PREPARATION DEVICE AND METHOD FOR SEMI-INSULATING INDIUM PHOSPHIDE

    公开(公告)号:US20240209546A1

    公开(公告)日:2024-06-27

    申请号:US18293137

    申请日:2021-12-08

    IPC分类号: C30B33/02 C30B29/40

    CPC分类号: C30B33/02 C30B29/40

    摘要: A preparation device and method of semi-insulated indium phosphide belong to the field of crystal preparation. The preparation device includes a furnace body, and a crucible, an injector and an in-situ annealing device within the furnace body. The method includes: A, heating indium to form an indium melt; B, filling the furnace body with hydrogen of 0.02-0.3 MPa and holding the pressure for 1-5 hours, and covering the surface of the melt with liquid boron oxide; C, filling the furnace body with an inert gas of 6-15 MPa; D, injecting a phosphorus gas into the indium melt by the injector; E, growing a crystal; and F, annealing the crystal within the in-situ annealing device. Using the present invention can complete the growth of the crystal and implement the in-situ annealing of the crystal in a suitable space, and especially when annealing under a phosphorus atmosphere is required, it ensures that the phosphorus gas does not condense to maintain the pressure in the annealing space and establish a good annealing environment, and the quality of the semi-insulated indium phosphide crystal is ensured.