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    Process for the preparation of a polyurethane polymer with secondary hydroxyl end groups comprising polyester polyols
    32.
    发明授权
    Process for the preparation of a polyurethane polymer with secondary hydroxyl end groups comprising polyester polyols 有权
    用于制备具有包含聚酯多元醇的仲羟基端基的聚氨酯聚合物的方法

    公开(公告)号：US09139685B2

    公开(公告)日：2015-09-22

    申请号：US13381139

    申请日：2010-06-29

    申请人： Hartmut Nefzger ,  Jörg Hofmann ,  Bert Klesczewski ,  Erika Bauer ,  Klaus Lorenz

    发明人： Hartmut Nefzger ,  Jörg Hofmann ,  Bert Klesczewski ,  Erika Bauer ,  Klaus Lorenz

    IPC分类号： C08G18/00 ,  C08G18/42 ,  C08G18/76 ,  C08G63/91 ,  C08G77/46 ,  C08G101/00

    CPC分类号： C08G18/4291 ,  C08G18/4241 ,  C08G18/4261 ,  C08G18/4263 ,  C08G18/7621 ,  C08G63/916 ,  C08G77/46 ,  C08G2101/0008 ,  C08G2101/005 ,  C08G2101/0083

    摘要： The invention relates to a process for the preparation of a polyurethane polymer, comprising the step of reaction ofA) polyester polyols with secondary hydroxyl end groups, which are obtainable from the reaction of a polyester comprising carboxyl end groups with an epoxide of the general formula (1): wherein R1 represents an alkyl radical or an aryl radical and wherein the polyester comprising carboxyl end groups has an acid number of from ≧25 mg of KOH/g to ≦400 mg of KOH/g and a hydroxyl number of ≦5 mg of KOH/g, with B) polyisocyanates which are chosen from the group comprising toluoylene-diisocyanate, diphenylmethane-diisocyanate, polymeric diphenylmethane-diisocyanate, xylylene-diisocyanate, naphthylene-diisocyanate, hexamethylene-diisocyanate, diisocyanatodicyclohexylmethane and/or isophorone-diisocyanate. The invention furthermore relates to polyurethane polymers prepared by such a process.

    摘要翻译： 本发明涉及一种制备聚氨酯聚合物的方法，包括A）聚酯多元醇与仲羟基端基反应的步骤，其可从包含羧基端基的聚酯与通式 （1）表示：其中R1表示烷基或芳基，其中包含羧基端基的聚酯的酸值为≥25mgKOH / g至＆lt; NlE; 400mg KOH / g，羟值为＆ ; B）多异氰酸酯，其选自甲苯二异氰酸酯，二苯基甲烷二异氰酸酯，聚合二苯基甲烷二异氰酸酯，亚二甲苯基二异氰酸酯，亚萘基二异氰酸酯，六亚甲基二异氰酸酯，二异氰酸二环己基甲烷和/或异佛尔酮 - 二异氰酸酯。 本发明还涉及通过这种方法制备的聚氨酯聚合物。

    PROCESS FOR THE PREPARATION OF POLYETHER POLYOLS
    36.
    发明申请
    PROCESS FOR THE PREPARATION OF POLYETHER POLYOLS 审中-公开
    制备聚醚多元醇的方法

    公开(公告)号：US20140107245A1

    公开(公告)日：2014-04-17

    申请号：US14122723

    申请日：2012-05-30

    申请人： Jörg Hofmann ,  Bert Klesczewski ,  Michael Schneider

    发明人： Jörg Hofmann ,  Bert Klesczewski ,  Michael Schneider

    IPC分类号： C08G65/331 ,  C08G71/04

    CPC分类号： C08G65/331 ,  C08G18/4866 ,  C08G18/4887 ,  C08G64/183 ,  C08G64/34 ,  C08G65/2663 ,  C08G65/2696 ,  C08G71/04 ,  C08G2101/0008 ,  C08G2101/005 ,  C08G2101/0083

    摘要： The invention relates to a method for producing polyether carbonate polyols, wherein (i) in a first step a polyether carbonate polyol is produced from one or more H-functional starter substances, one or more alkylene oxides, and carbon dioxide in the presence of at least one DMC catalyst, and (ii) in a second step the polyether carbonate polyol is chain-extended with a mixture of at least two different alkylene oxides in the presence of at least one DMC catalyst. The invention further relates to polyether carbonate polyols that contain a terminal mixed block of at least two alkylene oxides and to a method for producing soft polyurethane foams, wherein a polyol component containing a polyether carbonate polyol according to the invention is used.

    摘要翻译： 本发明涉及一种生产聚醚碳酸酯多元醇的方法，其中（i）在第一步中聚醚碳酸酯多元醇由一种或多种H官能起始物质，一种或多种环氧烷和二氧化碳在有 至少一种DMC催化剂，和（ii）在至少一种DMC催化剂的存在下，聚醚碳酸酯多元醇与至少两种不同的环氧烷烃的混合物链延伸。 本发明还涉及含有至少两种烯化氧的末端混合嵌段的聚醚碳酸酯多元醇和用于生产软质聚氨酯泡沫体的方法，其中使用含有本发明的聚醚碳酸酯多元醇的多元醇组分。

    PROCESS FOR THE PRODUCTION OF POLYETHER POLYOLS WITH A HIGH ETHYLENE OXIDE CONTENT
    38.
    发明申请
    PROCESS FOR THE PRODUCTION OF POLYETHER POLYOLS WITH A HIGH ETHYLENE OXIDE CONTENT 审中-公开
    具有高乙烯氧化物含量的聚醚多元醇的生产方法

    公开(公告)号：US20110230581A1

    公开(公告)日：2011-09-22

    申请号：US12725631

    申请日：2010-03-17

    申请人： Bert Klescewski ,  Jörg Hofmann ,  Klaus Lorenz ,  Jack R. Reese ,  Jose F. Pazos

    发明人： Bert Klescewski ,  Jörg Hofmann ,  Klaus Lorenz ,  Jack R. Reese ,  Jose F. Pazos

    IPC分类号： C07C43/11 ,  C08G18/32

    CPC分类号： C08G65/2663 ,  C08G65/2696 ,  C08G2650/24

    摘要： Polyether polyols with an OH number of from 15 to 120 mg of KOH/g are produced by (i) introducing a mixture of DMC catalyst and a poly(oxyalkylene)polyol or a mixture of DMC catalyst and a polyether polyol (“heel”) obtainable by the process according to the invention is initially into a reactor and (ii) continuously introducing one (or more) low molecular weight starter compound(s) with a (mixed) hydroxyl functionality of from 2.2 to 6.0 and a mixture composed of a) 73 to 80 parts by weight (per 100 parts by weight of a) plus b)) of ethylene oxide and b) 27 to 20 parts by weight (per 100 parts by weight of a) plus b)) of at least one substituted alkylene oxide corresponding to a specified formula into the mixture from step (i). These polyether polyols are particularly useful for the production of flexible polyurethane foams.

    摘要翻译： 通过（i）引入DMC催化剂和聚（氧化烯）多元醇或DMC催化剂和聚醚多元醇（“跟”）的混合物的混合物制备OH数为15至120mg KOH / g的聚醚多元醇， 通过根据本发明的方法可获得的化合物最初进入反应器，和（ii）连续引入一种（或多种）低分子量起始化合物与（混合）羟基官能度为2.2至6.0的混合物和由 ）73至80重量份（每100重量份a）加b））环氧乙烷和b）27至20重量份（每100重量份a）加b））至少一个取代的 对应于规定式的氧化烯进入步骤（i）的混合物中。 这些聚醚多元醇特别可用于生产软质聚氨酯泡沫体。