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    Method for producing highly-branched glycidol-based polyols
    11.
    发明授权
    Method for producing highly-branched glycidol-based polyols 失效
    高度支化的缩水甘油基多元醇的制备方法

    公开(公告)号：US06822068B2

    公开(公告)日：2004-11-23

    申请号：US10335667

    申请日：2003-01-02

    Applicant: Alexander Sunder ,  Rolf Mülhaupt

    Inventor： Alexander Sunder ,  Rolf Mülhaupt

    IPC: C08G6528

    CPC classification number: C08G18/48 ,  C08G65/22 ,  C08G65/2648

    Abstract: This invention relates to a process for the preparation of highly-branched polyols by polymerisation of glycidol in the presence of a hydrogen-active starter compound with basic catalysis, wherein glycidol is added in dilute solution and the solvent used for the dilution is continuously distilled off. The polyols thus prepared are colorless, contain as the core unit solely the starter compound used and have polydispersities of less than 1.7. The present invention also relates to polyols that comprise the reaction product of the polyols based on glycidol with one or more expoxide monomers. This invention also relates to a process for the preparation of these polyols.

    Abstract translation: 本发明涉及通过在具有碱催化作用的氢活化起始化合物存在下缩水甘油聚合来制备高支化多元醇的方法，其中将缩水甘油加入稀溶液中，用于稀释的溶剂被连续地蒸馏掉 。 如此制备的多元醇是无色的，仅含有起始化合物的核心单元，并且具有小于1.7的多分散性。 本发明还涉及包含基于缩水甘油的多元醇与一种或多种过氧化物单体的反应产物的多元醇。 本发明还涉及制备这些多元醇的方法。

    POLYMER- GRAPHITE NANOCOMPOSITES
    14.
    发明申请
    POLYMER- GRAPHITE NANOCOMPOSITES 有权
    聚合物 - 石墨纳米复合材料

    公开(公告)号：US20120187348A1

    公开(公告)日：2012-07-26

    申请号：US13496806

    申请日：2010-09-13

    Applicant: Hans-Helmut Görtz ,  Rolf Minkwitz ,  Rolf Mülhaupt ,  Rainer Wissert ,  Peter Steurer

    Inventor： Hans-Helmut Görtz ,  Rolf Minkwitz ,  Rolf Mülhaupt ,  Rainer Wissert ,  Peter Steurer

    IPC: H01B1/24

    CPC classification number: C08K3/04 ,  C08J3/215 ,  C08J2325/12 ,  C08K3/041 ,  C08K2201/011 ,  H01B1/24 ,  C08L25/12

    Abstract: Process for producing a polymer-graphite nanocomposite, which comprises the steps a) oxidation of graphite to graphite oxide, b) conversion of the graphite oxide into an aqueous dispersion, c) mixing of the aqueous dispersion comprising graphite oxide or, if appropriate, reduced graphite oxide which is obtained from b) with an aqueous polymer dispersion comprising at least one polymer and d) separating off the polymer-graphite mixture from the aqueous phase, wherein the graphite oxide which has been oxidized in step a) is reduced to graphite between step b) and c) or between step c) and d).

    Abstract translation: 制备聚合物 - 石墨纳米复合材料的方法，其包括以下步骤：a）将石墨氧化成氧化石墨，b）将石墨氧化物转化为水分散体，c）将包含氧化石墨的水性分散体，或如果合适的话， 由b）得到的石墨氧化物与包含至少一种聚合物的聚合物水分散体分散体，和d）从水相中分离出聚合物 - 石墨混合物，其中在步骤a）中被氧化的氧化石墨被还原成石墨在 步骤b）和c）或步骤c）和d）之间。

    Catalyst system for polymerization of olefinic monomers, process for preparing polymers, and polymers prepared by the process
    15.
    发明授权
    Catalyst system for polymerization of olefinic monomers, process for preparing polymers, and polymers prepared by the process 失效
    用于聚合烯烃单体的催化剂体系，制备聚合物的方法和通过该方法制备的聚合物

    公开(公告)号：US08133832B2

    公开(公告)日：2012-03-13

    申请号：US12452713

    申请日：2008-07-22

    Applicant: Marc Oliver Kristen ,  Rolf Mülhaupt ,  Georg Müller

    Inventor： Marc Oliver Kristen ,  Rolf Mülhaupt ,  Georg Müller

    IPC: C08F4/02 ,  C08F4/642 ,  C08F4/6592

    CPC classification number: C08F10/00 ,  C08F4/65925 ,  Y10S526/943 ,  Y10T428/249924 ,  C08F4/027

    Abstract: The present invention relates to new catalyst supports comprising nanofibers, a catalyst system comprising these supports as well as a process for preparing nanocomposites and the nanocomposites prepared. The invention especially concerns a supported catalyst system for polymerization of olefins, comprising a support made of fibers or a fleece of fibers, wherein the mean fiber diameter is less than 1000 nm, preferably less than 500 nm and the mean fiber length is more than 200,000 nm, preferably more than 500,000 nm and especially preferred more than 1,000,000 nm as well as a process for polymerizing olefinic systems in the presence of these catalyst systems and the resulting nanocomposites.

    Abstract translation: 本发明涉及包含纳米纤维的新催化剂载体，包含这些载体的催化剂体系以及制备纳米复合材料的方法和制备的纳米复合材料。 本发明特别涉及用于烯烃聚合的负载型催化剂体系，其包括由纤维制成的载体或纤维的绒毛，其中平均纤维直径小于1000nm，优选小于500nm，平均纤维长度大于20万 nm，优选大于500,000nm，特别优选大于1,000,000nm，以及在这些催化剂体系存在下聚合烯属体系的方法和所得的纳米复合材料。

    Method for the emulsion polymerization of olefins
    17.
    发明授权
    Method for the emulsion polymerization of olefins 失效
    烯烃乳液聚合方法

    公开(公告)号：US07129292B1

    公开(公告)日：2006-10-31

    申请号：US10168113

    申请日：2000-10-18

    Applicant: Marc Oliver Kristen ,  Lambertus Manders ,  Stefan Mecking ,  Florian M. Bauers ,  Rolf Mülhaupt

    Inventor： Marc Oliver Kristen ,  Lambertus Manders ,  Stefan Mecking ,  Florian M. Bauers ,  Rolf Mülhaupt

    IPC: C08F2/16

    CPC classification number: C08F10/02 ,  C08F10/00 ,  C08F2/22 ,  C08F4/80 ,  C08F4/7006 ,  C08F4/7031 ,  C08F4/7022 ,  C08F4/7027 ,  C08F4/7019

    Abstract: A process for emulsion polymerizing one or more olefins involves reacting it/them with at least one complex compound of the formula Ia or b where M is a transition metal from groups 7 to 10 of the Periodic Table of the Elements and is preferably Ni in aqueous dispersion and at least one radical R1 to R3 and optionally one radical R4 to R9 contains a hydrophilic group X, selection being made from —SO3−, —O—PO32−, NH(R15)2+, N(R15)3+ or —(OCH2CH2)nOH, where n is an integer between 1 and 15. For the process of the invention it is optional to use an activator such as, for example, olefin complexes of rhodium or of nickel. This invention further relates to dispersions of polyolefins such as polyethylene and ethylene copolymers in water, for example, and to the use of the aqueous dispersions of the invention for paper applications such as paper coating or surface sizing, paints, adhesive base materials, molded foams such as mattresses, textile and leather applications, carpet back coatings, or pharmaceutical applications.

    Abstract translation: 用于将一种或多种烯烃乳液聚合的方法涉及使其与至少一种式Ia或b的络合物反应，其中M是元素周期表第7至10族的过渡金属，并且优选为Ni 分散体和至少一个R 1至R 3基团和任选的一个基团R 4至R 9包含一个 亲水基团X，选自-SO 3 - ， - O-PO 3 - ， - NH 2， - NH （R 15）2 N 2 O 3 N（R 15）3 或+ - 或 - （OCH 2 CH 2）n OH，其中n是1和15之间的整数。对于 本发明的方法任选使用活化剂，例如铑或镍的烯烃络合物。 本发明还涉及聚烯烃如聚乙烯和乙烯共聚物在水中的分散体，以及本发明的水性分散体用于纸张涂布或表面施胶，涂料，粘合剂基材，模塑泡沫 例如床垫，纺织和皮革应用，地毯背部涂层或药物应用。

    Method for producing highly-branched glycidol-based polyols
    18.
    发明授权
    Method for producing highly-branched glycidol-based polyols 失效
    高度支化的缩水甘油基多元醇的制备方法

    公开(公告)号：US06765082B2

    公开(公告)日：2004-07-20

    申请号：US10335681

    申请日：2003-01-02

    Applicant: Alexander Sunder ,  Rolf Mülhaupt

    Inventor： Alexander Sunder ,  Rolf Mülhaupt

    IPC: C08G6526

    CPC classification number: C08G18/48 ,  C08G65/22 ,  C08G65/2648

    Abstract: This invention relates to as process for the preparation of highly-branched polyols by polymerization of glycidol in the presence of a hydrogen-active starter compound with basic catalysis, wherein glycidol is added in dilute solution and the solvent used for the dilution is continuously distilled off. The polyols thus prepared are colorless, contain as the core unit solely the starter compound used and have polydispersities of less than 1.7.

    Abstract translation: 本发明涉及通过在具有碱催化作用的氢活化起始化合物存在下，缩水甘油聚合制备高支化多元醇的方法，其中将缩水甘油加入稀溶液中，用于稀释的溶剂被连续蒸馏除去 。 如此制备的多元醇是无色的，仅含有起始化合物的核心单元，并且具有小于1.7的多分散性。

    Filler mixtures
    19.
    发明授权
    Filler mixtures 失效
    填料混合物

    公开(公告)号：US06683122B1

    公开(公告)日：2004-01-27

    申请号：US10031134

    申请日：2002-01-14

    Applicant: Carsten Zilg ,  Rolf Mülhaupt ,  Jürgen Finter

    Inventor： Carsten Zilg ,  Rolf Mülhaupt ,  Jürgen Finter

    IPC: C08K904

    CPC classification number: C08K9/04 ,  C08K3/013

    Abstract: A filler mixture comprising an organophilic layer silicate obtainable by treatment of a natural or synthetic layer silicate with a swelling agent selected from sulfonium, phosphonium and ammonium compounds (salts of melamine compounds and cyclic amidine compounds being excluded as ammonium compounds) and a mineral filler different therefrom, yields, in combination with thermosetting resins, nanocomposites having improved mechanical properties.

    Abstract translation: 一种填料混合物，其包含通过用选自锍，鏻和铵化合物的溶胀剂（三聚氰胺化合物的盐和作为铵化合物排除的环状脒化合物）处理天然或合成层状硅酸盐而获得的亲有机层硅酸盐和不同的矿物填料 与热固性树脂组合产生具有改进的机械性能的纳米复合材料。

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