Organometallic compound vaporizing/feeding system
    11.
    发明授权
    Organometallic compound vaporizing/feeding system 失效
    有机金属化合物蒸发/送料系统

    公开(公告)号:US06987565B2

    公开(公告)日:2006-01-17

    申请号:US10666258

    申请日:2003-09-22

    IPC分类号: G01N21/73

    CPC分类号: G01N21/714

    摘要: An organometallic compound vaporizing and feeding system includes a carrier gas feed passageway connecting a carrier gas source to a container containing an organometallic compound MO and having a carrier gas mass flow controller, an MO gas passageway connecting the container to an in-line monitor for transporting the MO gas, a sample gas passageway connecting the in-line monitor to a sample inlet of an ICP spectrometer, a standard gas passageway connecting a gas cylinder filled with a calibration standard gas to the sample gas passageway and having a standard gas mass flow controller, and a diluent gas passageway connected to the standard gas passageway for passing a diluent gas for adjusting the concentration of the standard gas and having a diluent gas mass flow controller.

    摘要翻译: 有机金属化合物蒸发和进料系统包括将载气源连接到容纳有机金属化合物MO并且具有载气质量流量控制器的容器的载气进料通道,将该容器连接到在线监测器的MO气体通道,用于运输 MO气体,将在线监测器连接到ICP光谱仪的样品入口的样品气体通道,将填充有校准标准气体的气瓶连接到样品气体通道的标准气体通道,并具有标准气体质量流量控制器 以及连接到标准气体通道的稀释气体通道,用于通过稀释气体以调节标准气体的浓度并具有稀释气体质量流量控制器。

    Cross-linked polymer solid electrolyte, method of manufacturing
cross-linked solid polymer electrolyte, composite solid electrolyte,
and thin solid cell employing composite solid electrolyte
    13.
    发明授权
    Cross-linked polymer solid electrolyte, method of manufacturing cross-linked solid polymer electrolyte, composite solid electrolyte, and thin solid cell employing composite solid electrolyte 失效
    交联聚合物固体电解质,交联固体高分子电解质的制造方法,复合固体电解质和采用复合固体电解质的薄型固体电池

    公开(公告)号:US6096234A

    公开(公告)日:2000-08-01

    申请号:US9066

    申请日:1998-01-20

    摘要: There is disclosed a cross-linked polymer solid electrolyte and a method of manufacturing the same. A crosslinking agent is added to a block-graft copolymer composed of a polymer block chain A represented by formula I and a polymer block chain B represented by formula II; a high energy ray is irradiated to the block-graft polymer in order to crosslink the entire system; and an nonaqueous electrolytic solution is added to the block-graft polymer. There is also disclosed a composite solid electrolyte for use in a solid electrochemical element. The composite solid electrolyte includes an electrically insulating material, an alkali metal salt, a block-graft copolymer composed of a polymer block chain A represented by formula I and a polymer block chain B represented by formula II, and an aprotic organic solvent. ##STR1##

    摘要翻译: 公开了一种交联聚合物固体电解质及其制造方法。 将交联剂加入到由式I表示的聚合物嵌段链A和由式II表示的聚合物嵌段链B组成的嵌段共聚物中; 为了交联整个体系,将高能射线照射到嵌段接枝聚合物上; 并向嵌段聚合物中加入非水电解液。 还公开了一种用于固体电化学元件的复合固体电解质。 复合固体电解质包括电绝缘材料,碱金属盐,由式I表示的聚合物嵌段链A和由式II表示的聚合物嵌段链B组成的嵌段共聚物和非质子性有机溶剂。

    Preparation of crosslinked solid polymer electrolyte
    16.
    发明授权
    Preparation of crosslinked solid polymer electrolyte 失效
    交联固体高分子电解质的制备

    公开(公告)号:US06322924B1

    公开(公告)日:2001-11-27

    申请号:US09493278

    申请日:2000-01-28

    IPC分类号: H01M618

    摘要: A crosslinked solid polymer electrolyte is prepared by adding a reactive polyalkylene oxide and an inorganic lithium salt to a block-graft copolymer comprising first and second block chains, and subjecting the reactive polyalkylene oxide to crosslinking reaction. The crosslinked solid polymer electrolyte has a high ionic conductivity and can be readily formed into a tough film and is thus suited for use in large-size secondary batteries.

    摘要翻译: 通过将反应性聚环氧烷和无机锂盐加入到包含第一和第二嵌段链的嵌段共聚物共聚物中并使反应性聚环氧烷进行交联反应来制备交联固体聚合物电解质。 交联固体高分子电解质具有高的离子电导率,并且可以容易地形成韧性膜,因此适用于大尺寸二次电池。

    Method for vaporizing and supplying organometal compounds
    17.
    发明授权
    Method for vaporizing and supplying organometal compounds 失效
    蒸发和供应有机金属化合物的方法

    公开(公告)号:US5377616A

    公开(公告)日:1995-01-03

    申请号:US150532

    申请日:1993-11-09

    摘要: A method for vaporizing an organometal compound and supplying the resulting vapor thereof to a crystal growth chamber which comprises the steps of heating an organometal compound to a predetermined temperature to obtain vapor of the compound at a predetermined vapor pressure and supplying, in a constant flow rate, the vapor to the surface of a substrate heated under a reduced pressure: an apparatus for vaporizing an organometal compound and supplying the resulting vapor thereof to a crystal growth chamber 11 comprising a first gas flow path for the vapor of the organometal compound which connects a container 20, in which the organometal compound is charged, to a crystal growth chamber heated under a reduced pressure through a first valve 21, a first massflow controller 22 and a second valve 23 in this order; and a constant temperature oven 24 and 25 for controlling the temperature of the container 20 and the first gas flow path extending from the container 20 to the second valve 23, are herein disclosed. The method and the apparatus makes it possible to form a thin film on substrate having even a large surface area and uniform composition and thickness with good reproducibility and to provide an epitaxial thin film of a compound semiconductor having good sharpness of the crystal growing boundary; the method further makes it possible to prevent the contamination of the solid organometal compound and to provide good workability.

    摘要翻译: 一种用于蒸发有机金属化合物并将其产生的蒸气供应到晶体生长室的方法,该方法包括以下步骤:将有机金属化合物加热至预定温度以获得化合物的蒸气,并以预定的蒸汽压进行,并以恒定的流量 蒸气到减压下加热的基底表面:用于蒸发有机金属化合物并将其产生的蒸气供应到晶体生长室11的装置,该结晶生长室11包括有机金属化合物蒸汽的第一气体流路, 通过第一阀21,第一质量流量控制器22和第二阀23依次向经过减压加热的晶体生长室中装入有机金属化合物的容器20; 以及用于控制容器20的温度和从容器20延伸到第二阀23的第一气体流路的恒温箱24和25。 该方法和装置使得可以在具有大的表面积和均匀的组成和厚度的基板上形成薄膜,具有良好的再现性,并且提供具有良好的晶体生长边界锐度的化合物半导体的外延薄膜; 该方法还可以防止固体有机金属化合物的污染并提供良好的可加工性。