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    PROCESS FOR THE ENZYMATIC SYNTHESIS OF TRIGLYCERIDES
    1.
    发明申请
    PROCESS FOR THE ENZYMATIC SYNTHESIS OF TRIGLYCERIDES 审中-公开
    合成酶的合成方法

    公开(公告)号：US20070148746A1

    公开(公告)日：2007-06-28

    申请号：US11565696

    申请日：2006-12-01

    申请人： ULRICH SCHOERKEN ,  Carolin Meyer ,  Peter Horlacher ,  Sabine Both

    发明人： ULRICH SCHOERKEN ,  Carolin Meyer ,  Peter Horlacher ,  Sabine Both

    IPC分类号： C12P7/64 ,  C07C57/02

    CPC分类号： C12P7/6472 ,  C12P7/6454

    摘要： The invention relates to a process for the enzymatic synthesis of esters of polyunsaturated, short-chain or sensitive fatty acids with a high triglyceride content, which is made up of an enzymatic synthesis of the mixture of triglycerides and partial glycerides starting from free fatty acid, methyl or ethyl esters and glycerol, a subsequent selective enzymatic back-hydrolysis of the partial glycerides to fatty acid and glycerol and distillation-based separation of the triglycerides, and to the triglyceride-rich ester mixtures obtainable by this process. The process is preferably carried out as a one-pot process in the same reactor and in the presence of the same enzyme.

    摘要翻译： 本发明涉及一种用于酶促合成具有高甘油三酯含量的多不饱和，短链或敏感脂肪酸酯的方法，其由甘油三酯和偏甘油酯从游离脂肪酸开始的混合物的酶合成， 甲基或乙酯和甘油，随后将部分甘油酯选择性酶促回水解成脂肪酸和甘油，并且基于蒸馏的甘油三酸酯分离，以及通过该方法可获得的富含甘油三酯的酯混合物。 该方法优选在同一反应器中和在相同酶存在下作为一锅法进行。

    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes
    2.
    发明授权
    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes 有权
    在酶存在下生产不饱和脂肪酸甘油三酸酯的方法

    公开(公告)号：US07981641B2

    公开(公告)日：2011-07-19

    申请号：US12061005

    申请日：2008-04-02

    申请人： Ulrich Schoerken ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    发明人： Ulrich Schoerken ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    IPC分类号： C12P7/64 ,  C08L91/00

    CPC分类号： C12P7/6472

    摘要： Processes for the enzyme-catalyzed production of triglycerides using polyunsaturated fatty acids, in which (a) the reaction of polyunsaturated fatty acids and/or C1-4 alkyl esters thereof with glycerol in vacuo in the presence of an immobilized enzyme to form their triglycerides is accelerated by addition of an additive from the group of weakly basic salts, complexing agents and ion exchangers and/or addition of a weakly basic salt and/or addition of an entraining agent in the form of a solvent or a gas and/or addition of glycerol-binding adsorbers and/or heat treatment of the partial glyceride intermediate product, (b) the immobilized enzymes are removed from the triglyceride by separation or filtration and (c) the remaining fatty acids and/or C1-4 alkyl esters thereof are removed from the triglyceride by distillation, refining or extraction.

    摘要翻译： 使用多不饱和脂肪酸进行酶催化生产甘油三酸酯的方法，其中（a）在固定化酶存在下，多不饱和脂肪酸和/或其中C 1-4烷基酯与甘油在真空中反应形成其甘油三酸酯的方法是 通过加入来自弱碱性盐，络合剂和离子交换剂的添加剂和/或加入弱碱性盐和/或以溶剂或气体的形式加入夹带剂和/或添加 甘油结合吸附剂和/或热处理部分甘油酯中间产物，（b）通过分离或过滤从甘油三酯中除去固定化的酶，和（c）除去剩余的脂肪酸和/或其中的C 1-4烷基酯 从甘油三酯通过蒸馏，精制或提取。

    PROCESSES FOR THE PRODUCTION OF TRIGLYCERIDES OF UNSATURATED FATTY ACIDS IN THE PRESENCE OF ENZYMES
    3.
    发明申请
    PROCESSES FOR THE PRODUCTION OF TRIGLYCERIDES OF UNSATURATED FATTY ACIDS IN THE PRESENCE OF ENZYMES 有权
    在酶的存在下生产不饱和脂肪酸的三聚氰胺的方法

    公开(公告)号：US20080182304A1

    公开(公告)日：2008-07-31

    申请号：US12061005

    申请日：2008-04-02

    申请人： ULRICH SCHOERKEN ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    发明人： ULRICH SCHOERKEN ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    IPC分类号： C12P7/64

    CPC分类号： C12P7/6472

    摘要： Processes for the enzyme-catalyzed production of triglycerides using polyunsaturated fatty acids, in which (a) the reaction of polyunsaturated fatty acids and/or C1-4 alkyl esters thereof with glycerol in vacuo in the presence of an immobilized enzyme to form heir triglycerides is accelerated by addition of an additive from the group of weakly basic salts, complexing agents and ion exchangers and/or addition of a weakly basic salt and/or addition of an entraining agent in the form of a solvent or a gas and/or addition of glycerol-binding adsorbers and/or heat treatment of the partial glyceride intermediate product, (b) the immobilized enzymes are removed from the triglyceride by separation or filtration and (c) the remaining fatty acids and/or C1-4 alkyl esters thereof are removed from the triglyceride by distillation, refining or extraction.

    摘要翻译： 使用多不饱和脂肪酸酶催化生产甘油三酸酯的方法，其中（a）多不饱和脂肪酸和/或其中C 1-4烷基酯与甘油在真空中的存在下反应， 通过从弱碱性盐，络合剂和离子交换剂组中加入添加剂和/或加入弱碱性盐和/或加入溶剂形式的夹带剂来加速形成继承甘油三酯的固定化酶 或甘油结合吸附剂的气体和/或加成物和/或热处理部分甘油酯中间产物，（b）通过分离或过滤从甘油三酯中除去固定化的酶，和（c）剩余的脂肪酸和/或 通过蒸馏，精制或萃取，从甘油三酯中除去C 1-4烷基酯。

    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes
    4.
    发明申请
    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes 审中-公开
    在酶存在下生产不饱和脂肪酸甘油三酸酯的方法

    公开(公告)号：US20050233426A1

    公开(公告)日：2005-10-20

    申请号：US11093410

    申请日：2005-03-30

    申请人： Ulrich Schoerken ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    发明人： Ulrich Schoerken ,  Sabine Both ,  Carolin Meyer ,  Peter Horlacher

    IPC分类号： C11C3/06 ,  C11C3/10 ,  C12P7/64

    CPC分类号： C12P7/6472

    摘要： Processes for the enzyme-catalyzed production of triglycerides using polyunsaturated fatty acids, in which (a) the reaction of polyunsaturated fatty acids and/or C1-4 alkyl esters thereof with glycerol in vacuo in the presence of an immobilized enzyme to form their triglycerides is accelerated by addition of an additive from the group of weakly basic salts, complexing agents and ion exchangers and/or addition of a weakly basic salt and/or addition of an entraining agent in the form of a solvent or a gas and/or addition of glycerol-binding adsorbers and/or heat treatment of the partial glyceride intermediate product, (b) the immobilized enzymes are removed from the triglyceride by separation or filtration and (c) the remaining fatty acids and/or C1-4 alkyl esters thereof are removed from the triglyceride by distillation, refining or extraction.

    摘要翻译： 使用多不饱和脂肪酸酶催化生产甘油三酸酯的方法，其中（a）多不饱和脂肪酸和/或其中C 1-4烷基酯与甘油在真空中的存在下反应， 通过从弱碱性盐，络合剂和离子交换剂组中加入添加剂和/或加入弱碱性盐和/或以溶剂形式加入夹带剂来加速形成它们的甘油三酯的固定化酶 或甘油结合吸附剂的气体和/或加成物和/或热处理部分甘油酯中间产物，（b）通过分离或过滤从甘油三酯中除去固定化的酶，和（c）剩余的脂肪酸和/或 通过蒸馏，精制或萃取，从甘油三酯中除去C 1-4烷基酯。

    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes
    5.
    发明申请
    Processes for the production of triglycerides of unsaturated fatty acids in the presence of enzymes 审中-公开
    在酶存在下生产不饱和脂肪酸甘油三酸酯的方法

    公开(公告)号：US20050233427A1

    公开(公告)日：2005-10-20

    申请号：US11093534

    申请日：2005-03-30

    申请人： Ulrich Schoerken ,  Carolin Meyer ,  Sabine Both ,  Peter Horlacher

    发明人： Ulrich Schoerken ,  Carolin Meyer ,  Sabine Both ,  Peter Horlacher

    IPC分类号： C11C1/04 ,  C11C3/06 ,  C11C3/10 ,  C12P7/64

    CPC分类号： C12P7/6472 ,  C11C3/06

    摘要： Processes for the enzyme-catalyzed synthesis of triglycerides containing polyunsaturated fatty acids in which the synthesis is preceded by a pre-hydrolysis in which (a) C1-4 alkyl esters of polyunsaturated fatty acids are completely or partly hydrolyzed in vacuo with continuous addition of water or are partly hydrolyzed in several stages without vacuum, (b) after the hydrolysis, the water is removed by separation or distillation and (c) the synthesis of the polyunsaturated fatty acids with glycerol in vacuo in the presence of an enzyme to form their triglycerides is carried out under low-water conditions, (d) the enzymes are removed from the triglyceride by separation or filtration and (e) the remaining fatty acids and/or possible residues of C1-4 alkyl esters are removed from the triglyceride by distillation or refining; the pre-hydrolysis and the subsequent synthesis preferably being carried out as a one-pot process in the same reactor and in the presence of the same enzyme.

    摘要翻译： 用于酶催化合成含有多不饱和脂肪酸的甘油三酯的方法，其中合成之前是预水解，其中（a）多不饱和脂肪酸的C 1-4烷基酯是完全或部分 在不加入水的情况下在真空中水解或在几个阶段内没有真空部分水解，（b）水解后，通过分离或蒸馏除去水，和（c）在真空中合成甘油的多不饱和脂肪酸 在低水条件下进行酶的形成甘油三酯的存在，（d）通过分离或过滤从甘油三酯中除去酶，和（e）C 1的剩余脂肪酸和/或可能的残基 通过蒸馏或精制从甘油三酯中除去-4.0烷基酯; 预水解和随后的合成优选在相同的反应器中和在相同的酶的存在下作为一锅法进行。

    Method for producing conjugated linoleic acid
    6.
    发明申请
    Method for producing conjugated linoleic acid 失效
    共轭亚油酸的制备方法

    公开(公告)号：US20050255570A1

    公开(公告)日：2005-11-17

    申请号：US10516987

    申请日：2003-05-28

    申请人： Lars Zander ,  Stefan Busch ,  Carolin Meyer ,  Sabine Both ,  Ulrich Schoerken

    发明人： Lars Zander ,  Stefan Busch ,  Carolin Meyer ,  Sabine Both ,  Ulrich Schoerken

    IPC分类号： C12P7/64 ,  C12R1/05

    CPC分类号： C12P7/6427

    摘要： Processes for preparing conjugated linoleic acid are described wherein a conjugated linoleic acid lower alkyl ester is subjected to hydrolysis in the presence of an enzyme to form a hydrolyzate comprising a conjugated linoleic acid and a lower alkanol, wherein at least a portion of the lower alkanol is continuously removed; the hydrolyzate is separated into an organic phase and an aqueous/alcoholic phase; and the conjugated linoleic acid is separated from the organic phase.

    摘要翻译： 描述制备共轭亚油酸的方法，其中共轭亚油酸低级烷基酯在酶存在下进行水解以形成包含共轭亚油酸和低级链烷醇的水解产物，其中至少一部分低级烷醇为 连续删除 将水解产物分离成有机相和水相/醇相; 共轭亚油酸与有机相分离。

    Processes for preparing conjugated linoleic acid from conjugated linoleic acid esters
    7.
    发明授权
    Processes for preparing conjugated linoleic acid from conjugated linoleic acid esters 失效
    从共轭亚油酸酯制备共轭亚油酸的方法

    公开(公告)号：US07138256B2

    公开(公告)日：2006-11-21

    申请号：US10516987

    申请日：2003-05-28

    申请人： Lars Zander ,  Stefan Busch ,  Carolin Meyer ,  Sabine Both ,  Ulrich Schoerken

    发明人： Lars Zander ,  Stefan Busch ,  Carolin Meyer ,  Sabine Both ,  Ulrich Schoerken

    IPC分类号： C12P7/64

    CPC分类号： C12P7/6427

    摘要： Processes for preparing conjugated linoleic acid are described wherein a conjugated linoleic acid lower alkyl ester is subjected to hydrolysis in the presence of an enzyme to form a hydrolyzate comprising a conjugated linoleic acid and a lower alkanol, wherein at least a portion of the lower alkanol is continuously removed; the hydrolyzate is separated into an organic phase and an aqueous/alcoholic phase; and the conjugated linoleic acid is separated from the organic phase.

    摘要翻译： 描述制备共轭亚油酸的方法，其中共轭亚油酸低级烷基酯在酶存在下进行水解以形成包含共轭亚油酸和低级链烷醇的水解产物，其中至少一部分低级烷醇为 连续删除 将水解产物分离成有机相和水相/醇相; 共轭亚油酸与有机相分离。

    Production and Use of Monoglycerides
    10.
    发明申请
    Production and Use of Monoglycerides 有权
    单酸甘油酯的生产和使用

    公开(公告)号：US20080045606A1

    公开(公告)日：2008-02-21

    申请号：US11813939

    申请日：2006-01-10

    申请人： Ulrich Schoerken ,  Sabine Both ,  Frank Bongardt ,  Diana Stuhlmann

    发明人： Ulrich Schoerken ,  Sabine Both ,  Frank Bongardt ,  Diana Stuhlmann

    IPC分类号： A61K47/12 ,  A61P43/00 ,  A61Q99/00 ,  C12P7/64

    CPC分类号： C10L1/191 ,  A61K47/44 ,  C10L10/08 ,  C10M129/76 ,  C10M2207/289 ,  C12P7/6445 ,  C12P7/6472 ,  C12P7/649 ,  Y02E50/13

    摘要： A higher-yielding process for the production of monoglycerides in which triglycerides are enzymatically reacted with a catalytic amount of an esterase, preferably lipase, that has been activated by the addition of alkaline salts, in the presence of linear or branched alcohols containing 1 to 8 carbon atoms, then the esterase may be deactivated and it and the remaining alcohol removed, with the monoglycerides thus produced useful in lubricants, fuel additives, and emulsifying constituents in foods, and cosmetic and/or pharmaceutical formulations.

    摘要翻译： 用于生产甘油三酸酯的较高产量的方法，其中甘油三酸酯在催化量的酯酶（优选脂肪酶）中酶催化，其通过加入碱性盐在含有1至8个的直链或支链醇的存在下活化 碳原子，那么酯酶可以失活，并且其和除去的剩余的醇与由此产生的单酸甘油酯可用于食品中的润滑剂，燃料添加剂和乳化成分，以及化妆品和/或药物制剂。