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    High performance environmentally friendly drilling fluids
    2.
    发明授权
    High performance environmentally friendly drilling fluids 失效
    高性能环保钻井液

    公开(公告)号：US6096690A

    公开(公告)日：2000-08-01

    申请号：US83489

    申请日：1998-05-22

    Applicant: Robert Jay Wittenbrink ,  Charles John Mart ,  Daniel Francis Ryan ,  Bruce Randall Cook

    Inventor： Robert Jay Wittenbrink ,  Charles John Mart ,  Daniel Francis Ryan ,  Bruce Randall Cook

    IPC: C09K8/34 ,  C09K8/36 ,  C09K7/00 ,  C07C7/20 ,  C09K7/06

    CPC classification number: C09K8/36 ,  C09K8/34 ,  Y10S507/905

    Abstract: Discloses environmentally friendly, low temperature base oils and drilling fluids, or drilling mud compositions useful in the production of oil and gas. The drilling fluid is constituted of one or more of weighting agents, emulsifiers, wetting agents, viscosifiers, fluid loss control agents, proppants, and other particulates such as used in a gravel pack, emulsified with a paraffinic solvent composition which forms a continuous oil phase, or water-in-oil invert phase. The solvent composition is constituted of a mixture of C.sub.10- C.sub.24 n-paraffins and isoparaffins having an isoparaffin:n-paraffin molar ratio ranging from about 0.5:1 to about 9:1, the isoparaffins of the mixture contain greater than 30 percent, preferably from about 30 percent to about 50 percent, of mono-methyl species, and greater than 30 percent, preferably from about 30 percent to about 50 percent of multi-methyl branched species and isoparaffins which contain one or more branches of carbon number higher than methyl, based on the total weight of the isoparaffins in the mixture. The presence of the mono-methyl species is sufficient to provide the admirable environmentally friendly qualities, and the multi-methyl branched and isoparaffin species more highly branched than methyl provide low temperature properties.

    Abstract translation: 公开了环保的低温基础油和钻井液，或用于生产油和气的钻井泥浆组合物。 钻井液由一种或多种增重剂，乳化剂，润湿剂，增粘剂，流体损失控制剂，支撑剂和其它颗粒组成，例如在用石蜡溶剂组合物乳化的砾石包装中使用的颗粒，其形成连续油相 ，或油包水反相。 溶剂组合物由具有约0.5:1至约9:1的异链烷烃：正链烷烃摩尔比的C10-C24正链烷烃和异链烷烃的混合物构成，混合物的异链烷烃含量大于30％ 约30％至约50％的单甲基物质，以及大于30％，优选约30％至约50％的多甲基支链物质和含有一个或多个碳数高于甲基的支链的异链烷烃 ，基于混合物中异链烷烃的总重量。 单甲基物质的存在足以提供令人敬佩的环境友好的品质，并且比甲基更高支化的多甲基支链和异链烷烃提供低温性能。

    High purity paraffinic solvent compositions
    3.
    发明授权
    High purity paraffinic solvent compositions 失效
    高纯度链烷烃溶剂组合物

    公开(公告)号：US5906727A

    公开(公告)日：1999-05-25

    申请号：US81364

    申请日：1998-05-19

    Applicant: Robert Jay Wittenbrink ,  Steven Earl Silverberg ,  Daniel Francis Ryan

    Inventor： Robert Jay Wittenbrink ,  Steven Earl Silverberg ,  Daniel Francis Ryan

    IPC: C07C9/14 ,  C07C5/13 ,  C10G2/00 ,  C10G35/04 ,  C10G45/58 ,  C10G47/02 ,  C10L1/04

    CPC classification number: C10G45/58

    Abstract: Discloses high purity solvent compositions constituted of n-paraffins and isoparaffins, with the isoparaffins containing predominantly methyl branches, and having an isoparaffin:n-paraffin ratio sufficient to provide superior low temperature properties and low viscosities. The solvent compositions are made by a process wherein a waxy, or long chain paraffinic feed, especially a Fischer-Tropsch wax, is reacted over a dual function catalyst to produce hydroisomerization and hydrocracking reactions at 700.degree. F.+ conversion levels ranging from about 20 to 90 wt.% to provide a C.sub.5 -1050.degree. F. crude fraction. The C.sub.5 -1050.degree. F. crude fraction is then topped via atmospheric distillation to produce a low boiling fraction with an upper end point boiling between about 650.degree. F. and 750.degree. F. The low boiling fraction is fractionated and a narrow boiling range solvent obtained therefrom; one which can be further divided into solvent grades of various boiling ranges.

    Abstract translation: 公开了由正链烷烃和异链烷烃构成的高纯度溶剂组合物，其中主要含有甲基支链的异链烷烃，并且具有足以提供优异的低温性能和低粘度的异链烷烃：正链烷烃比率。 溶剂组合物通过以下方法制备，其中蜡状或长链石蜡原料，特别是费 - 托蜡在双功能催化剂上反应，以在700°F下进行加氢异构化和加氢裂化反应。+转化率范围为约20 至90重量％以提供C5-1050°F粗馏分。 然后通过常压蒸馏将C5-1050°F粗馏分顶起来产生沸点高于约650°F至750°F的高沸点馏分。将低沸点馏分分馏，并将窄沸点溶剂 由此获得; 可以进一步分为各种沸程的溶剂等级。

    Biodegradable high performance hydrocarbon base oils
    5.
    发明授权
    Biodegradable high performance hydrocarbon base oils 失效
    可生物降解的高性能烃基油

    公开(公告)号：US06506297B1

    公开(公告)日：2003-01-14

    申请号：US09547809

    申请日：2000-04-11

    Applicant: Robert Jay Wittenbrink ,  Richard Frank Bauman ,  Daniel Francis Ryan

    Inventor： Robert Jay Wittenbrink ,  Richard Frank Bauman ,  Daniel Francis Ryan

    IPC: C10G7100

    CPC classification number: C10G45/58 ,  C10G67/04 ,  C10G2400/10 ,  C10G2400/12 ,  C10G2400/14 ,  C10M107/02 ,  C10M2205/173 ,  C10N2220/028 ,  C10N2270/00

    Abstract: Discloses novel biodegradable high performance hydrocarbon base oils useful as lubricants in engine oil and industrial compositions, and process for their manufacture. A waxy, or paraffinic feed, particularly a Fischer-Tropsch wax, is reacted over a dual function catalyst to produce hydroisomerization and hydrocracking reactions, at 700° F.+ conversion levels ranging from about 20 to 50 wt. %, preferably about 25-40 wt. %, sufficient to produce a crude fraction, e.g., a C5-1050° F.+ crude fraction, containing 700° F.+ isoparaffins having from about 6.0 to about 7.5 methyl branches per 100 carbon atoms in the molecule. The methyl paraffins containing crude fraction is topped via atmospheric distillation to produce a bottoms fraction having an initial boiling point between about 650° F. and 750° F. which is then solvent dewaxed, and the dewaxed oil is then fractionated under high vacuum to produce biodegradable high performance hydrocarbon base oils.

    Abstract translation: 公开了可用作发动机油和工业组合物中的润滑剂的新型可生物降解的高性能烃基油及其制造方法。 蜡状或石蜡原料，特别是费 - 托蜡在双功能催化剂上反应，产生加氢异构化和加氢裂化反应，在700°F +转化率范围为约20至50wt。 ％，优选约25-40wt。 ％，足以产生含有分子中每100个碳原子具有约6.0至约7.5个甲基支链的含有700°F +的异构烷烃的粗馏分，例如C5-1050°F +粗馏分。 含有粗制部分的甲基链烷烃通过常压蒸馏来顶部，产生沸点在约650°F至750°F之间的塔底馏分，然后进行溶剂脱蜡，然后将脱蜡油在高真空下分馏， 可生物降解的高性能烃基油。

    Hydroisomerization of a predominantly N-paraffin feed to produce high purity solvent compositions
    6.
    发明授权
    Hydroisomerization of a predominantly N-paraffin feed to produce high purity solvent compositions 失效
    主要是N-链烷烃进料的加氢异构化以产生高纯度溶剂组合物

    公开(公告)号：US5866748A

    公开(公告)日：1999-02-02

    申请号：US636424

    申请日：1996-04-23

    Applicant: Robert Jay Wittenbrink ,  Daniel Francis Ryan ,  Steven Earl Silverberg

    Inventor： Robert Jay Wittenbrink ,  Daniel Francis Ryan ,  Steven Earl Silverberg

    IPC: B01J23/44 ,  C10G45/58 ,  C10G45/62

    CPC classification number: C10G45/58 ,  Y10S208/95

    Abstract: A process for the hydroisomerization of a predominantly C.sub.8 -C.sub.20 n-paraffinic feed to produce a high purity C.sub.8 -C.sub.20 paraffinic solvent composition having superior low temperature properties, and low viscosities. The feed is contacted, with hydrogen, over a dual functional catalyst to hydroisomerize and convert the feed to a product comprising a mixture of n-paraffins and isoparaffins, the isoparaffins component of which contains greater than 50 percent of mono-methyl species, with the molar ratio of isoparaffins:n-paraffins ranging from about 0.5:1 to 9:1.

    Abstract translation: 主要C8-C20正链烷烃进料加氢异构化的方法，以产生具有优异的低温性能和低粘度的高纯度C8-C20链烷烃溶剂组合物。 进料与氢气在双官能催化剂上接触，将进料加氢异构化并转化成包含正链烷烃和异链烷烃的混合物的产物，其异链烷烃组分含有大于50％的单甲基物质，其中 异链烷烃的摩尔比：正链烷烃的范围为约0.5:1至9:1。

    Process for softening fischer-tropsch wax with mild hydrotreating
    9.
    发明授权
    Process for softening fischer-tropsch wax with mild hydrotreating 有权
    用轻度加氢处理软化费 - 托蜡的方法

    公开(公告)号：US06776898B1

    公开(公告)日：2004-08-17

    申请号：US09542894

    申请日：2000-04-04

    Applicant: Robert J. Wittenbrink ,  Daniel Francis Ryan

    Inventor： Robert J. Wittenbrink ,  Daniel Francis Ryan

    IPC: C10G4500

    CPC classification number: C10G73/44

    Abstract: A novel process for forming hydrocarbon waxes from synthesis gas is disclosed. This invention teaches a process whereby a Fischer-Tropsch wax can be formulated such that the wax softness as defined by ASTM Standard Test Method for Needle Penetration of waxes (ASTM D-1321) can be adjusted to within a region most preferred for end use applications while simultaneously removing undesirable impurities, such as oxygenates (e.g., primary alcohols), olefins, and trace levels of aromatics. In a Fischer-Tropsch reactor, Fischer-Tropsch wax is formed from synthesis gas in a catalyzed reaction. The Fischer Tropsch wax is then subjected to a relatively mild hydroprocessing over a hydroisomerization catalyst under conditions such that essentially no boiling point conversion is obtained, but yet chemical conversions (e.g., hydrogenation and mild isomerization) occur yielding a high purity, hydrocarbon wax product of reduced hardness.

    Abstract translation: 公开了一种从合成气中形成烃蜡的新方法。 本发明教导了一种方法，其中可以配制费 - 托蜡，使得ASTM标准测试方法针对蜡的渗透（ASTM D-1321）所定义的蜡柔软度可以调整到最适用于最终用途应用的区域内 同时除去不需要的杂质，例如含氧化合物（例如伯醇），烯烃和痕量芳族化合物。 在费 - 托反应器中，费 - 托蜡在催化反应中由合成气形成。 然后在基本上不获得沸点转化率的条件下，在加氢异构化催化剂上进行相对温和的加氢处理，但是仍然发生化学转化（例如氢化和轻度异构化），产生高纯度烃蜡产物 降低硬度。

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