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    Preparation of antioxidants
    21.
    发明授权
    Preparation of antioxidants 失效
    抗氧化剂的制备

    公开(公告)号：US4317933A

    公开(公告)日：1982-03-02

    申请号：US849828

    申请日：1977-11-09

    申请人： Dane K. Parker

    发明人： Dane K. Parker

    IPC分类号： C07C37/00 ,  C07C67/03 ,  C09K15/08 ,  C07C47/56

    CPC分类号： C07C45/68 ,  C07C37/002 ,  C07C67/03 ,  C09K15/08

    摘要： This invention comprises an alkylation, reduction and transesterification process for the preparation of ester substituted phenols. The products are useful as antioxidants and may be prepared in high yields and with a high degree of purity.

    摘要翻译： 本发明包括用于制备酯取代的酚的烷基化，还原和酯交换方法。 该产品可用作抗氧化剂并且可以以高产率和高纯度制备。

    Compatibilized polymeric systems
    23.
    发明授权
    Compatibilized polymeric systems 失效
    增容聚合体系

    公开(公告)号：US5523351A

    公开(公告)日：1996-06-04

    申请号：US394865

    申请日：1995-02-27

    申请人： Howard A. Colvin ,  Muhanad A. Alsamarraie ,  Dane K. Parker

    发明人： Howard A. Colvin ,  Muhanad A. Alsamarraie ,  Dane K. Parker

    IPC分类号： C08G18/40 ,  C08G18/72 ,  C08L19/00 ,  C08L67/00 ,  C08L77/00 ,  C08L79/02 ,  C08L101/00

    CPC分类号： C08L77/00 ,  C08G18/4009 ,  C08G18/4054 ,  C08G18/728 ,  C08L101/00 ,  C08L19/006 ,  C08L67/00 ,  C08L79/02 ,  C08L2205/08 ,  Y10S525/931

    摘要： The subject invention relates to a process for preparing a compatibilized blend of a first polymer which is a rubber containing free nitrile groups, hydroxyl groups, carboxyl groups, amide groups, amine groups or mercapto groups and a second dissimilar polymer which is a thermoplastic polymer containing nitrile groups, hydroxyl groups, carboxyl groups, amide groups, amine groups or mercapto groups, which comprises reacting a rubber having pendant blocked isocyanate groups bound thereto with the first polymer and the second dissimilar polymer, wherein the compatibilized blend contains from about 55 weight percent to about 75 weight percent of the rubber containing nitrile groups, hydroxyl groups, amide groups, amine groups or mercapto groups.

    摘要翻译： 本发明涉及一种制备第一聚合物的相容化共混物的方法，第一聚合物是含有游离腈基，羟基，羧基，酰胺基，胺基或巯基的橡胶和第二异种聚合物，其是含有 腈基，羟基，羧基，酰胺基，胺基或巯基，其包括使与其结合的侧嵌嵌异氰酸酯基的橡胶与第一聚合物和第二不同聚合物反应，其中相容化共混物含有约55重量％ 至约75重量％的含有腈基的橡胶，羟基，酰胺基，胺基或巯基。

    Process to produce reinforced tire cords with plasma treated fibers incorporated into a rubber/blocked isocyanate composition
    24.
    发明授权
    Process to produce reinforced tire cords with plasma treated fibers incorporated into a rubber/blocked isocyanate composition 失效
    生产具有掺入橡胶/封闭异氰酸酯组合物中的等离子体处理的纤维的加强轮胎帘线的方法

    公开(公告)号：US5501880A

    公开(公告)日：1996-03-26

    申请号：US327333

    申请日：1994-10-21

    申请人： Dane K. Parker ,  Derek Shuttleworth

    发明人： Dane K. Parker ,  Derek Shuttleworth

    IPC分类号： B60C1/00 ,  B60C9/00 ,  C08G18/72 ,  C08G18/80 ,  C08J5/06 ,  C08K7/00 ,  C08K7/02 ,  C08L21/00 ,  D06M10/02 ,  B05D3/02 ,  H05H1/00

    CPC分类号： C08J5/06 ,  B60C1/00 ,  B60C9/00 ,  C08G18/728 ,  C08G18/807 ,  D06M10/025 ,  C08G2380/00 ,  C08J2321/00 ,  D06M2200/50 ,  Y10S156/91

    摘要： By utilizing the process of this invention, the adhesion between polymeric reinforcements and rubber compositions can be greatly improved. This invention more specifically discloses a process for preparing a rubber article containing a polymeric reinforcement which comprises: (1) plasma treating the polymeric reinforcement in a manner whereby reactive groups containing Zerewitinoff active hydrogen atoms are bonded to the surface thereof; (2) incorporating the polymeric reinforcement having Zerewitinoff active hydrogen atoms bonded to the surface thereof into an uncured rubber composition, wherein said rubber composition has pendant blocked isocyanate groups bound thereto; and (3) curing the uncured rubber into the desired shape for the rubber article at an elevated temperature sufficient to deblock the isocyanate groups bonded to the uncured rubber allowing for the isocyanate groups to react with the Zerewitinoff active hydrogen atoms bonded to the surface of the polymeric reinforcement.

    摘要翻译： 通过利用本发明的方法，可以大大提高聚合物增强剂和橡胶组合物之间的粘合性。 本发明更具体地公开了一种制备含有聚合物增强材料的橡胶制品的方法，该方法包括：（1）以含有齐来维诺夫活性氢原子的反应性基团与其表面结合的方式等离子体处理聚合物增强体; （2）将具有与其表面结合的Zerewitinoff活性氢原子的聚合物增强物结合到未固化的橡胶组合物中，其中所述橡胶组合物具有与其结合的侧嵌的异氰酸酯基团; 和（3）将未固化的橡胶固化成橡胶制品所需的形状，使其在足以使结合到未固化橡胶上的异氰酸酯基团脱粘的高温下使异氰酸酯基与与Zerewitinoff活性氢原子键合的 聚合物增强。

    Preparation of sulfur-containing organosilicon compounds
    25.
    发明授权
    Preparation of sulfur-containing organosilicon compounds 失效
    含硫有机硅化合物的制备

    公开(公告)号：US5405985A

    公开(公告)日：1995-04-11

    申请号：US272366

    申请日：1994-07-08

    申请人： Dane K. Parker ,  Richard T. Musleve ,  Robert C. Hirst ,  Roger J. Hopper

    发明人： Dane K. Parker ,  Richard T. Musleve ,  Robert C. Hirst ,  Roger J. Hopper

    IPC分类号： C07F7/18 ,  C07F7/08

    CPC分类号： C07F7/1892

    摘要： The present invention relates to a process for the production of organosilicon compounds of the formulaZ-Alk-S.sub.n -Alk-Z (I)in which Z is selected from the group consisting of ##STR1## where R.sub.1 is an alkyl group of 1 to 4 carbon atoms, cyclohexyl or phenyl;R.sub.2 is alkoxy of 1 to 8 carbon atoms, or cycloalkoxy of 5 to 8 carbon atoms;Alk is a divalent hydrocarbon of 1 to 18 carbon atoms and n is an integer of 2 to 8; comprising reacting (A) a compound of the formula:Z-Alk-X (II)when X is Cl, Br or I; with (B) a compound of the formulaMe.sub.2 S.sub.n (III)where Me is ammonium, or an alkali metal;wherein the reaction is conducted in the presence of a phase transfer catalyst and an aqueous phase.

    摘要翻译： 本发明涉及一种制备式Z-Alk-Sn-Alk-Z（I）的有机硅化合物的方法，其中Z选自下组，其中R 1是1至 4个碳原子，环己基或苯基; R 2是1至8个碳原子的烷氧基或5至8个碳原子的环烷氧基; Alk为1〜18个碳原子的二价烃，n为2〜8的整数， 包括当X是Cl，Br或I时，使（A）式：Z-Alk-X（II）的化合物反应; 与（B）式Me2Sn（III）的化合物，其中Me是铵或碱金属; 其中反应在相转移催化剂和水相存在下进行。

    Polymerizable synergist and antidegradant
    26.
    发明授权
    Polymerizable synergist and antidegradant 失效
    可聚合增效剂和抗降解剂

    公开(公告)号：US5216049A

    公开(公告)日：1993-06-01

    申请号：US946722

    申请日：1992-09-18

    申请人： Dane K. Parker ,  Gerald O. Schulz

    发明人： Dane K. Parker ,  Gerald O. Schulz

    IPC分类号： C08K5/17 ,  C08K5/13 ,  C08K5/36 ,  C08K5/375 ,  C08L7/00 ,  C08L9/00 ,  C08L21/00 ,  C08L23/02 ,  C08L101/00

    CPC分类号： C08K5/375

    摘要： The present invention relates to an antidegradant system comprised of (A) an antidegradant selected from the group consisting of phenolic antidegradants, amine antidegradants and mixtures thereof; and (B) a unique polymerizable synergist. In addition, there is disclosed a stabilized polymer comprising (A) a polymer selected from the group consisting of (1) homopolymers and copolymers of monoolefins; (2) natural rubber; and (3) synthetic rubber derived from a diene monomer; (B) from about 0.05 to about 10 parts by weight based upon 100 parts of polymer of an antidegradant selected from the group consisting of phenolic antidegradants, amine antidegradants and mixtures thereof; and (C) from about 0.05 to about 20 parts by weight based upon 100 parts of polymer of a unique polymerizable aromatic sulfide synergist.

    摘要翻译： 本发明涉及一种抗降解剂体系，其包含（A）选自酚类抗降解剂，胺类抗降解剂及其混合物的抗降解剂; 和（B）独特的可聚合增效剂。 此外，公开了一种稳定的聚合物，其包含（A）选自（1）单烯烃的均聚物和共聚物的聚合物; （2）天然橡胶; 和（3）衍生自二烯单体的合成橡胶; （B）约0.05至约10重量份，基于100份选自酚类抗降解剂，胺类抗降解剂及其混合物的抗降解剂的聚合物; 和（C）约0.05至约20重量份，基于100份独特的可聚合芳族硫醚增效剂的聚合物。

    Crosslinkable rubber composition
    27.
    发明授权
    Crosslinkable rubber composition 失效
    可交联橡胶组合物

    公开(公告)号：US5173557A

    公开(公告)日：1992-12-22

    申请号：US716455

    申请日：1991-06-17

    申请人： Dane K. Parker ,  Arthur H. Weinstein ,  Howard A. Colvin

    发明人： Dane K. Parker ,  Arthur H. Weinstein ,  Howard A. Colvin

    IPC分类号： C08C19/30 ,  C08G18/69 ,  C08G18/72 ,  C08J3/24

    CPC分类号： C08J3/24 ,  C08C19/30 ,  C08G18/69 ,  C08G18/728 ,  C08J2321/00

    摘要： It is sometimes desirable to cure rubber compositions utilizing non-sulfur curing agents. The subject invention reveals rubber compositions which can be cured without utilizing sulfur or sulfur containing compounds. The subject invention more specifically discloses a rubber composition which can be crosslinked by heating which is comprised of (1) at least one rubber having pendant blocked isocyanate groups bound thereto; and (2) at least one compound which contains at least 2 Zerewitinoff active hydrogens.This invention also discloses crosslinking of elastomer compounds containing (1) at least one rubber having functionalized groups containing at least one Zerewitinoff active hydrogen and (2) at least one compound which contains at least two blocked isocyanate groups. This invention also discloses self-curing elastomers containing both blocked isocyanate groups and groups containing at least one active Zerewitinoff hydrogen.

    摘要翻译： 有时希望使用非硫固化剂固化橡胶组合物。 本发明揭示了可以在不使用含硫或含硫化合物的情况下固化的橡胶组合物。 本发明更具体地公开了一种可通过加热交联的橡胶组合物，其包含（1）至少一种具有与其结合的侧嵌的异氰酸酯基的橡胶; 和（2）至少一种含有至少2个Zerewitinoff活性氢的化合物。 本发明还公开了含有（1）至少一种含有至少一个Zerewitinoff活性氢的官能化基团的橡胶和（2）至少一种含有至少两个封端异氰酸酯基团的化合物的弹性体化合物的交联。 本发明还公开了含有封端异氰酸酯基团和含有至少一种活性齐维诺芬氢的基团的自固化弹性体。