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    Process for preparing monochlorinated hydrocarbons having a high isomeric purity
    12.
    发明授权
    Process for preparing monochlorinated hydrocarbons having a high isomeric purity 失效
    具有高异构纯度的单氯代烃的方法

    公开(公告)号：US06756513B2

    公开(公告)日：2004-06-29

    申请号：US10219289

    申请日：2002-08-16

    Applicant: Manfred Neumann ,  Clemens Osterholt

    Inventor： Manfred Neumann ,  Clemens Osterholt

    IPC: C07C1702

    CPC classification number: C07C17/16 ,  C07C22/04 ,  C07C19/01

    Abstract: Monochlorinated hydrocarbons of high isomeric purity are prepared by a process, which comprises: reacting a monoalcohol having an alkyl radical having from 3 to 20 carbon atoms with cyanuric chloride; and purifying the resulting monochlorinated hydrocarbon by distillation after separation of salts and washing the monochlorinated hydrocarbon with alkali. The invention relates to a process for preparing monochlorinated hydrocarbons which contain an alkyl radical having from 3 to 20 carbon atoms and have a high isomeric purity by reacting a monoalcohol having a hydrocarbon radical containing an alkyl radical having from 3 to 20 carbon atoms to which additional cycloaliphatic radicals, aryl radicals, aralkyl radicals and alkylaryl radicals may be bound with cyanuric chloride, separating off salts, washing the reaction mixture with alkali and purifying the resulting monochlorinated hydrocarbons by distillation.

    Abstract translation: 通过一种方法制备高异构纯度的一氯化烃，该方法包括：使具有3-20个碳原子的烷基的一元醇与氰尿酰氯反应; 并在分离盐后通过蒸馏对所得一氯化烃进行纯化，并用碱洗涤一氯化烃。本发明涉及一种制备含有具有3至20个碳原子并具有高异构纯度的单氯代烃的方法，其通过使 具有含有具有3至20个碳原子的烷基的烃基的一元醇，其中另外的脂环族基团，芳基，芳烷基和烷基芳基可以与氰尿酰氯结合，分离出盐，用碱洗涤反应混合物并纯化 通过蒸馏得到单氯化烃。

    Method for preparing 1,3-dioxane compounds
    13.
    发明授权
    Method for preparing 1,3-dioxane compounds 失效
    1,3-二恶烷化合物的制备方法

    公开(公告)号：US5932747A

    公开(公告)日：1999-08-03

    申请号：US44995

    申请日：1998-03-20

    Applicant: Frank Bauer ,  Manfred Neumann

    Inventor： Frank Bauer ,  Manfred Neumann

    IPC: C07D317/72 ,  C07D319/06 ,  C07D319/08

    CPC classification number: C07D317/72 ,  C07D319/06

    Abstract: A method for preparing 1,3-dioxane compounds of the formula (I): ##STR1## wherein R.sup.1 and R.sup.2, independently of one another, represent hydrogen or a hydrocarbon radical; and X.sup.1 and X.sup.2, independently of one another, represent an electronegative groups, which method entails reacting a bis(hydroxymethyl) compound of the formula (II): ##STR2## in which X.sup.1 and X.sup.2 each, independently of one another, are as defined above, with an orthocarboxylic acid ester of the formula R.sup.4 --C(OR.sup.5).sub.3 (III), in which R.sup.4 represents hydrogen or a hydrocarbon radical and R.sup.5 represents a hydrocarbon radical, and with an aldehyde or ketone of the formula R.sup.1 --CO--R.sup.2 (IV), in which R and R each, independently of one another, are as defined above.

    Abstract translation: 一种制备式（I）的1,3-二恶烷化合物的方法：其中R1和R2彼此独立地代表氢或烃基; 并且X1和X2彼此独立地表示电负性基团，该方法需要使式（II）的双（羟甲基）化合物反应：其中X1和X2各自彼此独立地如上定义，与 式R 4 -C（OR 5）3（III）的原羧酸酯，其中R 4表示氢或烃基，R 5表示烃基，并且与式R 1 -CO-R 2（IV）的醛或酮 ），其中R和R各自彼此独立地如上所定义。

    Cigarette tube filling device
    14.
    发明授权
    Cigarette tube filling device 失效
    香烟管灌装装置

    公开(公告)号：US5657768A

    公开(公告)日：1997-08-19

    申请号：US596368

    申请日：1996-02-22

    Applicant: Manfred Neumann ,  Josef Lier

    Inventor： Manfred Neumann ,  Josef Lier

    IPC: A24C5/42 ,  A24C5/00

    CPC classification number: A24C5/42

    Abstract: The cigarette tube filling device (100) comprises a housing bottom part (1), consisting of a base part (2) and of a cover part (3), as well as a housing top part (6). There is formed a press chamber (8), the lower half of which is formed by a tongue (12) and the upper half (11) of which is formed by a part-cylindrical recess (11) of the top part (6). The housing top part (6) is mounted on the housing bottom part (1) pivotably about an axis (7) extending parallel to the press chamber (8). In the housing bottom part (1), a straight guide (27, 28) parallel to the press chamber (8) is provided for the slide (20) comprising the tongue (12).

    Abstract translation: PCT No.PCT / DE94 / 00930 Sec。 371日期1996年2月22日 102（e）日期1996年2月22日PCT 1994年8月13日PCT PCT。 公开号WO95 / 05756 日期1995年3月2日香烟管填充装置（100）包括由基部（2）和盖部分（3）组成的壳体底部部分（1）以及壳体顶部部分（6）。 形成有压力室（8），其下半部分由舌部（12）形成，上半部分（11）由顶部部分（6）的部分圆柱形凹部（11）形成， 。 壳体顶部部分（6）围绕平行于压力室（8）延伸的轴线（7）可枢转地安装在壳体底部部分（1）上。 在壳体底部部分（1）中，为包括舌部（12）的滑动件（20）提供平行于压力室（8）的直的引导件（27,28）。

    Method for plasma-assisted reactive electron beam vaporization
    15.
    发明授权
    Method for plasma-assisted reactive electron beam vaporization 失效
    等离子体辅助反应电子束蒸发的方法

    公开(公告)号：US5614248A

    公开(公告)日：1997-03-25

    申请号：US424418

    申请日：1995-05-30

    Applicant: Siegfried Schiller ,  Manfred Neumann ,  Volker Kirchhoff ,  Gerhard Zeissig ,  Nicolas Schiller ,  Klaus Goedicke

    Inventor： Siegfried Schiller ,  Manfred Neumann ,  Volker Kirchhoff ,  Gerhard Zeissig ,  Nicolas Schiller ,  Klaus Goedicke

    IPC: C23C14/30 ,  C23C14/00 ,  C23C14/32 ,  C23C14/54 ,  C23C14/56 ,  B05D3/06 ,  H05H1/02

    CPC classification number: C23C14/54 ,  C23C14/0021

    Abstract: Certain non-optical characteristics and, in particular, mechanical characteristics are not measurable in situ in the industrial production of layers using plasma-assisted reactive electron beam vaporization, particularly if high demands are made on the hardness, wear resistance and barrier action, so as to be able to reproducibly apply the layers. The values of the optical layer characteristics are to be used as a control signal. In this method, immediately after the substrate has passed through the vaporizing zone, the reflection and/or transmission and absorption capacity are measured in the wavelength range .DELTA..sub.k =150 to 800 nm and from this are determined the refractive index and optical absorption coefficient. These determined values are compared with an experimentally determined desired value. A control signal obtained therefrom, in the case of a constant reactive gas partial pressure, controls the plasma and maintains constant the optical characteristics of the layer. The method is used in the vapor-deposition of wear-resistance, hard layers or barrier layers, e.g. of metal oxide on glass, plastic and other materials, e.g. in the building industry for facade glass and in the packaging industry.

    Abstract translation: PCT No.PCT / DE93 / 00748 Sec。 371日期：1995年5月30日 102（e）日期1995年5月30日PCT提交1993年8月18日PCT公布。 公开号WO94 / 10356 日期1994年5月11日具有非光学特性，特别是在使用等离子体辅助的反应电子束蒸发的工业生产中不能测量机械特性，特别是如果对硬度，耐磨性和阻挡层有高要求 动作，以便能够可重复地应用层。 光层特性的值被用作控制信号。 在该方法中，在基板通过蒸发区之后，在DELTA k = 150〜800nm的波长范围内测定反射和/或透射吸收能力，由此确定折射率和光吸收系数。 将这些确定的值与实验确定的期望值进行比较。 在恒定的反应气体分压的情况下，从其获得的控制信号控制等离子体并保持该层的光学特性恒定。 该方法用于耐磨性，硬质层或阻挡层的气相沉积，例如， 玻璃，塑料和其他材料上的金属氧化物，例如。 在建筑行业的立面玻璃和包装行业。

    Device for filling cigarette tubes
    16.
    发明授权
    Device for filling cigarette tubes 失效
    用于灌装香烟管的装置

    公开(公告)号：US5398701A

    公开(公告)日：1995-03-21

    申请号：US949803

    申请日：1993-04-08

    Applicant: Manfred Neumann ,  Josef Lier ,  Wolfgang Rosner

    Inventor： Manfred Neumann ,  Josef Lier ,  Wolfgang Rosner

    IPC: A24C5/42 ,  A24C5/00 ,  A24C5/06 ,  A24F47/00

    CPC classification number: A24C5/425

    Abstract: A device for filling prefabricated cigarette tubes, having a housing (1), a tobacco chamber (17), a trough-shaped tobacco holder (7), a compression bar (23), a stop (31) for one end of the plug of tobacco, a finger or bushing (14) on which one end of a cigarette tube can be placed and a sliding cover (11). The length of the plug of tobacco formed can be adjusted to fit cigarette tubes of different lengths by adjusting the length of the tobacco chamber (17) and the length of the compression bar (23). The invention does this by virtue of the fact that the stop (31) defining one end of the tobacco chamber is adjustable in a direction parallel to the longitudinal axis of the tobacco holder (7) and that at least two movable sections (41, 42, 43) of the compression bar, each of different length and each capable of acting as an extension to a stationary part (30) of the bar, are mounted on a rotatable component (40) whose axis of rotation (45) is parallel to the surface (44) of the compression bar.

    Abstract translation: PCT PCT / DE92 / 00261 Sec。 371日期：1993年4月8日 102（e）日期1993年4月8日PCT提交于1992年3月30日PCT公开号 出版物WO92 / 17078 一种用于填充预制香烟管的装置，具有壳体（1），烟草室（17），槽形烟草支架（7），压缩杆（23），止动件（31） ），烟丝插头的一端，可以放置香烟管的一端的手指或衬套（14）和滑盖（11）。 可以通过调节烟草室（17）的长度和压缩杆（23）的长度来调节形成烟草的塞子的长度以适应不同长度的香烟管。 本发明通过限定烟草室的一端的止动件（31）在平行于烟草支架（7）的纵向轴线的方向上是可调节的，并且至少两个可移动部分（41,42 每个不同长度并且每个能够用作到杆的固定部分（30）的延伸部的压缩杆（43）安装在其旋转轴线（45）平行于 压缩杆的表面（44）。

    Pressure filtration device
    17.
    发明授权
    Pressure filtration device 失效

    公开(公告)号：US4136029A

    公开(公告)日：1979-01-23

    申请号：US889738

    申请日：1978-03-24

    Applicant: Klaus Cosack ,  Wolfgang Hein ,  Manfred Neumann

    Inventor： Klaus Cosack ,  Wolfgang Hein ,  Manfred Neumann

    IPC: B01D29/05 ,  B01D25/00

    CPC classification number: B01D29/05

    Abstract: A pressure filtration apparatus including an upper portion with an inflow channel and a discharge channel for the concentrate and a lower portion with a filter support and a discharge channel for the filtrate, the upper and lower portions being releaseably connectable with one another while forming a pressure space. The apparatus contains a distributor plate whose underside is disposed parallel to the upper side of the filter and snugly above the latter while forming an intervening space, and in the center of which is an opening for the concentrate discharge channel. The outer edge of the distributor plate forms a small annular opening which extends all around closely against a basically vertically interior of the pressure space. The top side of the distributor plate has a peripherally raised outer edge which while forming a narrow annular clearance extends to close up against a downwardly pointing horizontal interior wall of the upper portion. The distributor plate has an annular distributor ring surface which grows steadily deeper from the outer edge toward the center of the distributor plate and in the center has a short connecting bushing by way of which the distributor plate is secured to the upper portion and through which the discharge channel for the concentrate runs. The apparatus also includes an inflow channel which opens up in the upper portion in the region of the deepest point of the distributor ring surface above the latter, and at least along a length disposed in front of the opening determining the direction of flow of the emerging inflow current, slopes toward the horizontal at an angle of about 35.degree. to about 55.degree., preferably about 45.degree., and relative to the vertical projection of its axis runs basicaly tangentially to the vertical projection of the distributor ring surface.In preferred embodiments of the invention, the upper portion, lower portion, the distributor plate, the inflow channel, the inflow channel bushing, the filter support, the filtrate discharge channel, and the filtrate discharge bushing may be made of polytetrafluoroethylene (PTFE). If all are made of PTFE, the inflow, the concentrate and the filtrate will be in contact only with PTFE.

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