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公开(公告)号：US07780822B2
公开(公告)日：2010-08-24
申请号：US11795122
申请日：2006-01-25
Applicant: Roland Beckmann , Karl Heinz Dulle , Frank Funck , Randolf Kiefer , Peter Woltering
Inventor： Roland Beckmann , Karl Heinz Dulle , Frank Funck , Randolf Kiefer , Peter Woltering
Abstract: An electrolytic cell consisting of two semi-shells and encompassing mainly the inlet and outlet devices, components for the flow control, a membrane as well as anode and cathode.
Abstract translation: 由两个半壳组成的电解槽，主要包括入口和出口装置，用于流量控制的部件，膜以及阳极和阴极。
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公开(公告)号：US20080116081A1
公开(公告)日：2008-05-22
申请号：US11795474
申请日：2006-02-10
Applicant: Karl Heinz Dulle , Roland Beckmann , Randolf Kiefer , Peter Woltering
Inventor： Karl Heinz Dulle , Roland Beckmann , Randolf Kiefer , Peter Woltering
Abstract: An electrode for electrochemical processes for gas production, which in the installed state is located parallel and opposite to an ion exchange membrane and consists of a multitude of horizontal lamellar elements which are structured and three-dimensionally shaped and are in contact with only one surface with the membrane, wherein the lamellar elements have grooves and holes, the major part of the holes being placed in the grooves and the surfaces of such holes or part thereof are located in the grooves or extend into the grooves whereby the holes are ideally placed in the contact area of the respective lamellar element with the membrane.
Abstract translation: 一种用于气体生产的电化学方法的电极，其在安装状态下与离子交换膜平行和相对设置，并且由多个水平层状元件组成，其被构造和三维成形并且仅与一个表面接触 膜，其中层状元件具有凹槽和孔，孔的主要部分被放置在凹槽中，并且这些孔或其一部分的表面位于凹槽中或延伸到凹槽中，从而孔理想地放置在凹槽中 相应层状元件与膜的接触面积。
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公开(公告)号：US10030300B2
公开(公告)日：2018-07-24
申请号：US13702387
申请日：2011-05-23
Applicant: Karl-Heinz Dulle , Frank Funck , Dirk Hoormann , Stefan Oelmann , Peter Woltering , Carsten Schmitt , Philipp Hofmann , Ulf-Steffen Baeumer
Inventor： Karl-Heinz Dulle , Frank Funck , Dirk Hoormann , Stefan Oelmann , Peter Woltering , Carsten Schmitt , Philipp Hofmann , Ulf-Steffen Baeumer
IPC: C23C14/00 , C23C14/32 , C23C14/22 , B01J21/06 , B01J23/46 , B01J37/14 , B01J37/34 , C23C14/02 , C23C14/08 , C23C14/16 , C25B11/04
CPC classification number: C23C14/22 , B01J21/063 , B01J23/462 , B01J23/468 , B01J37/14 , B01J37/341 , B01J37/347 , C23C14/0021 , C23C14/024 , C23C14/08 , C23C14/083 , C23C14/16 , C23C14/325 , C25B11/0478
Abstract: A method for coating a substrate on one or more sides having catalytically active material producible by material deposition under vacuum in a vacuum chamber, using the following steps: loading a substrate in the chamber evacuating the chamber, cleaning the substrate by introducing a gaseous reducing agent, removing the gaseous reducing agent, applying an intermediate layer by means of vacuum arc evaporation, wherein a substrate comprising the same or similar material is introduced into the vacuum chamber, controlling the chamber temperature, coating by vacuum arc evaporation, a metal taken from the group ruthenium, iridium, titanium and mixtures thereof while oxygen is supplied, in a last step the coated substrate is removed from the chamber, wherein at least 99% of the substrate coating is free of constituents originally contained in the substrate itself, and at least 99% of the coating applied on the intermediate layer is kept free of non-oxidized metals.
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公开(公告)号：US09045837B2
公开(公告)日：2015-06-02
申请号：US13994042
申请日：2011-11-15
Applicant: Peter Woltering , Randolf Kiefer , Rainer Weber , Andreas Bulan
Inventor： Peter Woltering , Randolf Kiefer , Rainer Weber , Andreas Bulan
Abstract: Electrolyzer comprising at least one single electrolyzer element which comprises at least one anode compartment with an anode, one cathode compartment with a cathode and one ion exchange membrane arranged between the anode and the cathode compartments, with the anode and/or cathode being a gas diffusion electrode. A gap is provided between the gas diffusion electrode and the ion exchange membrane, with an electrolyte inlet arranged at the upper end of the gap and an electrolyte outlet at the lower end of the gap and a gas inlet and a gas outlet. The electrolyte outlet extending into a discharge header, and the electrolyte inlet connected to an electrolyte feed tank and having an overflow, the overflow connected to the discharge header, with a coiled hose connecting the electrolyte feed tank with the electrolyte inlet and with a coiled hose connecting the overflow with the discharge header.
Abstract translation: 电解器包括至少一个单个电解器元件，其包括具有阳极的至少一个阳极室，具有阴极的一个阴极室和布置在阳极和阴极室之间的一个离子交换膜，阳极和/或阴极是气体扩散 电极。 在气体扩散电极和离子交换膜之间设置有间隙，电解液入口布置在间隙的上端，并且间隙的下端具有电解液出口，气体入口和气体出口。 电解液出口延伸到排放集管中，电解质入口连接到电解质进料罐并具有溢流，溢流口连接到排出集管，连接软管将电解质进料罐与电解液入口连接，并且连接软管 将溢流与排放管连接。
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公开(公告)号：US07785453B2
公开(公告)日：2010-08-31
申请号：US11795474
申请日：2006-02-10
Applicant: Karl Heinz Dulle , Roland Beckmann , Randolf Kiefer , Peter Woltering
Inventor： Karl Heinz Dulle , Roland Beckmann , Randolf Kiefer , Peter Woltering
Abstract: An electrode for electrochemical processes for gas production, which in the installed state is located parallel and opposite to an ion exchange membrane and consists of a multitude of horizontal lamellar elements which are structured and three-dimensionally shaped and are in contact with only one surface with the membrane, wherein the lamellar elements have grooves and holes, the major part of the holes being placed in the grooves and the surfaces of such holes or part thereof are located in the grooves or extend into the grooves whereby the holes are ideally placed in the contact area of the respective lamellar element with the membrane.
Abstract translation: 一种用于气体生产的电化学方法的电极，其在安装状态下与离子交换膜平行和相对设置，并且由多个水平层状元件组成，其被构造和三维成形并且仅与一个表面接触 膜，其中层状元件具有凹槽和孔，孔的主要部分被放置在凹槽中，并且这些孔或其一部分的表面位于凹槽中或延伸到凹槽中，从而孔理想地放置在凹槽中 相应层状元件与膜的接触面积。
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Patent Agency Ranking
公开(公告)号：US20100092692A1
公开(公告)日：2010-04-15
申请号：US12312999
申请日：2007-11-15
Applicant: Karl-Heinz Dulle , Ulf-Steffen Baeumer , Randolf Kiefer , Peter Woltering , Dirk Hoormann , Stefan Oelmann , Joachim-H. Hoedtke , Oliver Kayser
Inventor： Karl-Heinz Dulle , Ulf-Steffen Baeumer , Randolf Kiefer , Peter Woltering , Dirk Hoormann , Stefan Oelmann , Joachim-H. Hoedtke , Oliver Kayser
CPC classification number: C23C14/024 , C23C14/566
Abstract: The invention relates to a method for coating one or more sides of substrates with catalytically active material, comprising material deposition under vacuum in a vacuum chamber, wherein the following steps are performed: (a) loading the vacuum chamber with at least one substrate, (b) closing and evacuating the vacuum chamber, (c) cleaning the substrate by introducing a gaseous reducing agent into the vacuum chamber, (d) increasing the size of the substrate surface by depositing a vaporous component on the substrate surface, (e) coating by a coating process taken from the group of plasma coating processes, physical gas deposition, sputtering processes or the like, wherein one or more metals and/or alkaline and/or earth alkaline metals or their oxides are applied to the surface of the substrate. This method may be used, for example, for coating electrodes which are used in the chlor-alkali electrolysis.
Abstract translation: 本发明涉及一种用催化活性材料涂覆一层或多层衬底的方法，包括在真空室中真空沉积材料，其中执行以下步骤：（a）用至少一个衬底装载真空室， （b）关闭并排空真空室，（c）通过将气态还原剂引入真空室来清洁基板;（d）通过在基板表面上沉积气态成分来增加基板表面的尺寸，（e）涂层 通过从等离子体涂覆工艺，物理气体沉积，溅射工艺等组中获得的涂覆工艺，其中将一种或多种金属和/或碱土金属和/或碱土金属或其氧化物施加到基材的表面。 该方法可以用于例如用于氯碱电解中的涂覆电极。
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公开(公告)号：US20090236220A1
公开(公告)日：2009-09-24
申请号：US12311309
申请日：2007-09-27
Applicant: Peter Woltering , Karl Heinz Dulle , Randolf Kiefer , Stefan Oelmann , Ulf-Steffen Bäumer
Inventor： Peter Woltering , Karl Heinz Dulle , Randolf Kiefer , Stefan Oelmann , Ulf-Steffen Bäumer
IPC: C25B9/08
Abstract: The invention relates to an electrolysis cell of the single-element type design for chlor-alkali electrolysis plants, comprising an anode compartment and a cathode compartment, each of the two compartments containing an electrode connected to the rear wall of the respective compartment by means of parallel bars. The electrodes are thus subdivided into several sections. In accordance with the invention, at least one of two electrodes is provided with a curved shape in each section, this curved section protruding towards the opposite electrode and pressing a membrane area against the opposite electrode. According to a preferred embodiment, the curved shape of the various electrode sections is obtained by means of springs.
Abstract translation: 本发明涉及一种用于氯碱电解设备的单元型设计的电解槽，包括阳极室和阴极室，两个隔室中的每一个均包含通过相应隔室的后壁连接的电极，借助于 双杠。 电极因此被细分为几个部分。 根据本发明，两个电极中的至少一个在每个部分中设置有弯曲形状，该弯曲部分朝向相对电极突出并且将膜区域压靠在相对电极上。 根据优选实施例，通过弹簧获得各种电极部分的弯曲形状。
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公开(公告)号：US20090159435A1
公开(公告)日：2009-06-25
申请号：US12226100
申请日：2007-04-27
Applicant: Ulf Baumer , Randolf Kiefer , Karl Heinz Dulle , Stefan Oelmann , Peter Woltering , Wolfram Stolp
Inventor： Ulf Baumer , Randolf Kiefer , Karl Heinz Dulle , Stefan Oelmann , Peter Woltering , Wolfram Stolp
IPC: C25B9/08
CPC classification number: C25B9/08
Abstract: The invention relates to an insulating frame of an electrolysis cell having a microstructured internal section allowing the penetration of the electrolyte even if the structured section is partly or completely overlapped by the membrane, and to an electrolysis cell equipped with the same.
Abstract translation: 本发明涉及具有微结构化内部部分的电解槽的绝缘框架，即使结构化部分与膜部分或完全重叠，也允许电解质渗透到电解槽中。
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29.发明申请公开(公告)号：US20080280204A1
公开(公告)日：2008-11-13
申请号：US11632790
申请日：2005-07-09
Applicant: Roland Beckmann , Karl-Heinz Dulle , Peter Woltering , Randolf Kiefer , Frank Holthuis , Frank Funck , Wolfram Stolp , Hans-Joachim Kohnke , Joachim Helmke
Inventor： Roland Beckmann , Karl-Heinz Dulle , Peter Woltering , Randolf Kiefer , Frank Holthuis , Frank Funck , Wolfram Stolp , Hans-Joachim Kohnke , Joachim Helmke
CPC classification number: C25B11/041 , H01M4/32 , H01M4/485 , H01M4/52 , H01M4/8817 , H01M4/8882 , H01M4/9016
Abstract: The invention relates to a method for producing electrically conducting nickel oxide surfaces made of nickel-containing material. According to said method, the nickel surface is first degreased and is then roughened for approximately ten minutes in a solution containing about one percent of hydrochloric acid, said process being accelerated by adding hydrogen peroxide solution, resulting in the electrolyte turning green. The nickel surface is briefly wetted, the nickel material is introduced into a solution of 3.5 molar lye to which about ten percent of hydrogen peroxide is added and is kept therein for ten minutes, and the resulting nickel hydroxide surface is dehydrated in a subsequent thermal process and is then further oxidized to obtain nickel oxide. The invention further relates to a conductive boundary layer that is produced according to said method, the electrodes therefrom, and the use thereof in chlorine-alkali electrolysis processes, in fuel cells and storage batteries.
Abstract translation: 本发明涉及一种用于制造由含镍材料制成的导电氧化镍表面的方法。 根据所述方法，镍表面首先脱脂，然后在含有约1％盐酸的溶液中粗糙化大约十分钟，所述方法通过加入过氧化氢溶液加速，导致电解质变绿。 镍表面短暂润湿，将镍材料引入3.5摩尔碱液的溶液中，向其中加入约10％的过氧化氢并保存在其中10分钟，并将所得氢氧化镍表面在随后的热处理中脱水 然后进一步氧化以获得氧化镍。 本发明还涉及根据所述方法制备的导电边界层，其电极及其在氯碱电解过程中，在燃料电池和蓄电池中的应用。
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公开(公告)号：US20080245661A1
公开(公告)日：2008-10-09
申请号：US11795174
申请日：2006-01-25
Applicant: Roland Beckmann , Karl Heinz Dulle , Randolf Kiefer , Peter Woltering
Inventor： Roland Beckmann , Karl Heinz Dulle , Randolf Kiefer , Peter Woltering
IPC: C25B9/10
Abstract: The invention relates to an electrolytic cell for the production of chlorine from an aqueous alkali halide solution, which mainly consists of two semi-shells, an anode, a cathode and an ion exchange membrane arranged between the electrodes. Spacer elements are arranged between the ion-exchange membrane and the electrodes for fixing the membrane in position and distributing the compressive forces, made of electrically conductive and corrosion-resistant material on at least one side of the membrane
Abstract translation: 本发明涉及一种用于从卤化碱水溶液中生产氯的电解槽，其主要由两个半壳体，阳极，阴极和布置在电极之间的离子交换膜组成。 间隔元件布置在离子交换膜和电极之间，用于将膜固定在适当位置，并将由导电和耐腐蚀材料制成的压缩力分布在膜的至少一侧
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