A NOVEL LIVING RADICAL POLYMERIZATION METHOD
    31.
    发明申请
    A NOVEL LIVING RADICAL POLYMERIZATION METHOD 有权
    一种新型的生物辐射聚合方法

    公开(公告)号:US20070049715A1

    公开(公告)日:2007-03-01

    申请号:US11459370

    申请日:2006-07-24

    摘要: A highly active and environment-friendly catalyst for use in a living radical polymerization is provided. A catalyst for use in a living radical polymerization method is provided. The catalyst comprises a central element, which is selected from germanium, tin and antimony, and at least one halogen atom, which is bound to the central element. A monomer having a radical reactive unsaturated bond is subjected to a radical polymerization reaction under the presence of the catalyst, thereby it is possible to obtain a polymer having narrow molecular weight distribution. The present invention has the merits such as low toxicity of the catalyst, a small amount of the catalyst can be used, high solubility of the catalyst, mild reaction conditions, no coloration, no odor (unnecessary post-treatment of molded products). The method of the present invention is more environment-friendly and economical than a conventional living radical polymerization method.

    摘要翻译: 提供了用于活性自由基聚合的高活性和环境友好的催化剂。 提供了一种用于活性自由基聚合方法的催化剂。 该催化剂包括选自锗,锡和锑的中心元素和与中心元素结合的至少一个卤素原子。 具有自由基反应性不饱和键的单体在催化剂的存在下进行自由基聚合反应,从而可以得到分子量分布窄的聚合物。 本发明具有催化剂毒性低,可使用少量催化剂,催化剂溶解性高,反应条件温和,无着色,无异味(成型品不必要后处理)等优点。 本发明的方法比常规的活性自由基聚合方法更环保且更经济。

    Optical waveguide in the interior of silica glass and method of forming optical waveguide
    33.
    发明授权
    Optical waveguide in the interior of silica glass and method of forming optical waveguide 失效
    石英玻璃内部的光波导和形成光波导的方法

    公开(公告)号:US06945078B2

    公开(公告)日:2005-09-20

    申请号:US10644827

    申请日:2003-08-21

    摘要: When an optical waveguide is formed by focused femtosecond laser pulses in a pure silica glass to induce a refractive index increase region, a pulse width of femtosecond laser pulses are changed, a peak power of femtosecond laser pulses at the focal point is changed, or both the pulse width and the peak power are changed simultaneously. Under conditions where a pulse width of the femtosecond laser pulses is in a range of 210 to 420 fs and a peak power at the focal point is not greater than 8.7×1011 W/cm2, an optical waveguide having a mode field of 10 to 14 μm such that an aspect ratio is 1 (one) can be obtained. By doing this, it is possible to control a mode field diameter of an optical waveguide and an aspect ratio of the mode field diameter.

    摘要翻译: 当通过在纯二氧化硅玻璃中的聚焦飞秒激光脉冲形成光波导以引起折射率增加区域时,飞秒激光脉冲的脉冲宽度改变,焦点处的飞秒激光脉冲的峰值功率改变,或两者都改变 脉冲宽度和峰值功率同时变化。 在飞秒激光脉冲的脉冲宽度在210至420fs的范围内且焦点处的峰值功率不大于8.7x10 11 / cm 2的条件下, / SUP>,具有10〜14μm的模场的光波导,使得可以获得纵横比为1(1)。 通过这样做,可以控制光波导的模场直径和模场直径的纵横比。

    Method for the continuous production of silicon oxide powder
    35.
    发明授权
    Method for the continuous production of silicon oxide powder 有权
    连续生产氧化硅粉末的方法

    公开(公告)号:US06821495B2

    公开(公告)日:2004-11-23

    申请号:US09773677

    申请日:2001-02-02

    IPC分类号: C01B3320

    摘要: A silicon oxide powder can be continuously prepared by feeding a raw material powder mixture containing silicon dioxide powder into a reaction chamber (2) at a temperature of 1,100-1,600° C., to produce a silicon oxide gas, transferring the silicon oxide gas to a deposition chamber (11) through a transfer conduit (10) maintained at a temperature of from higher than 1,000° C. to 1,300° C., causing silicon oxide to deposit on a substrate (13) which is disposed and cooled in the deposition chamber, scraping the silicon oxide deposit, and recovering the deposit in a recovery chamber (18). The method and apparatus is capable of continuous and stable production of amorphous silicon oxide powder of high purity.

    摘要翻译: 可以通过在1100〜1600℃的温度下将含有二氧化硅粉末的原料粉末混合物进料到反应室(2)中来连续制备氧化硅粉末,以产生氧化硅气体,将氧化硅气体转移到 沉积室(11),其通过保持在高于1,000℃至1300℃的温度的转移管道(10),使得氧化硅沉积在沉积物中的基底(13)上,所述基底(13)在沉积物中被设置和冷却 刮除氧化硅沉积物,并将沉积物回收到回收室(18)中。 该方法和装置能够连续且稳定地生产高纯度的无定形氧化硅粉末。

    Rotary developing device having adjustably mounted developing units
    36.
    发明授权
    Rotary developing device having adjustably mounted developing units 失效
    具有可调节安装的显影单元的旋转显影装置

    公开(公告)号:US6104898A

    公开(公告)日:2000-08-15

    申请号:US373981

    申请日:1999-08-16

    IPC分类号: G03G15/01 G03G15/08

    CPC分类号: G03G15/0126 G03G2215/0177

    摘要: A rotary developing device which facilitates a positional adjustment of developing units and prevents the developing units from being shifted even when they are used for a long period. Pins protruding from a revolver are inserted into elongated holes formed in developing units so that developing units are held in such a manner that the developing units are movable relative to the revolver. By mounting a spacer between the elongated hole and the pin, the positional adjustment of the photosensitive drum and the tracking roller is completed. Furthermore, a plurality of spacers which differ in thickness are prepared and by merely selectively mounting an appropriate spacer, the position adjustment of the tracking roller is completed.

    摘要翻译: 一种旋转显影装置,其便于显影单元的位置调整,并且即使长时间使用也可防止显影单元的移位。 从左轮手枪突出的销钉插入形成在显影单元中的长孔中,使得显影单元被保持为使得显影单元相对于左轮可移动。 通过在长孔和销之间安装间隔件,完成感光鼓和跟踪辊的位置调整。 此外,准备了多个不同厚度的间隔件,并且通过仅选择性地安装适当的间隔件,完成了跟踪辊的位置调整。

    Alumina particles having high dispersibility and plasticity
    37.
    发明授权
    Alumina particles having high dispersibility and plasticity 失效
    氧化铝颗粒具有高分散性和可塑性

    公开(公告)号:US06015456A

    公开(公告)日:2000-01-18

    申请号:US697470

    申请日:1996-08-23

    摘要: Alumina particles having high dispersibility and plasticity, at least on the surface of which a phosphoric acid or phosphate is present and suitable for use as a material for pigments for paints, precision abrasives or ceramics. The alumina particles are produced by adding a crystallization inhibitor containing at least phosphate ion to aluminum hydroxide or alumina hydrate and then conducting a hydrothermal synthesis treatment. The amount of the phosphate ion to be added is in the range of 3.0.times.10.sup.-3 to 2.5.times.10.sup.-2 mol per mol of aluminum hydroxide or alumina hydrate. The particle size of aluminum hydroxide or alumina hydrate is 0.1 to 5.0 .mu.m. The hydrothermal synthesis is preferably conducted at 350.degree. C. or above under a pressure of 50 to 200 atm and at a temperature elevation rate of 50.degree. C./min to 0.3.degree. C./min. The thus obtained alumina is .alpha.-alumina in the form of hexagonal plate single crystal having a particle size of 0.2 to 15 .mu.m, an aspect ratio of 15 to 50 and an isoelectric point at which the zeta-potential is 0 of pH 4 to 8.

    摘要翻译: 氧化铝颗粒具有高分散性和可塑性,至少在其表面上存在磷酸或磷酸盐,并且适合用作涂料,精密磨料或陶瓷颜料的材料。 氧化铝颗粒通过向氢氧化铝或氧化铝水合物中加入至少含有磷酸根离子的结晶抑制剂,然后进行水热合成处理来制备。 磷酸根离子的添加​​量相对于每摩尔氢氧化铝或氧化铝水合物为3.0×10 -3〜2.5×10 -2摩尔。 氢氧化铝或氧化铝水合物的粒径为0.1〜5.0μm。 水热合成优选在50〜200atm的压力和50℃/分钟〜0.3℃/分钟的升温速度下在350℃以上进行。 由此获得的氧化铝是粒径为0.2至15μm,纵横比为15至50的六方板单晶形式的α-氧化铝,ζ电位为0的等电点为pH4至 8。

    Method of and apparatus for performing continuous hydrothermal synthesis
    38.
    发明授权
    Method of and apparatus for performing continuous hydrothermal synthesis 失效
    进行连续水热合成的方法和装置

    公开(公告)号:US5910298A

    公开(公告)日:1999-06-08

    申请号:US779351

    申请日:1997-01-06

    摘要: A continuous hydrothermal synthesis method which comprises pressurizing and heating a material slurry below a saturated vapor temperature or pressurizing a material slurry at normal temperature, pressurizing and heating an aqueous liquid above the saturated vapor temperature, atomizing and mixing the slurry and the aqueous liquid, effecting hydrothermal synthesis in a reaction section above the saturated vapor temperature, cooling the reaction product and taking out the product while retaining the pressurized state in the system by alternately opening and closing shut-off valves provided above and below a product discharging section or through a thin pipe provided in the product discharging section. The method is performed using an apparatus comprising heating-pressurizing sections respectively connected to a material slurry feeding section and an aqueous liquid feeding section, an atomizing-mixing section and a reaction section provided after these feeding sections, and a product discharging section.

    摘要翻译: 一种连续的水热合成方法,其特征在于,在饱和蒸气温度以下加压和加热材料浆料或在常温下加压材料浆料,对饱和蒸汽温度以上的水性液体进行加压加热,雾化并混合浆料和水性液体, 在高于饱和蒸汽温度的反应段中进行水热合成,冷却反应产物并取出产物,同时通过交替地打开和关闭设置在产品排放部分上方和下方的截止阀,或通过薄的 产品排放部分设有管道。 该方法使用包括分别连接到材料浆料供给部分和水性液体供给部分的加热加压部分,设置在这些进料部分之后的雾化混合部分和反应部分的装置以及产品排出部分进行。