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    Organic-inorganic composite
    11.
    发明授权
    Organic-inorganic composite 有权
    有机 - 无机复合材料

    公开(公告)号：US07048794B2

    公开(公告)日：2006-05-23

    申请号：US10952122

    申请日：2004-09-27

    Applicant: Christopher D. Tagge ,  Jacob Freas Pollock ,  Ken Saito

    Inventor： Christopher D. Tagge ,  Jacob Freas Pollock ,  Ken Saito

    IPC: C04B24/10 ,  C04B28/10 ,  C08L3/04 ,  C08L3/06 ,  C08L3/08

    CPC classification number: C04B28/14 ,  C04B24/383 ,  C04B2111/0062 ,  C08L3/04 ,  C04B20/023 ,  C04B14/42

    Abstract: An inorganic-organic composite comprises an inorganic phase, such as gypsum crystals, and a film forming organic phase. The film forming organic phase is selected from substituted starches having a degree of polymerization; degree of substitution and viscosity such that the substituted starches are insoluble in water during mixing but dissolve at a higher processing temperature during forming, setting or drying of the composite. Thus, excessive migration of the substitute starch is prevented and the composite is substantially strengthened.

    Abstract translation: 无机 - 有机复合材料包括无机相，例如石膏晶体和成膜有机相。 成膜有机相选自具有聚合度的取代淀粉; 取代度和粘度使得取代的淀粉在混合期间不溶于水，但在复合材料的成型，固化或干燥过程中在较高的加工温度下溶解。 因此，可以防止替代淀粉的过度迁移，并且复合物显着增强。

    Reaction calorimeter and differential scanning calorimeter for the high-throughput synthesis, screening and characterization of combinatorial libraries
    12.
    发明授权
    Reaction calorimeter and differential scanning calorimeter for the high-throughput synthesis, screening and characterization of combinatorial libraries 失效
    用于高通量合成，筛选和表征组合文库的反应量热计和差示扫描量热计

    公开(公告)号：US07033840B1

    公开(公告)日：2006-04-25

    申请号：US09708687

    申请日：2000-11-09

    Applicant: Christopher D. Tagge ,  Robert B. Wilson, Jr. ,  Seajin Oh ,  Albert S. Hirschon

    Inventor： Christopher D. Tagge ,  Robert B. Wilson, Jr. ,  Seajin Oh ,  Albert S. Hirschon

    IPC: G01N25/20 ,  G01N31/10

    CPC classification number: B01L3/50851 ,  B01J2219/00317 ,  B01J2219/00351 ,  B01J2219/00495 ,  B01J2219/00585 ,  B01J2219/00704 ,  B01J2219/00747 ,  B01L3/50853 ,  B01L2300/0654 ,  B01L2300/1827 ,  B01L2300/185 ,  B01L2400/065 ,  G01N25/4846 ,  H01J49/04

    Abstract: Workstation, apparatuses and methods for the high-throughput synthesis, screening and/or characterization of combinatorial libraries. The invention relates to an array, which permits various high-throughput methods for synthesis, screening and/or characterization in the same array, without requiring sample transfer from the array. In a preferred embodiment, the synthesis, screening, and/or characterization steps are carried out in a highly parallel fashion, where more than one compound is synthesized, screened, and/or characterized at the same time. The invention may be practiced at the microscale. The array may comprise thermal channels, for regulating the temperature of the wells in the array. The wells of the array may comprise a membrane, which is used in various screening and characterization methods. The invention also relates to a covered array, comprising the array and an array cover, as well as an apparatus comprising the array, which comprises the array, an array cover and a stage. The array, array cover, and the stage may be modified as required for a variety of synthesis and/or analysis techniques. The array is easily interchangeable between different analytical instruments, and in an embodiment, the invention relates to an automated workstation, where the array is transferred between different synthesis, screening, and characterization stations. The invention also relates to a variety of methods for synthesis, screening, and characterization, which are adapted for combinatorial chemistry. Any of the embodiments of the invention may be used either alone or taken in various combinations.

    Abstract translation: 用于组合库的高通量合成，筛选和/或表征的工作站，设备和方法。 本发明涉及阵列，其允许在相同阵列中进行合成，筛选和/或表征的各种高通量方法，而不需要从阵列转移样品。 在优选实施方案中，合成，筛选和/或表征步骤以高度平行的方式进行，其中多于一种化合物被同时合成，筛选和/或表征。 本发明可以在微尺度下实施。 阵列可以包括用于调节阵列中的阱的温度的热通道。 阵列的孔可以包括膜，其用于各种筛选和表征方法。 本发明还涉及包括阵列和阵列盖的覆盖阵列，以及包括阵列的装置，其包括阵列，阵列盖和台。 可以根据各种合成和/或分析技术的要求来修改阵列，阵列覆盖物和载物台。 该阵列在不同的分析仪器之间易于互换，并且在一个实施例中，本发明涉及自动化工作站，其中阵列在不同的合成，筛选和表征台之间传送。 本发明还涉及适用于组合化学的各种合成，筛选和表征的方法。 本发明的任何实施方案可以单独使用或以各种组合使用。

    Complexes of mid-transition metals and unsaturated nitrogenous ligands as single-site catalysts
    13.
    发明授权
    Complexes of mid-transition metals and unsaturated nitrogenous ligands as single-site catalysts 失效
    中间过渡金属和不饱和含氮配体的复合物作为单中心催化剂

    公开(公告)号：US06841676B2

    公开(公告)日：2005-01-11

    申请号：US10023920

    申请日：2001-12-17

    Applicant: Christopher D. Tagge ,  Robert B. Wilson, Jr.

    Inventor： Christopher D. Tagge ,  Robert B. Wilson, Jr.

    IPC: C07C251/12 ,  C07D213/53 ,  C07D241/12 ,  C07F7/00 ,  C07F11/00 ,  C08F4/02 ,  C08F4/22 ,  C08F4/78 ,  C08F10/00 ,  C07F9/80

    CPC classification number: C07D213/53 ,  C07C251/12 ,  C07D241/12 ,  C07F7/003 ,  C07F11/005 ,  C08F10/00 ,  C08F4/69034 ,  C08F4/69043 ,  C08F4/64013

    Abstract: Novel compounds are provided which are useful as catalysts, particularly in the polymerization of addition polymerizable monomers such as olefinic or vinyl monomers. The compounds are complexes of a mid-transition metal coordinated to at least two ligands, at least one of which is an unsaturated nitrogenous ligand. Depending on ligand substitution, stereospecific catalysts can be provided, including isospecific catalysts and syndiospecific catalysts. Catalyst systems containing the novel compounds in combination with a catalyst activator are provided as well, as are methods of using the novel compounds in the preparation of polyolefins. One embodiment of the present invention is a compound having the formula L1[MQ1Q2]L2 in which M is Nb, Ta, Mo, W, Mn or Re, Q1 and Q2 are each a univalent substituent, and L1 and L2 are ligands coordinated to M, wherein L1 contains a first coordinating nitrogen atom within a C═N group, and a second coordinating atom that is either a second nitrogen atom, optionally present in a second C═N group, or an oxygen, sulfur or phosphorus atom. The L2 group contains a coordinating atom that is either a second nitrogen atom, optionally within a C═N group, or a sulfur or phosphorus atom.

    Abstract translation: 提供了可用作催化剂的新型化合物，特别是在可加聚单体如烯属或乙烯基单体的聚合中。 这些化合物是与至少两个配体配位的中间过渡金属的络合物，其中至少一个是不饱和含氮配体。 取决于配体取代，可以提供立体特异性催化剂，包括异相催化剂和间同立构催化剂。 还提供了含有新型化合物与催化剂活化剂组合的催化剂体系，以及在制备聚烯烃中使用新化合物的方法。 本发明的一个实施方案是具有式L 1 [MQ 1 Q 2] L 2的化合物，其中M是Nb，Ta，Mo，W，Mn或Re，Q 1， 和Q 2各自是一价取代基，L 1和L 2是与M配位的配位体，其中L 1在C = N基团中含有第一配位氮原子，第二配位原子 即第二个氮原子，任选存在于第二个C = N基团中，或者是氧，硫或磷原子。 L 2基团包含任选在C = N基团中的第二氮原子或硫或磷原子的配位原子。

    Unsaturated nitrogenous compounds as electron donors for use with ziegler-natta catalysts
    14.
    发明授权
    Unsaturated nitrogenous compounds as electron donors for use with ziegler-natta catalysts 失效
    不饱和含氮化合物作为电子给体用于齐格勒 - 纳塔催化剂

    公开(公告)号：US06436864B1

    公开(公告)日：2002-08-20

    申请号：US09414131

    申请日：1999-10-06

    Applicant: Christopher D. Tagge

    Inventor： Christopher D. Tagge

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/6495 ,  C08F4/651

    Abstract: Unsaturated nitrogenous compounds are used as electron donors in conjunction with catalytic polymerization of addition polymerizable monomers such as olefins, using supported Ziegler-Natta catalysts. The electron donors may be used in the preparation of catalyst systems, thus serving as “internal” electron donors, or they may be added during or just prior to polymerization, as an “external” electron donor.

    Abstract translation: 使用负载的齐格勒 - 纳塔催化剂，将不饱和含氮化合物用作电子给体结合可加聚的单体如烯烃的催化聚合。 电子给体可用于制备催化剂体系，因此用作“内部”电子给体，或者它们可以在聚合过程中或之前加入作为“外部”电子给体。

    Mixed organic and inorganic composites with intermingled facial layers
    17.
    发明授权
    Mixed organic and inorganic composites with intermingled facial layers 有权
    混合的有机和无机复合材料与混合的面层

    公开(公告)号：US06846856B1

    公开(公告)日：2005-01-25

    申请号：US10442467

    申请日：2003-05-20

    Applicant: David S. Soane ,  Christopher D. Tagge

    Inventor： David S. Soane ,  Christopher D. Tagge

    IPC: C08K3/26 ,  C08K3/36 ,  C08K9/04 ,  C08K9/08

    CPC classification number: C08K9/04 ,  C08K9/08

    Abstract: A composite structure comprises an inorganic discrete phase, an organic matrix phase and an interfacial layer comprising both the inorganic and organic phases. In one process, the inorganic discrete phase is partially dissolved and the precipitated by a chemical reaction forming an interfacial layer having a finite thickness and transitioning from 100% inorganic to 100% organic.

    Abstract translation: 复合结构包括无机离散相，有机基质相和包含无机相和有机相的界面层。 在一个过程中，无机离散相部分溶解，并通过化学反应沉淀，形成具有有限厚度并从100％无机转变为100％有机物的界面层。

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