摘要:
An aqueous titanium oxide-dispersed sol comprising titanium oxide particles dispersed in water, said sol comprising chloride ions in an amount of 50 to 10,000 ppm by weight as the chlorine element. Titanium tetrachloride is hydrolyzed to form an aqueous titanium oxide-dispersed sol and the chloride ion concentration thereof is controlled. Another aqueous titanium oxide-dispersed sol comprising brookite-type titanium oxide particles dispersed in water, said titanium oxide particles having an average particle size of not more than 0.5 μm and a specific surface area of not less than 20 m2/g. Addition of titanium tetrachloride to hot water at 75 to 100° C. followed by hydrolysis at 75° C. to the boiling point of the mixture.
摘要:
A motion detection means 5 has a power generation detection circuit 51 for detecting the output voltage of a generating means 4, and a decision unit 52 for determining if the radio-controlled timepiece 1 is moving based on the output voltage from the power generation detection circuit 51. If when a standard time signal is to be received by means of a receiver 2 the not moving detection signal indicating that the radio-controlled timepiece 1 is not moving is output from the motion detection means 5, the reception operation is executed and the time displayed on the time display means 3 is adjusted. By receiving the standard time signal when the radio-controlled timepiece 1 is not moving, accurate time information can be received and the reliability of standard time signal reception can be improved because the reception success rate is also improved.
摘要:
An aqueous titanium oxide-dispersed sol comprising titanium oxide particles dispersed in water, said sol comprising chloride ions in an amount of 50 to 10,000 ppm by weight as the chlorine element. Titanium tetrachloride is hydrolyzed to form an aqueous titanium oxide-dispersed sol and the chloride ion concentration thereof is controlled. Another aqueous titanium oxide-dispersed sol comprising brookite-type titanium oxide particles dispersed in water, said titanium oxide particles having an average particle size of not more than 0.5 &mgr;m and a specific surface area of not less than 20 m2/g. Addition of titanium tetrachloride to hot water at 75 to 100° C. followed by hydrolysis at 75° C. to the boiling point of the mixture.
摘要:
An aqueous titanium oxide-dispersed sol comprising titanium oxide particles dispersed in water, said sol comprising chloride ions in an amount of 50 to 10,000 ppm by weight as the chlorine element. Titanium tetrachloride is hydrolyzed to form an aqueous titanium oxide-dispersed sol and the chloride ion concentration thereof is controlled. Another aqueous titanium oxide-dispersed sol comprising brookite-type titanium oxide particles dispersed in water, said titanium oxide particles having an average particle size of not more than 0.5 &mgr;m and a specific surface area of not less than 20 m2/g. Addition of titanium tetrachloride to hot water at 75 to 100° C. followed by hydrolysis at 75° C. to the boiling point of the mixture.
摘要:
A fine silica tube composed of silica gel and having an outer diameter of 0.05 to 2 .mu.m wherein the cylindrical wall portion of the tube has a cross-section defined by a substantially square outer periphery and a substantially square vacant center, or by a circular outer periphery and a substantially square vacant center; and a fine silica tube composed of silica glass and having an outer diameter of 0.05 to 1.4 .mu.m wherein the cylindrical wall portion of the tube has a cross-section defined by a substantially square outer periphery and a substantially square vacant center. The fine silica gel tube is made by treating a tetraalkoxysilane with ammonia or aqueous ammonia in a water-soluble alcohol medium in the presence of tartaric acid, citric acid, a tartaric acid salt or a citric acid salt, whereby the tetraalkoxysilane is hydrolyzed. The fine silica glass tube is made by calcining the fine silica gel tube at 800.degree. to 1,400.degree. C.
摘要:
Disclosed is a non-aqueous secondary battery having a positive electrode composed of a polymer of aniline or an aniline derivative and a negative electrode composed of (i) and alkali metal, (ii) an alkali metal alloy, (iii) an electroconductive polymer or (iv) an alkali metal or alkali metal alloy/electroconductive polymer composite, wherein the polymer of aniline or an aniline derivative is formed by converting a doped polymer obtained by oxidative polymerization to an undoped state.
摘要:
A battery having electrodes, at least one of which is made of a polymeric compound having conjugated double bonds in the main chain, is described. The organic solvent of an electrolytic solution in the battery is selected from nitrile compounds of the formulae (I) and (II):R--CN (I)wherein R is a C2-7 alkyl, a saturated alicyclic C3-7 hydrocarbon residue, CH.sub.3 --(CH.sub.2).sub.x --O--(CH.sub.2).sub.y or NC--CH.sub.2).sub.z (x, y and z are 0 or a positive integer of up to 5), and ##STR1## wherein R.sub.1 is --(CH.sub.2).sub.p --CN, --O--(CH.sub.2).sub.q --CN or ##STR2## in which R.sub.3 is a C1-5 alkyl and p, q and r are 0 or a positive integer of up to 5, R.sub.2 is C1-5 alkyl, C1-5 alkoxy or --CH.sub.2).sub.l --CN in which l is 0 or a positive integer of up to 3, and m is a positive integer of up to 3, and n is 0 or a positive integer of up to 3.