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公开(公告)号：US5338884A
公开(公告)日：1994-08-16
申请号：US913124
申请日：1992-10-02
IPC分类号： B01J23/42 , B01J23/44 , B01J23/46 , B01J23/755 , C07B61/00 , C07C213/00 , C07C213/02 , C07C215/28 , C07C215/30 , C07C231/10 , C07C233/18 , C07C235/08 , C07C209/00
CPC分类号： C07C231/10 , C07C213/02 , C07C215/30 , C07C233/18
摘要： Acylamides or amine acylate salts of arylalkanolamines are prepared by reacting an arylisonitrosoalkanone with hydrogen and a carboxylic acid, carboxylic acid anhydride or carboxylic acid ester or mixture thereof in the presence of a transition metal catalyst; optionally the product is converted to the corresponding arylalkanolamine hydrochloride salt by reaction of the acylamide or amine acylate salt of the arylalkanolamine with hydrogen chloride in a C.sub.1 -C.sub.3 alkyl alcohol.
摘要翻译： 芳基烷醇胺的酰胺或胺酰化盐通过芳基亚硝基烷酮与氢和羧酸，羧酸酐或羧酸酯或其混合物在过渡金属催化剂存在下反应来制备; 任选地，通过芳基烷醇胺的酰基酰胺或酰胺化物盐与氯化氢在C1-C3烷基醇中的反应，将产物转化成相应的芳基烷醇胺盐酸盐。
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公开(公告)号：US08013040B2
公开(公告)日：2011-09-06
申请号：US10984370
申请日：2004-11-08
IPC分类号： C08L97/02
CPC分类号： C08K5/20 , Y10T428/31989
摘要： This invention is directed to an extruded product, extrudable compound, and an extrusion method using a polymer, a cellulosic fiber, and at least one lubricant selected from the group consisting of ethoxylated esters of hydantoins, ethoxylated esters of sorbitol or sorbitan, or N, N′-bisalkanoylethylenediamines containing from 8 to 14 carbons of the alkanoyl group and compositions manufactured through such processes which simulate conventional wood products. The N,N′-bisalkanoylethylenediamines are new compositions of matter containing from 8 to 14 carbons of the alkanoyl group having a particle size range from about 90 to 150 μm, preferably from about 120 to 140 μm.
摘要翻译： 本发明涉及挤出产品，可挤出化合物和使用聚合物，纤维素纤维和至少一种选自乙内酰脲的乙氧基化酯，山梨醇或脱水山梨醇的乙氧基化酯或N， 含有8〜14个碳烷基的N'-双链烷酰基亚乙基二胺以及通过模拟常规木制品的方法制造的组合物。 N，N'-二烷酰基亚乙基二胺是含有8至14个碳原子的物质的新组合物，其中烷酰基的粒度范围为约90至150μm，优选约120至140μm。
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13.发明授权Process for the preparation of arylalkylamines and substituted arylalkylamines 失效制备芳基烷基胺和取代的芳基烷基胺的方法
公开(公告)号：US5175368A
公开(公告)日：1992-12-29
申请号：US908587
申请日：1992-06-29
IPC分类号： C07C213/02 , C07C215/52
CPC分类号： C07C213/02 , C07C215/52
摘要： Arylalkylamines (as the hydrochloride salt), e.g. tyramine hydrochloride, are prepared by hydrogenating substituted or unsubstituted aryl-.alpha.-oximinoalkyl ketones, e.g. p-hydroxyisonitroacetophenone, in either in an aqueous reaction medium comprising hydrochloric acid, essentially without the presence of a lower alkyl alcohol in said reaction medium, or in an aqueous reaction medium comprising water, hydrochloric acid, and a lower alkyl alcohol, wherein the alcohol comprises less than about 90% by volume of the reaction medium. A substituent on the aryl portion of the aryl-.alpha.-oximinoalkyl ketone must be on a position which activates the aromatic ring.
摘要翻译： 芳烷基胺（作为盐酸盐），例如 通过氢化取代或未取代的芳基-α-肟基烷基酮来制备盐酸酪胺。 在包含盐酸的水性反应介质中，在所述反应介质中基本上不存在低级烷基醇，或者在包含水，盐酸和低级烷基醇的水性反应介质中，其中所述醇与对羟基硝基苯乙酮 包含小于约90体积％的反应介质。 芳基-α-肟基烷基酮的芳基部分上的取代基必须在活化芳环的位置。
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14.发明申请公开(公告)号：US20120145781A1
公开(公告)日：2012-06-14
申请号：US13323906
申请日：2011-12-13
申请人： Yaron Nemet , Ephraim Brand , Ahmed M. Tafesh
发明人： Yaron Nemet , Ephraim Brand , Ahmed M. Tafesh
CPC分类号： G06K19/0614 , G01D7/00 , G01D7/005 , G06K7/1413 , G06K7/1417 , G06K19/06028 , G06K19/06037 , G06K19/06046 , G06K19/0615 , G06Q10/087 , G06Q30/06
摘要： A quality management system for products including a multiplicity of barcoded quality indicators, a barcode indicator reader and a product type responsive indication interpreter, each of the barcoded quality indicators including a first barcode including at least one first colorable area, the first barcode being machine-readable before exceedance of the at least one time and temperature threshold, at least a second barcode including at least one second colorable area, the second barcode not being machine-readable before exceedance of the at least one time and temperature threshold, a coloring agent located at a first location on the indicator and a coloring agent pathway operative to allow the coloring agent to move, from the first location to the first and second colorable areas simultaneously thereby causing the first barcode to become unreadable and at the same time causing the second barcode to become machine-readable.
摘要翻译： 一种用于产品的质量管理系统，包括多个条形码质量指示器，条形码指示器读取器和产品类型响应指示解释器，每个条形码质量指示器包括包括至少一个第一可着色区域的第一条形码， 在超过所述至少一个时间和温度阈值之前可读的至少第二条形码，至少包括至少一个第二可着色区域的第二条形码，所述第二条形码在超过所述至少一个时间和温度阈值之前不是机器可读的，着色剂位于 在指示器上的第一位置和着色剂通道可操作以允许着色剂从第一位置同时移动到第一和第二可着色区域，从而导致第一条形码变得不可读，并且同时导致第二条形码 变得机器可读。
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公开(公告)号：US07151125B2
公开(公告)日：2006-12-19
申请号：US10424168
申请日：2003-04-18
IPC分类号： C08L97/02
CPC分类号： C08L23/06 , C08L1/00 , C08L97/02 , C08L2205/16 , C08L2666/26 , C08L2666/02 , C08L2666/06
摘要： This invention is directed to an extrudable compound, an extrusion method using a polymer, a cellulosic fiber, and at least one lubricant selected from the group consisting of ethoxylated esters of hydantoins, ethoxylated esters of sorbitol and sorbitan, and ethylene bisamides made from fatty acids containing 6–10 carbons and composites manufactured through such processes which simulate conventional wood products.Another embodiment of the invention is directed to a composition containing polymer, a cellulosic fiber from an agricultural waste product and a lubricant containing a mixture of an alkylene bisamide derived from a C10–C18 is fatty acid and an alkaline earth salt of a fatty acid.
摘要翻译： 本发明涉及可挤出化合物，使用聚合物的挤出方法，纤维素纤维和选自乙内酰脲的乙氧基化酯，山梨糖醇和脱水山梨糖醇的乙氧基化酯和由脂肪酸制备的亚乙基双酰胺的至少一种润滑剂 含有6-10个碳和通过模拟常规木制品的工艺制造的复合材料。 本发明的另一个实施方案涉及含有聚合物的组合物，来自农业废物的纤维素纤维和含有衍生自C 10 -C 18的亚烷基双酰胺的混合物的润滑剂， / SUB>是脂肪酸和脂肪酸的碱土金属盐。
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公开(公告)号：US5430189A
公开(公告)日：1995-07-04
申请号：US185098
申请日：1994-01-19
IPC分类号： C07C209/00 , C07C209/40 , C07C215/52 , C07C249/08 , C07C209/38
CPC分类号： C07C215/52 , C07C209/00 , C07C209/40 , C07C249/08
摘要： An arylisonitrosoalkanone is hydrogenated in the presence of a noble metal catalyst and a weak carboxylic acid to form an arylalkanolamine which is then hydrogenated in the presence of a strong mineral acid and the transition metal catalyst to form an arylalkylamine. When the arylisonitrosoalkanone is an isonitrosoacetophenone, the isonitrosoacetophenone is prepared by one of two methods.In the first method, a substituted or an unsubstituted isonitrosoacetophenone is prepared from a corresponding substituted or unsubstituted acetophenone by oxidizing the acetophenone to form a substituted or an unsubstituted phenylglyoxalacetal in a reactor, hydrolyzing the phenylglyoxal acetal in the same reactor to form a corresponding substituted or unsubstituted phenylglyoxal, and condensing the phenylglyoxal with hydroxylamine or a salt thereof in the same reactor to form the substituted or unsubstituted isonitrosoacetophenone. Alternatively, the substituted or unsubstituted isonitrosoacetophenone is prepared from the corresponding substituted or unsubstituted acetophenone by reacting the substituted or unsubstituted acetophenone in water with a source of a nitrosonium ion in the presence of a strong acid to form a corresponding substituted or unsubstituted phenylglyoxal, and condensing the phenylglyoxal with hydroxylamine or a salt thereof to form the substituted or unsubstituted isonitrosoacetophenone. In either method, any strong acid that might be present in the reaction mass following the condensation to the isonitrosoacetophenone shall be removed therefrom prior to initiating the hydrogenation of the isonitrosoacetophenone to the arylalkanolamine.
摘要翻译： 芳基亚硝基烷酮在贵金属催化剂和弱羧酸的存在下氢化形成芳基烷醇胺，然后在强无机酸和过渡金属催化剂的存在下氢化形成芳基烷基胺。 当芳基亚硝基烷酮是异硝基苯乙酮时，通过两种方法之一制备异硝基苯乙酮。 在第一种方法中，通过在反应器中氧化苯乙酮以形成取代或未取代的苯基乙醛缩醛，由相应的取代或未取代的苯乙酮制备取代或未取代的异硝基苯乙酮，在相同的反应器中水解苯乙醛缩醛形成相应的取代或未取代的苯乙酮缩醛， 未取代的苯基乙二醛，并将苯乙醛酸与羟胺或其盐在同一反应器中缩合形成取代或未取代的异硝基苯乙酮。 或者，取代或未取代的异硝基苯乙酮由相应的取代或未取代的苯乙酮通过在强酸存在下使取代或未取代的苯乙酮在水中与亚硝鎓离子源反应形成相应的取代或未取代的苯基乙二醛，并将 苯基乙二醛与羟胺或其盐形成取代或未取代的异硝基苯乙酮。 在任一种方法中，在将异亚氨基苯乙酮氢化成芳基烷醇胺之前，任何在与异亚硝基苯乙酮缩合后可能存在于反应物质中的强酸应从其中除去。
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公开(公告)号：US5393924A
公开(公告)日：1995-02-28
申请号：US235582
申请日：1994-04-29
IPC分类号： C07C213/02 , C07C215/30 , C07C231/10 , C07C233/18 , C07C231/00
CPC分类号： C07C215/30 , C07C213/02 , C07C231/10 , C07C233/18
摘要： Acylamides or amine acylate salts of arylalkanolamines are prepared by reacting an arylisonitrosoalkanone with hydrogen and a carboxylic acid, carboxylic acid anhydride or carboxylic acid ester or mixture thereof in the presence of a transition metal catalyst; optionally the product is converted to the corresponding arylalkanolamine hydrochloride salt by reaction of the acylamide or amine acylate salt of the arylalkanolamine with hydrogen chloride in a C.sub.1 -C.sub.3 alkyl alcohol.
摘要翻译： 芳基烷醇胺的酰胺或胺酰化盐通过芳基亚硝基烷酮与氢和羧酸，羧酸酐或羧酸酯或其混合物在过渡金属催化剂存在下反应来制备; 任选地，通过芳基烷醇胺的酰基酰胺或酰胺化物盐与氯化氢在C1-C3烷基醇中的反应，将产物转化成相应的芳基烷醇胺盐酸盐。
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公开(公告)号：US5198585A
公开(公告)日：1993-03-30
申请号：US726063
申请日：1991-07-05
IPC分类号： C07C221/00
CPC分类号： C07C221/00
摘要： Acid addition salts of arylketoamines are prepared by reacting arylisonitrosoalkanones with hydrogen in the presence of a transition metal catalyst and strong acid in a dipolar aprotic solvent.
摘要翻译： 芳基酮胺的酸加成盐通过在过渡金属催化剂和强酸在偶极非质子传递溶剂中存在下使芳基亚硝基烷基酮与氢反应来制备。
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公开(公告)号：US07582694B2
公开(公告)日：2009-09-01
申请号：US10526784
申请日：2003-08-29
CPC分类号： C08L23/06 , C08K5/0058 , C08L97/02 , C08L2205/16 , D21H19/36 , C08L2666/26 , C08L2666/02 , C08L2666/06 , C08L2666/04
摘要： The invention relates to a polymer-cellulosic fiber composition comprising a polymer, a cellulosic fiber, and a quaternary ammonium alkyl salt wherein the latter imparts antimicrobial properties to the composition and functions as a lubricant during the formation of the composition. The quaternary ammonium alkyl salts may be alkyl carboxylate, alkyl sulfate, alkyl sulphonate, alkyl phosphate, or alkyl phosphite. Certain of the salts are new compositions of matter. The method of extruding and the extrudate are also claimed.
摘要翻译： 本发明涉及一种聚合物 - 纤维素纤维组合物，其包含聚合物，纤维素纤维和季铵烷基盐，其中后者赋予组合物抗微生物性能并且在组合物形成期间用作润滑剂。 季铵烷基盐可以是烷基羧酸盐，烷基硫酸盐，烷基磺酸盐，烷基磷酸盐或亚磷酸烷基酯。 某些盐是物质的新组合物。 还要求权利要求的挤出方法和挤出物。
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公开(公告)号：US5319142A
公开(公告)日：1994-06-07
申请号：US957335
申请日：1992-10-06
IPC分类号： C07C209/00 , C07C209/40 , C07C215/52 , C07C249/08 , C07C209/38
CPC分类号： C07C215/52 , C07C209/00 , C07C209/40 , C07C249/08
摘要： An arylisonitrosoalkanone is hydrogenated in the presence of a noble metal catalyst and a weak carboxylic acid to form an arylalkanolamine which is then hydrogenated in the presence of a strong mineral acid and the transition metal catalyst to form an arylalkylamine. When the arylisonitrosoalkanone is an isonitrosoacetophenone, the isonitrosoacetophenone is prepared by one of two methods.In the first method, a substituted or an unsubstituted isonitrosoacetophenone is prepared from a corresponding substituted or unsubstituted acetophenone by oxidizing the acetophenone to form a substituted or an unsubstituted phenylglyoxalacetal in a reactor, hydrolyzing the phenylglyoxal acetal in the same reactor to form a corresponding substituted or unsubstituted phenylglyoxal, and condensing the phenylglyoxal with hydroxylamine or a salt thereof in the same reactor to form the substituted or unsubstituted isonitrosoacetophenone. Alternatively, the substituted or unsubstituted isonitrosoacetophenone is prepared from the corresponding substituted or unsubstituted acetophenone by reacting the substituted or unsubstituted acetophenone in water with a source of a nitrosonium ion in the presence of a strong acid to form a corresponding substituted or unsubstituted phenylglyoxal, and condensing the phenylglyoxal with hydroxylamine or a salt thereof to form the substituted or unsubstituted isonitrosoacetophenone. In either method, any strong acid that might be present in the reaction mass following the condensation to the isonitrosoacetophenone shall be removed therefrom prior to initiating the hydrogenation of the isonitrosoacetophenone to the arylalkanolamine.
摘要翻译： 芳基亚硝基烷酮在贵金属催化剂和弱羧酸的存在下氢化形成芳基烷醇胺，然后在强无机酸和过渡金属催化剂的存在下氢化形成芳基烷基胺。 当芳基亚硝基烷酮是异硝基苯乙酮时，通过两种方法之一制备异硝基苯乙酮。 在第一种方法中，通过在反应器中氧化苯乙酮以形成取代或未取代的苯基乙醛缩醛，由相应的取代或未取代的苯乙酮制备取代或未取代的异硝基苯乙酮，在相同的反应器中水解苯乙醛缩醛形成相应的取代或未取代的苯乙酮缩醛， 未取代的苯基乙二醛，并将苯乙醛酸与羟胺或其盐在同一反应器中缩合形成取代或未取代的异硝基苯乙酮。 或者，取代或未取代的异硝基苯乙酮由相应的取代或未取代的苯乙酮通过在强酸存在下使取代或未取代的苯乙酮在水中与亚硝鎓离子源反应形成相应的取代或未取代的苯基乙二醛，并将 苯基乙二醛与羟胺或其盐形成取代或未取代的异硝基苯乙酮。 在任一种方法中，在将异亚氨基苯乙酮氢化成芳基烷醇胺之前，任何在与异亚硝基苯乙酮缩合后可能存在于反应物质中的强酸应从其中除去。
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