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11.发明授权Fischer-Tropsch synthesis using microchannel technology and novel catalyst and microchannel reactor 有权使用微通道技术的费 - 托合成和新型催化剂和微通道反应器公开(公告)号：US09023900B2
公开(公告)日：2015-05-05
申请号：US13397942
申请日：2012-02-16
Applicant: Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
Inventor： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
IPC: C10G2/00 , C07C1/04 , B01J19/00 , B01J37/03 , B01J38/48 , B01J23/94 , B01J37/02 , B01J23/755 , B01J23/83 , B01J23/889 , B01J23/89 , B01J35/00 , B01J35/04 , B01J35/10 , C10G45/58 , C10G47/00 , B01J23/75 , B01J21/04 , B01J38/58
CPC classification number: C10G2/332 , B01J19/0093 , B01J23/75 , B01J23/755 , B01J23/83 , B01J23/8896 , B01J23/8913 , B01J23/892 , B01J23/894 , B01J23/8986 , B01J23/94 , B01J35/0066 , B01J35/04 , B01J35/1019 , B01J35/1038 , B01J37/0201 , B01J37/0205 , B01J37/038 , B01J38/48 , B01J38/58 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00835 , B01J2219/00855 , B01J2219/0086 , B01J2219/00873 , C10G2/331 , C10G2/334 , C10G2/34 , C10G2/341 , C10G21/00 , C10G45/58 , C10G47/00 , C10G2300/1022 , C10G2400/04 , C10G2400/10 , C10L1/08 , C10L2200/0492 , C10L2270/026 , C10L2290/42 , C10L2290/544 , C10M105/04 , Y02P20/582
Abstract: Disclosed is a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. Also disclosed is a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
Abstract translation: 公开了一种将包含H 2和CO的反应物组合物转化为包含至少一种具有至少约5个碳原子的脂族烃的产物的方法，该方法包括：使反应物组合物流过与费 - 托催化剂接触的微通道反应器 将反应物组合物转化成产物，微通道反应器包含多个含有催化剂的工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。 还公开了包含Co的载体催化剂和包含至少一个工艺微通道和至少一个相邻的热交换区的微通道反应器。
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12.发明授权Process for conducting an equilibrium limited chemical reaction using microchannel technology 有权使用微通道技术进行均衡有限化学反应的方法公开(公告)号：US08747805B2
公开(公告)日：2014-06-10
申请号：US10777033
申请日：2004-02-11
Applicant: Anna Lee Tonkovich , Kai Tod Paul Jarosch , Terry Mazanec , Francis P. Daly , Rachid Taha , Enrique Aceves de Alba
Inventor： Anna Lee Tonkovich , Kai Tod Paul Jarosch , Terry Mazanec , Francis P. Daly , Rachid Taha , Enrique Aceves de Alba
CPC classification number: C01B3/02 , B01J19/0093 , B01J21/12 , B01J23/80 , B01J35/0006 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00862 , B01J2219/00873 , C01B2203/02 , C01B2203/06 , C01B2203/0805 , Y02P20/582
Abstract: The disclosed invention relates to a process for conducting an equilibrium limited chemical reaction in a microchannel reactor. The process involves the use of active heat exchange and is suitable for conducting exothermic and endothermic reactions. The process is particularly suitable for synthesizing methanol and dimethyl ether.
Abstract translation: 所公开的发明涉及在微通道反应器中进行平衡限制化学反应的方法。 该方法涉及使用活性热交换并适用于进行放热和吸热反应。 该方法特别适用于合成甲醇和二甲醚。
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13.发明申请公开(公告)号：US20130217793A1
公开(公告)日：2013-08-22
申请号：US13397942
申请日：2012-02-16
Applicant: Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
Inventor： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
CPC classification number: C10G2/332 , B01J19/0093 , B01J23/75 , B01J23/755 , B01J23/83 , B01J23/8896 , B01J23/8913 , B01J23/892 , B01J23/894 , B01J23/8986 , B01J23/94 , B01J35/0066 , B01J35/04 , B01J35/1019 , B01J35/1038 , B01J37/0201 , B01J37/0205 , B01J37/038 , B01J38/48 , B01J38/58 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00835 , B01J2219/00855 , B01J2219/0086 , B01J2219/00873 , C10G2/331 , C10G2/334 , C10G2/34 , C10G2/341 , C10G21/00 , C10G45/58 , C10G47/00 , C10G2300/1022 , C10G2400/04 , C10G2400/10 , C10L1/08 , C10L2200/0492 , C10L2270/026 , C10L2290/42 , C10L2290/544 , C10M105/04 , Y02P20/582
Abstract: The disclosed invention relates to a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. The disclosed invention also relates to a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
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14.发明授权Process and apparatus for improved methods for making vinyl acetate monomer (VAM) 有权制备乙酸乙烯酯单体（VAM）的改进方法的方法和设备公开(公告)号：US08029748B2
公开(公告)日：2011-10-04
申请号：US12272804
申请日：2008-11-18
Applicant: Terry Mazanec , Victor J. Johnston , Michael Huckman , Sean P. Fitzgerald , James A. Foster , Daniel Lindley , Anna Lee Tonkovich , Francis P. Daly , Leslie Wade , Tony Hammock , Thomas Yuschak , Bin Yang , Kai Jarosch
Inventor： Terry Mazanec , Victor J. Johnston , Michael Huckman , Sean P. Fitzgerald , James A. Foster , Daniel Lindley , Anna Lee Tonkovich , Francis P. Daly , Leslie Wade , Tony Hammock , Thomas Yuschak , Bin Yang , Kai Jarosch
CPC classification number: B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00862 , B01J2219/00873 , B01J2219/00889 , C07C67/055 , C07C69/01 , C07C69/15
Abstract: The invention provides methods, apparatus and chemical systems for making vinyl acetate from ethylene, oxygen, and acetic acid.
Abstract translation: 本发明提供从乙烯，氧和乙酸制备乙酸乙烯酯的方法，装置和化学体系。
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15.发明授权公开(公告)号：US07999144B2
公开(公告)日：2011-08-16
申请号：US11469847
申请日：2006-09-01
Applicant: Anna Lee Tonkovich , Bin Yang , Steven T. Perry , Terry Mazanec , Ravi Arora , Francis P. Daly , Richard Long , Thomas D. Yuschak , Paul W. Neagle , Amanda Glass
Inventor： Anna Lee Tonkovich , Bin Yang , Steven T. Perry , Terry Mazanec , Ravi Arora , Francis P. Daly , Richard Long , Thomas D. Yuschak , Paul W. Neagle , Amanda Glass
IPC: C07C5/32
CPC classification number: C07C5/48 , B01J19/0093 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/00891 , B01J2219/00984 , C01B3/386 , C01B3/50 , C01B2203/0261 , C01B2203/04 , C01B2203/048 , C01B2203/1035 , C01B2203/1041 , C01B2203/1064 , C01B2203/107 , C01B2203/1247 , C07C2523/42 , C07C2523/44 , C07C2523/52 , C07C11/04
Abstract: Methods of oxidative dehydrogenation are described. Surprisingly, Pd and Au alloys of Pt have been discovered to be superior for oxidative dehydrogenation in microchannels. Methods of forming these catalysts via an electroless plating methodology are also described. An apparatus design that minimizes heat transfer to the apparatus' exterior is also described.
Abstract translation: 描述了氧化脱氢方法。 令人惊奇的是，已经发现Pt的Pd和Au合金对于微通道中的氧化脱氢是优越的。 还描述了通过化学镀方法形成这些催化剂的方法。 还描述了最小化到设备外部的热传递的设备设计。
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Patent Agency Ranking
16.发明申请Protected Alloy Surfaces In Microchannel Apparatus and Catalysts, Alumina Supported Catalysts, Catalyst Intermediates, and Methods of Forming Catalysts and Microchannel Apparatus 有权微通道设备和催化剂中的保护合金表面，氧化铝负载催化剂，催化剂中间体和形成催化剂和微通道装置的方法公开(公告)号：US20110182804A1
公开(公告)日：2011-07-28
申请号：US13012797
申请日：2011-01-24
Applicant: Richard Long , Barry L. Yang , Francis P. Daly , Junko M. Watson , Terry Mazanec , Sean P. Fitzgerald , Bradley R. Johnson , Xiaohong Li , Chunshe Cao , Ya-Huei Chin , Anna Lee Tonkovich , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang
Inventor： Richard Long , Barry L. Yang , Francis P. Daly , Junko M. Watson , Terry Mazanec , Sean P. Fitzgerald , Bradley R. Johnson , Xiaohong Li , Chunshe Cao , Ya-Huei Chin , Anna Lee Tonkovich , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang
CPC classification number: C01B3/384 , B01J19/0093 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/0236 , C01B2203/0233 , C01B2203/0811 , C23C8/10 , C23C16/12 , C23C16/56 , H01M2008/1293 , Y02P20/52 , Y10S585/92 , Y10S585/924
Abstract: The invention describes microchannel apparatus and catalysts that contain a layer of a metal aluminide or are made in a process in which a metal aluminide layer is formed as an intermediate. Certain processing conditions have surprisingly been found to result in superior coatings. The invention includes chemical processes conducted through apparatus described in the specification. Other catalysts and catalyst synthesis techniques are also described.
Abstract translation: 本发明描述了包含金属铝化物层的微通道装置和催化剂，或者是在其中形成金属铝化物层作为中间体的方法制造的。 令人惊奇地发现某些加工条件导致优异的涂层。 本发明包括通过本说明书中描述的设备进行的化学过程。 还描述了其它催化剂和催化剂合成技术。
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公开(公告)号：US20100174124A1
公开(公告)日：2010-07-08
申请号：US12576458
申请日：2009-10-09
Applicant: Anna Lee Tonkovich , Ravi Arora , John Brophy , Francis P. Daly , Soumitra Deshmukh , Maddalena Fanelli , Kai Tod Paul Jarosch , Timothy J. LaPlante , Richard Q. Long , Terry Mazanec , Daniel Francis Ryan , Laura J. Silva , Wayne W. Simmons , Bruce Stangeland , Yong Wang , Thomas Yuschak , Steven T. Perry , Jeffrey Dale Marco , Michael Alan Marchiando , Robert Dwayne Litt
Inventor： Anna Lee Tonkovich , Ravi Arora , John Brophy , Francis P. Daly , Soumitra Deshmukh , Maddalena Fanelli , Kai Tod Paul Jarosch , Timothy J. LaPlante , Richard Q. Long , Terry Mazanec , Daniel Francis Ryan , Laura J. Silva , Wayne W. Simmons , Bruce Stangeland , Yong Wang , Thomas Yuschak , Steven T. Perry , Jeffrey Dale Marco , Michael Alan Marchiando , Robert Dwayne Litt
CPC classification number: C10G47/14 , B01J19/0093 , B01J21/12 , B01J23/42 , B01J23/75 , B01J23/96 , B01J35/023 , B01J2219/00783 , B01J2219/00788 , B01J2219/00835 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00984 , C10G2/32 , C10G45/02 , C10G47/00 , C10G47/02 , C10G2300/202 , C10G2300/4018 , Y02P20/582
Abstract: This invention relates to a process for conducting a hydrocracking or a hydrotreating process in a microchannel reactor. This invention also relates to a process and apparatus for flowing a vapor and liquid into a plurality of microchannels in a microchannel processing unit.
Abstract translation: 本发明涉及在微通道反应器中进行加氢裂化或加氢处理工艺的方法。 本发明还涉及一种将蒸汽和液体流入微通道处理单元中的多个微通道的方法和装置。
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18.发明授权Process for conducting an equilibrium limited chemical reaction in a single stage process channel 有权在单级过程通道中进行平衡有限化学反应的方法公开(公告)号：US07255845B2
公开(公告)日：2007-08-14
申请号：US11201795
申请日：2005-08-11
Applicant: Anna Lee Tonkovich , Wayne W. Simmons , Kai Tod Paul Jarosch , Terry Mazanec , Eric Daymo , Ying Peng , Jennifer Lynne Marco
Inventor： Anna Lee Tonkovich , Wayne W. Simmons , Kai Tod Paul Jarosch , Terry Mazanec , Eric Daymo , Ying Peng , Jennifer Lynne Marco
IPC: C01B3/16
CPC classification number: B01J19/0093 , B01J23/80 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , C01B3/16 , C01B2203/0283 , C01B2203/1041 , Y02P20/52
Abstract: This invention relates to a process for conducting an equilibrium limited chemical reaction in a single stage process channel. A process for conducting a water shift reaction is disclosed. A multichannel reactor with cross flow heat exchange is disclosed.
Abstract translation: 本发明涉及在单级工艺通道中进行平衡有限化学反应的方法。 公开了进行水位变换反应的方法。 公开了一种具有横流热交换的多通道反应器。
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19.发明申请Fischer-Tropsch synthesis using microchannel technology and novel catalyst and microchannel reactor 有权使用微通道技术的费 - 托合成和新型催化剂和微通道反应器公开(公告)号：US20060251552A1
公开(公告)日：2006-11-09
申请号：US11484069
申请日：2006-07-11
Applicant: Yong Wang , Anna Tonkovich , Terry Mazanec , Francis Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael Briscoe , Nathan Gano , Ya-Huei Chin
Inventor： Yong Wang , Anna Tonkovich , Terry Mazanec , Francis Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael Briscoe , Nathan Gano , Ya-Huei Chin
CPC classification number: C10G2/332 , B01J19/0093 , B01J21/04 , B01J23/75 , B01J23/8896 , B01J23/8913 , B01J35/0066 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J37/0205 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , C10G2/341 , C10G2300/301 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/04 , C10G2400/10 , Y02P20/582
Abstract: The disclosed invention relates to a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. The disclosed invention also relates to a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
Abstract translation: 所公开的发明涉及将包含H 2 CO和CO的反应物组合物转化成包含至少一种具有至少约5个碳原子的脂族烃的产物的方法，该方法包括：使反应物组合物通过 与费 - 托催化剂接触以将反应物组合物转化成产物的微通道反应器，该微通道反应器包含多个含有该催化剂的工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。 所公开的发明还涉及包含Co的载体催化剂和包含至少一个工艺微通道和至少一个相邻的热交换区的微通道反应器。
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20.发明申请Process and apparatus for improved methods for making vinyl acetate monomer (VAM) 有权制备乙酸乙烯酯单体（VAM）的改进方法的方法和设备公开(公告)号：US20060116528A1
公开(公告)日：2006-06-01
申请号：US11256217
申请日：2005-10-20
Applicant: Terry Mazanec , Victor Johnston , Michael Huckman , Sean Fitzgerald , James Foster , Daniel Lindley , Anna Tonkovich , Francis Daly , Leslie Wade , Tony Hammock , Thomas Yuschak , Bin Yang , Kai Jarosch
Inventor： Terry Mazanec , Victor Johnston , Michael Huckman , Sean Fitzgerald , James Foster , Daniel Lindley , Anna Tonkovich , Francis Daly , Leslie Wade , Tony Hammock , Thomas Yuschak , Bin Yang , Kai Jarosch
IPC: C07C67/05
CPC classification number: B01J19/0093 , B01J2219/00783 , B01J2219/00835 , B01J2219/0086 , B01J2219/00862 , B01J2219/00873 , B01J2219/00889 , C07C67/055 , C07C69/01 , C07C69/15
Abstract: The invention provides methods, apparatus and chemical systems for making vinyl acetate from ethylene, oxygen, and acetic acid.
Abstract translation: 本发明提供从乙烯，氧和乙酸制备乙酸乙烯酯的方法，装置和化学体系。
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