/04 , C08K9/08 , C08L63/00 , C09C1/02 , C09C1/021 , C09C3/041 , C09C3/08 , C09C3/10
摘要： Nanoparticle compositions including calcite and a surface-modifying agent bonded to the calcite are described. The surface-modifying agent includes a binding group bonded to the calcite and a compatiblizing segment. The compatiblizing segment includes at least one of a polyethylene oxide, a polypropylene oxide, a polyester, a polyamide, or a combination thereof. The composition includes less than 2 wt. % solvents and/or resins. Methods of preparing nanoparticle compositions are also described.
摘要翻译： 描述了包括方解石和与方解石结合的表面改性剂的纳米颗粒组合物。 表面改性剂包括与方解石结合的结合基团和相容化部分。 相容片段包括聚环氧乙烷，聚环氧丙烷，聚酯，聚酰胺或其组合中的至少一种。 组合物包含小于2重量％ ％溶剂和/或树脂。 还描述了制备纳米颗粒组合物的方法。
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4.发明申请SOLVENTLESS FUNCTIONALIZATION, MILLING, AND COMPOUNDING PROCESS WITH REACTIVE DILUENTS 有权无溶剂功能化，研磨和复合方法与反应性稀释公开(公告)号：US20120214948A1
公开(公告)日：2012-08-23
申请号：US13500836
申请日：2010-10-21
申请人： Peter D. Condo , Jung-Sheng Wu , Chad A. Haraldson , William J. Schultz , Emily S. Goenner , James E. Thorson , Wendy L. Thompson
发明人： Peter D. Condo , Jung-Sheng Wu , Chad A. Haraldson , William J. Schultz , Emily S. Goenner , James E. Thorson , Wendy L. Thompson
IPC分类号： C08F118/04 , C08G59/02 , B82Y30/00
CPC分类号： C09C1/021 , B82Y30/00 , C01P2004/62 , C01P2004/64 , C08J3/203 , C08J2367/06
摘要： Methods of compounding nanoparticles with a resin, e.g., a curable resin and one or more surface modifying agents are described. The methods use wet milling technology, including both continuous and batch milling processes, and can be used to functionalize the nanoparticles and disperse the functionalized nanoparticles into the resin system in a single process. Methods of compounding curable resin systems containing reactive diluents are also disclosed.
摘要翻译： 描述了将纳米颗粒与树脂例如可固化树脂和一种或多种表面改性剂混合的方法。 该方法使用湿式研磨技术，包括连续和间歇式研磨方法，并且可用于官能化纳米颗粒并且在单一工艺中将功能化纳米颗粒分散到树脂体系中。 还公开了含有反应性稀释剂的可固化树脂体系的混合方法。
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公开(公告)号：US10035909B2
公开(公告)日：2018-07-31
申请号：US13502836
申请日：2009-12-17
申请人： William J. Schultz , Mary I. Buckett , Peter D. Condo , Douglas P. Goetz , Chad A. Haraldson , Mark McCormick , Wendy L. Thompson , Steven J. Pachuta
发明人： William J. Schultz , Mary I. Buckett , Peter D. Condo , Douglas P. Goetz , Chad A. Haraldson , Mark McCormick , Wendy L. Thompson , Steven J. Pachuta
CPC分类号： C08L63/00 , C08K3/26 , C08K5/42 , C08K9/04 , C08K2003/265
摘要： Compositions comprising surface-modified calcite nanoparticles dispersed in a curable resin and to coatings and fibrous composites incorporating such compositions are described. The nanocalcite particles have a high magnesium to calcium surface concentration ratio. The surface-modifying agents include a binding group ionically associated with the nanoparticles, and a compatiblizing segment compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites, and coatings and fibrous composites prepared from such nanocalcite composites are also described.
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公开(公告)号：US10023726B2
公开(公告)日：2018-07-17
申请号：US13502891
申请日：2010-12-13
摘要： Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin system comprising a vinyl ester, and coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin system. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
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公开(公告)号：US20120245253A1
公开(公告)日：2012-09-27
申请号：US13502836
申请日：2009-12-17
申请人： William J. Schultz , Mary I. Buckett , Peter D. Condo , Douglas P. Goetz , Chad A. Haraldson , Mark McCormick , Wendy L. Thompson , Steven J. Pachuta
发明人： William J. Schultz , Mary I. Buckett , Peter D. Condo , Douglas P. Goetz , Chad A. Haraldson , Mark McCormick , Wendy L. Thompson , Steven J. Pachuta
IPC分类号： C09D163/00 , B05D3/00
摘要： Compositions comprising surface-modified calcite nanoparticles dispersed in a curable resin and to coatings and fibrous composites incorporating such compositions are described. The nanocalcite particles have a high magnesium to calcium surface concentration ratio. The surface-modifying agents include a binding group ionically associated with the nanoparticles, and a compatiblizing segment compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites, and coatings and fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译： 描述了包含分散在可固化树脂中的表面改性方解石纳米颗粒的组合物和包含这种组合物的涂层和纤维复合材料。 纳米碳酸钙颗粒具有高镁/钙表面浓度比。 表面改性剂包括与纳米颗粒离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料的方法，以及由这种纳米碳酸钙复合材料制备的涂层和纤维复合材料。
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公开(公告)号：US20120244338A1
公开(公告)日：2012-09-27
申请号：US13502891
申请日：2010-12-13
IPC分类号： C09D167/06 , B32B5/16
CPC分类号： C08K9/08 , C08K3/26 , C08K2201/011 , C08L67/06 , C08L67/07 , Y10T428/25
摘要： Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin system comprising a vinyl ester, and coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin system. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译： 描述了包含分散在包含乙烯基酯的可固化树脂体系中的表面改性的纳米碳酸钙颗粒的组合物，以及包含这种组合物的涂层和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂还可以包括能够与可固化树脂体系反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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公开(公告)号：US08592496B2
公开(公告)日：2013-11-26
申请号：US13133419
申请日：2009-12-01
申请人： Jung-Sheng Wu , Jayshree Seth , Michael D. Determan , Peter D. Condo , Lian Soon Tan , Neeraj Sharma
发明人： Jung-Sheng Wu , Jayshree Seth , Michael D. Determan , Peter D. Condo , Lian Soon Tan , Neeraj Sharma
IPC分类号： C01B33/158
CPC分类号： C08G63/00 , C01B33/1585
摘要： Methods of forming hybrid aerogels are described. The methods include forming a hybrid aerogel from a metal oxide precursor and a branched telechelic copolymer, e.g., co-hydrolyzing and co-condensing the metal oxide precursor and the branched telechelic copolymer. Aerogels and aerogel articles, including hydrophobic aerogels and hydrophobic aerogel articles are also described.
摘要翻译： 描述形成混合气凝胶的方法。 所述方法包括从金属氧化物前体和支化的遥爪共聚物形成混合气凝胶，例如共同水解和共缩合金属氧化物前体和分支的遥爪共聚物。 还描述了气凝胶和气凝胶制品，包括疏水性气凝胶和疏水性气凝胶制品。
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公开(公告)号：US20110245359A1
公开(公告)日：2011-10-06
申请号：US13133711
申请日：2009-12-01
申请人： Peter D. Condo , Jayshree Seth , Jung-Sheng Wu , Neeraj Sharma , Lian Soon Tan
发明人： Peter D. Condo , Jayshree Seth , Jung-Sheng Wu , Neeraj Sharma , Lian Soon Tan
CPC分类号： C01B33/155 , C01B33/157 , C01B33/159 , Y02P20/544
摘要： Methods of preparing hybrid aerogels are described. The methods include co-condensing a metal oxide precursor and an organo-functional metal oxide precursor, and crosslinking the organo-functional groups with an ethylenically-unsaturated crosslink agent. Thermal energy and actinic radiation crosslinking are described. Both supercritical aerogel and xerogels, including hydrophobic supercritical aerogel and xerogels, are described. Aerogel articles, including flexible aerogel articles are also disclosed.
摘要翻译： 描述了制备混合气凝胶的方法。 所述方法包括将金属氧化物前体和有机官能金属氧化物前体共缩合，并将有机官能团与烯属不饱和交联剂交联。 描述了热能和光化辐射交联。 描述了超临界气凝胶和干凝胶，包括疏水超临界气凝胶和干凝胶。 还公开了气凝胶制品，包括柔性气凝胶制品。
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