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    Process for preparing filler-dispersed polymeric compositions
    11.
    发明申请
    Process for preparing filler-dispersed polymeric compositions 有权
    制备填料分散聚合物组合物的方法

    公开(公告)号：US20080033098A1

    公开(公告)日：2008-02-07

    申请号：US11890139

    申请日：2007-08-03

    申请人： Christopher Robertson ,  Terrence Hogan ,  William Hergenrother

    发明人： Christopher Robertson ,  Terrence Hogan ,  William Hergenrother

    IPC分类号： C08L101/00

    CPC分类号： C08J3/226

    摘要： A method for preparing a polymeric composition, the method comprising introducing a functionalized polymer and a filler. mixing the functionalized polymer and filler to form a first masterbatch, adding additional polymer to the first masterbatch, and mixing the additional polymer and the first masterbatch.

    摘要翻译： 一种制备聚合物组合物的方法，所述方法包括引入官能化聚合物和填料。 混合官能化的聚合物和填料以形成第一母料，向第一母料中加入另外的聚合物，并混合另外的聚合物和第一母料。

    Use of sulfur containing initiators for anionic polymerization of monomers
    12.
    发明申请
    Use of sulfur containing initiators for anionic polymerization of monomers 有权
    含硫引发剂用于单体阴离子聚合的用途

    公开(公告)号：US20080004386A1

    公开(公告)日：2008-01-03

    申请号：US11900686

    申请日：2007-09-13

    申请人： Terrence Hogan ,  William Hergenrother ,  Yuan-Yong Yan ,  David Lawson

    发明人： Terrence Hogan ,  William Hergenrother ,  Yuan-Yong Yan ,  David Lawson

    IPC分类号： C08F136/14 ,  C08K3/04 ,  C08K3/10 ,  C08K3/36 ,  C08K3/40 ,  C08K5/053 ,  C08K5/09

    CPC分类号： C08C19/44 ,  B60C1/0016 ,  C07F1/02 ,  C08F4/48 ,  C08F36/04 ,  C08K3/013 ,  Y02T10/862 ,  Y10S152/905 ,  C08L15/00

    摘要： An initiator is presented for anionically polymerizing monomers, to provide a functional head group on the polymer. A polymer having a functional head group derived from a sulfur containing anionic initiator, and optionally as additional functional group resulting from the use of a functional terminating reagent, coupling agent or linking agent is also provided. A method is presented for anionically polymerizing monomers comprising the step of polymerizing the monomers with a sulfur containing anionic initiator to provide a functional head group on the polymer. An elastomeric compound, comprising a functional polymer and filler is also described. Also provided is a tire having decreased rolling resistance resulting from a tire component containing a vulcanizable elastomeric compound.

    摘要翻译： 提供用于阴离子聚合单体的引发剂，以在聚合物上提供功能性头基。 还提供了具有衍生自含硫阴离子引发剂的功能性头基团和任选地作为由使用功能性终止试剂，偶联剂或连接剂引起的附加官能团的聚合物。 提出了一种阴离子聚合单体的方法，包括使单体与含硫阴离子引发剂聚合的步骤，以在聚合物上提供功能性头基。 还描述了包含功能聚合物和填料的弹性体化合物。 还提供了由含有可硫化弹性体化合物的轮胎成分导致的滚动阻力降低的轮胎。

    Solution masterbatch process using fine particle silica for low hysteresis rubber
    13.
    发明授权
    Solution masterbatch process using fine particle silica for low hysteresis rubber 有权
    解决方案母粒使用细颗粒二氧化硅用于低滞后橡胶

    公开(公告)号：US07312271B2

    公开(公告)日：2007-12-25

    申请号：US11321418

    申请日：2005-12-29

    申请人： Zhong-Ren Chen ,  Sunji Araki ,  William M. Cole ,  William Hergenrother ,  Sandra Warren

    发明人： Zhong-Ren Chen ,  Sunji Araki ,  William M. Cole ,  William Hergenrother ,  Sandra Warren

    IPC分类号： C08K3/36 ,  C08C2/00

    CPC分类号： C08K3/36 ,  B60C1/00 ,  B60C1/0016 ,  C08J3/226 ,  C08J2409/00 ,  C08K3/013 ,  C08L9/06 ,  C08L19/006 ,  C08L21/00

    摘要： Methods are provided for making a solution masterbatch containing a diene elastomer in an organic solvent and a reinforcing silica filler dispersed therein, comprising the steps of (a) mixing a precipitated silica having an average particle size substantially equivalent to an average particle size of a powdered silica, with a diene elastomer in a first organic solvent; and (b) desolventizing the mixture to form a solution masterbatch preparation. The use of such desolventized solution masterbatches in vulcanizable rubber compounds results in excellent processing characteristics with improved dispersion of fillers, including polymeric nanoparticles. The compounds also demonstrate improved properties, including reduced hysteresis.

    摘要翻译： 提供了制备含有分散在其中的有机溶剂和增强二氧化硅填料中的二烯弹性体的溶液母料的方法，包括以下步骤：（a）将平均粒径基本上等于粉末状的平均粒度的沉淀二氧化硅 二氧化硅，二烯弹性体在第一有机溶剂中; 和（b）将混合物脱溶剂以形成溶液母料制剂。 在可硫化橡胶化合物中使用这种脱溶剂溶液母料导致优异的加工特性，改善了包括聚合物纳米颗粒在内的填料的分散性。 化合物还表现出改进的性能，包括减少滞后。

    Technique for purifying polymer compositions
    15.
    发明申请
    Technique for purifying polymer compositions 有权
    聚合物组合物纯化技术

    公开(公告)号：US20070142593A1

    公开(公告)日：2007-06-21

    申请号：US11304473

    申请日：2005-12-15

    申请人： James Pawlow ,  William Hergenrother

    发明人： James Pawlow ,  William Hergenrother

    IPC分类号： C08F136/00

    CPC分类号： C08C2/04 ,  C08F6/02

    摘要： A method for preparing a polymer product, the method comprising polymerizing conjugated diene monomer, optionally together with vinyl aromatic monomer, within a hydrocarbon solvent by employing a lithium-containing initiator, thereby forming a living polymer cement, where about 0.04 to about 0.2 moles of the alkyl lithium initiator per 100 g of the monomer are employed, where the concentration of the monomer within the solvent is about 1 to about 30% by weight, and where the living polymer cement includes a lithium-containing residue, adding a quenching agent to the living polymer cement in an amount sufficient to quench all of the living polymer within the cement, thereby forming a non-living polymer cement, passing the non-living polymer cement through a purification medium, where the purification medium includes alumina, silica, or both, thereby separating at least part of the lithium-containing residue from the polymer cement, collecting the polymer cement after passing the cement through the purification medium, adding an antioxidant, and desolventizing the polymer cement.

    摘要翻译： 一种制备聚合物产品的方法，该方法包括通过使用含锂引发剂在烃溶剂内将共轭二烯单体（任选地与乙烯基芳族单体一起）聚合，由此形成活性聚合物粘合剂，其中约0.04至约0.2摩尔 使用每100g单体的烷基锂引发剂，其中溶剂中单体的浓度为约1至约30重量％，并且其中活性聚合物水泥包含含锂残渣，并将淬灭剂加入到 所述活性聚合物水泥的量足以使所述水泥中的所有活性聚合物淬火，从而形成非活性聚合物水泥，使所述非活性聚合物水泥通过净化介质，其中所述纯化介质包括氧化铝，二氧化硅或 从而将至少部分含锂残余物从聚合物水泥分离出来，在通过水泥之后收集聚合物水泥 通过净化介质，加入抗氧化剂，并使聚合物胶浆脱水。