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11.发明授权Carbonic acid diester, aromatic polycarbonate and facilities, and preparation thereof 有权碳酸二酯，芳族聚碳酸酯和设备及其制备公开(公告)号：US06323302B1
公开(公告)日：2001-11-27
申请号：US09445824
申请日：1999-12-14
申请人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
发明人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： Aromatic polycarbonate having a reduced discoloration and improved heat stability, hue, etc. is provided by keeping a pressure in a raw material melting vessel and the linear velocity of a gas in a transporting piping in a specific range, keeping the concentration of a nitrogen-containing basic compound in a specific range, recycling a byproduct containing specific amounts of impurities, suppressing the amounts of a nitrogen-containing basic compound, metallic elements and a silicic acid derivative in the carbonic acid diester at specific values or less, prescribing the material quality of the reaction facilities, and/or forming an oxide layer at the inner wall surfaces of the reaction facilities.
摘要翻译： 通过将原料熔融容器中的压力和输送管道中的气体的线速度保持在特定范围来提供具有减少变色和改善的热稳定性，色相等的芳族聚碳酸酯，保持氮气浓度， 含有特定范围的碱性化合物，回收含有特定量的杂质的副产物，抑制碳酸二酯中的含氮碱性化合物，金属元素和硅酸衍生物的量在特定值以下，规定材料质量 的反应设备，和/或在反应设备的内壁表面形成氧化物层。
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12.发明授权Polycarbonate resin composition optical recording medium, and substrate therefor 有权聚碳酸酯树脂组合物光记录介质及其基材公开(公告)号：US06407199B1
公开(公告)日：2002-06-18
申请号：US09744559
申请日：2001-01-26
申请人： Masumi Hirata , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Jyuhou Matsuo
发明人： Masumi Hirata , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Jyuhou Matsuo
IPC分类号： C08G6400
CPC分类号： C08L69/00 , C08K5/0008 , C08K5/06 , C08K5/101 , C08K5/103 , C08K5/13 , C08K5/156 , C08K5/1565 , C08K5/17 , C08K5/42 , C08K5/50 , C08K5/526 , C08K5/53 , G11B7/2534 , C08L2666/16
摘要： A polycarbonate resin composition which is excellent in thermal stability such as color retention at the time of melt molding, for example, the prevention of yellowing, and moldability such as releasability and transferability and therefore particularly suitable for the production of precision optical moldings such as optical disk substrates and lenses. The polycarbonate resin composition comprises (A) an aromatic polycarbonate, and (B) a cyclic carbonate compound, a monoester compound of a divalent aliphatic alcohol having 3 to 14 carbon.atoms and an aliphatic monocarboxylic acid having 12 to 24 carbon atoms, or an ether compound obtained by converting at least one hydroxyl group of a polyvalent aliphatic alcohol having 3 to 14 carbon atoms into an aliphatic oxy group having 1 to 18 carbon atoms, or (C) a partial ester compound of an aliphatic alcohol having a valence of 2 to 6 and 2 to 14 carbon atoms and an aliphatic monocarboxylic acid having 12 to 24 carbon atoms, a cyclic phenol compound or a compound selected from hydrochloric acid, phosphoric acid, phosphorous acid, boric acid, and amine salts and ammonium salts thereof.
摘要翻译： 熔融成型时的热稳定性优异的聚碳酸酯树脂组合物，例如防止黄变，以及脱模性和转印性等成型性，因此特别适用于制造精密光学模制品如光学 磁盘基板和透镜。 聚碳酸酯树脂组合物包含（A）芳族聚碳酸酯和（B）环状碳酸酯化合物，具有3〜14个碳原子的二价脂肪族醇的单酯化合物和碳原子数12〜24的脂肪族一元羧酸，或 通过将具有3〜14个碳原子的多元脂肪醇的至少一个羟基转化为碳原子数1〜18的脂肪族氧基而得到的醚化合物，或（C）2价的脂肪族醇的偏酯化合物 碳原子数为6〜2〜14的脂肪族单羧酸，环状酚化合物或选自盐酸，磷酸，亚磷酸，硼酸及其胺盐及铵盐的化合物。
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13.发明授权公开(公告)号：US07767302B2
公开(公告)日：2010-08-03
申请号：US12622999
申请日：2009-11-20
申请人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
发明人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
IPC分类号： B32B9/00
CPC分类号： D01F9/145 , C08J5/04 , C08K7/06 , D04H1/42 , H01L23/373 , H01L2924/0002 , H05K3/4641 , Y10T428/249928 , Y10T428/24994 , Y10T428/249945 , Y10T428/249957 , Y10T428/25 , Y10T428/2918 , Y10T428/30 , H01L2924/00
摘要： To provide a carbon fiber reinforcement having excellent thermal conductivity and mechanical properties which is manufactured by mixing together two different types of pitch-based carbon short fibers having a ratio of the degree of filament diameter distribution to average fiber diameter of 0.05 to 0.2 and a fiber length of 20 to 6,000 μm which differ from each other in average fiber diameter or by mixing one of them with a pitch-based carbon fiber web to improve dispersibility into a matrix resin or increase the dispersion ratio of the pitch-based carbon short fibers.
摘要翻译： 为了提供具有优异的导热性和机械性能的碳纤维增强材料，其通过将两种不同类型的具有直径分布度与平均纤维直径的比率为0.05至0.2的沥青类碳短纤维和纤维 长度为20〜6000μm，其平均纤维直径彼此不同，或者通过将它们中的一种与沥青类碳纤维网混合，以改善对基体树脂的分散性或增加沥青类碳短纤维的分散比。
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14.发明申请CARBON FIBER COMPOSITE SHEET, USE THEREOF AS A HEAT CONDUCTOR AND PITCH-BASED CARBON FIBER WEB SHEET FOR USE IN THE SAME 审中-公开碳纤维复合片，用作热导体和基于沥青的碳纤维网片，用于其中公开(公告)号：US20090061193A1
公开(公告)日：2009-03-05
申请号：US11912086
申请日：2006-04-14
申请人： Hiroshi Hara , Masumi Hirata , Tetsuo Ban
发明人： Hiroshi Hara , Masumi Hirata , Tetsuo Ban
CPC分类号： D21H13/50 , C08J5/042 , D01F9/145 , D04H3/007 , D04H3/16 , H01L23/367 , H01L23/373 , H01L2924/0002 , H05K3/4641 , Y10T428/24994 , Y10T428/25 , H01L2924/00
摘要： A carbon fiber composite sheet comprising a pitch-based carbon fiber web and a matrix resin, wherein carbon fibers constituting the pitch-based carbon fiber web have a crystallite size in the hexagonal net plane direction of 5 nm or more and a thermal conductivity in the thickness direction of 1 W/(m·K) or more. This carbon fiber composite sheet is used for radio shielding and heat conduction.
摘要翻译： 1.一种碳纤维复合片，其包含沥青类碳纤维网和基质树脂，其中构成沥青类碳纤维网的碳纤维的六方网面方向的微晶尺寸为5nm以上，导热率 厚度方向为1W /（mK）以上。 该碳纤维复合片用于无线电屏蔽和热传导。
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15.发明申请公开(公告)号：US20090075054A1
公开(公告)日：2009-03-19
申请号：US11911912
申请日：2006-04-13
申请人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
发明人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
CPC分类号： D01F9/145 , C08J5/04 , C08K7/06 , D04H1/42 , H01L23/373 , H01L2924/0002 , H05K3/4641 , Y10T428/249928 , Y10T428/24994 , Y10T428/249945 , Y10T428/249957 , Y10T428/25 , Y10T428/2918 , Y10T428/30 , H01L2924/00
摘要： To provide a carbon fiber reinforcement having excellent thermal conductivity and mechanical properties which is manufactured by mixing together two different types of pitch-based carbon short fibers having a ratio of the degree of filament diameter distribution to average fiber diameter of 0.05 to 0.2 and a fiber length of 20 to 6,000 μm which differ from each other in average fiber diameter or by mixing one of them with a pitch-based carbon fiber web to improve dispersibility into a matrix resin or increase the dispersion ratio of the pitch-based carbon short fibers.
摘要翻译： 为了提供具有优异的导热性和机械性能的碳纤维增强材料，其通过将两种不同类型的具有直径分布度与平均纤维直径的比率为0.05至0.2的沥青类碳短纤维和纤维 长度为20〜6000μm，其平均纤维直径彼此不同，或者将它们中的一个与沥青类碳纤维网混合，以改善对基体树脂的分散性或增加沥青类碳短纤维的分散比。
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16.发明授权公开(公告)号：US07651767B2
公开(公告)日：2010-01-26
申请号：US11911912
申请日：2006-04-13
申请人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
发明人： Masumi Hirata , Hiroshi Hara , Tetsuo Ban
IPC分类号： B32B9/00
CPC分类号： D01F9/145 , C08J5/04 , C08K7/06 , D04H1/42 , H01L23/373 , H01L2924/0002 , H05K3/4641 , Y10T428/249928 , Y10T428/24994 , Y10T428/249945 , Y10T428/249957 , Y10T428/25 , Y10T428/2918 , Y10T428/30 , H01L2924/00
摘要： To provide a carbon fiber reinforcement having excellent thermal conductivity and mechanical properties which is manufactured by mixing together two different types of pitch-based carbon short fibers having a ratio of the degree of filament diameter distribution to average fiber diameter of 0.05 to 0.2 and a fiber length of 20 to 6,000 μm which differ from each other in average fiber diameter or by mixing one of them with a pitch-based carbon fiber web to improve dispersibility into a matrix resin or increase the dispersion ratio of the pitch-based carbon short fibers.
摘要翻译： 为了提供具有优异的导热性和机械性能的碳纤维增强材料，其通过将两种不同类型的具有直径分布度与平均纤维直径的比率为0.05至0.2的沥青类碳短纤维和纤维 长度为20〜6000μm，其平均纤维直径彼此不同，或者将它们中的一个与沥青类碳纤维网混合，以改善对基体树脂的分散性或增加沥青类碳短纤维的分散比。
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公开(公告)号：US20090233092A1
公开(公告)日：2009-09-17
申请号：US12298745
申请日：2007-04-26
申请人： Hiroshi Hara , Masumi Hirata , Hiroki Sano , Shoichi Takagi
发明人： Hiroshi Hara , Masumi Hirata , Hiroki Sano , Shoichi Takagi
CPC分类号： C08J5/24 , C08J5/042 , C08J2363/00 , C08J2383/04 , Y10T428/249921 , Y10T428/249928 , Y10T428/24994 , Y10T428/269 , Y10T428/2918
摘要： A carbon fiber composite sheet obtained by combining a carbon fiber aggregate with a thermosetting resin component selected from the group consisting of thermosetting silicone-based gel components, thermosetting epoxy resin components and thermosetting silicone resin components, and then curing the thermosetting resin component, the carbon fiber composite sheet having crystallite sizes of at least 5 nm in the direction of growth of the hexagonal mesh surface of the carbon fibers composing the carbon fiber aggregate, and the carbon fiber composite sheet having a thermal conductivity of at least 2 W/(m·K).
摘要翻译： 一种碳纤维复合片材，其通过将碳纤维聚集体与选自热固性硅酮基凝胶组分，热固性环氧树脂组分和热固性有机硅树脂组分的热固性树脂组分组合，然后固化热固性树脂组分，碳 在构成碳纤维集合体的碳纤维的六边形网眼表面的生长方向上具有至少5nm的微晶尺寸的纤维复合片材和导热率至少为2W /（m·K）的碳纤维复合片材， 。
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公开(公告)号：US5516878A
公开(公告)日：1996-05-14
申请号：US386086
申请日：1995-02-09
CPC分类号： C08G64/307
摘要： A process for the production of an aromatic polycarbonate, which comprises polycondensing an aromatic dihydroxy compound and a diaryl carbonate in the presence, as a polycondensation catalyst, of at least one alkali metal salt selected from the group consisting of alkali metal salts of ate-complexes of a metal element, which is silicon, germanium, stannum or plumbum, and alkali metal salts of oxoacids of said metal elements. The above aromatic polycarbonate is almost free from being colored, is also almost free from a decrease in polymerization degree when molded, and is further almost free from forming branches and insolubles.
摘要翻译： 一种制备芳族聚碳酸酯的方法，该方法包括在作为缩聚催化剂存在下将芳族二羟基化合物和碳酸二芳基酯缩聚至少一种碱金属盐，所述碱金属盐选自由以下组成的组：碱金属盐 金属元素，其是硅，锗，锡或铅，以及所述金属元素的含氧酸的碱金属盐。 上述芳香族聚碳酸酯几乎没有着色，在成型时也几乎没有聚合度的降低，而且几乎不会形成分支和不溶物。
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公开(公告)号：US5494952A
公开(公告)日：1996-02-27
申请号：US437987
申请日：1995-05-10
申请人： Masumi Hirata , Wataru Funakoshi , Katsushi Sasaki
发明人： Masumi Hirata , Wataru Funakoshi , Katsushi Sasaki
CPC分类号： C08K5/42 , C08G64/307 , C08K5/41 , C08K5/50 , Y10S524/911 , Y10S524/912 , Y10S524/913
摘要： A process for the production of a stabilized polycarbonate which comprises melt-polycondensing an aromatic dihydroxy compound and a carbonic acid diester in the presence of a polycondensation catalyst and then, after the reaction mixture shows an intrinsic viscosity of at least 0.1, adding at least one stabilizer selected from the group consisting of specific compounds having a sulfanate group and a sulfonic acid anhydride group in an amount of 0.01 to 500 ppm of a polycarbonate to be formed, to form a polycarbonate having a desired intrinsic viscosity.
摘要翻译： 一种制备稳定化聚碳酸酯的方法，其包括在缩聚催化剂存在下使芳族二羟基化合物和碳酸二酯熔融缩聚，然后在反应混合物的特性粘度至少为0.1之后，加入至少一种 选自具有硫酸盐基和磺酸酐基团的具体化合物的稳定剂的量为0.01至500ppm的待形成的聚碳酸酯，以形成具有所需特性粘度的聚碳酸酯。
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公开(公告)号：US07947362B2
公开(公告)日：2011-05-24
申请号：US12298745
申请日：2007-04-26
申请人： Hiroshi Hara , Masumi Hirata , Hiroki Sano , Shoichi Takagi
发明人： Hiroshi Hara , Masumi Hirata , Hiroki Sano , Shoichi Takagi
IPC分类号： A01K1/015
CPC分类号： C08J5/24 , C08J5/042 , C08J2363/00 , C08J2383/04 , Y10T428/249921 , Y10T428/249928 , Y10T428/24994 , Y10T428/269 , Y10T428/2918
摘要： A carbon fiber composite sheet obtained by combining a carbon fiber aggregate with a thermosetting resin component selected from the group consisting of thermosetting silicone-based gel components, thermosetting epoxy resin components and thermosetting silicone resin components, and then curing the thermosetting resin component, the carbon fiber composite sheet having crystallite sizes of at least 5 nm in the direction of growth of the hexagonal mesh surface of the carbon fibers composing the carbon fiber aggregate, and the carbon fiber composite sheet having a thermal conductivity of at least 2 W/(m·K).
摘要翻译： 一种碳纤维复合片材，其通过将碳纤维聚集体与选自热固性硅酮基凝胶组分，热固性环氧树脂组分和热固性有机硅树脂组分的热固性树脂组分组合，然后固化热固性树脂组分，碳 在构成碳纤维集合体的碳纤维的六方网格面的生长方向上具有至少5nm的微晶尺寸的纤维复合片材和导热率为2W /（m·s）以上的碳纤维复合片材 K）。
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