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    METHOD FOR PRODUCING ISOLATABLE OXIDE MICROPARTICLES OR HYDROXIDE MICROPARTICLES
    3.
    发明申请
    METHOD FOR PRODUCING ISOLATABLE OXIDE MICROPARTICLES OR HYDROXIDE MICROPARTICLES 有权
    生产不溶性氧化镁微量元素或羟基微量元素的方法

    公开(公告)号：US20130156682A1

    公开(公告)日：2013-06-20

    申请号：US13818954

    申请日：2011-08-26

    申请人： Jun Kuraki ,  Kaeko Araki ,  Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

    发明人： Jun Kuraki ,  Kaeko Araki ,  Masaki Maekawa ,  Daisuke Honda ,  Masakazu Enomura

    IPC分类号： C01G23/053 ,  C01F5/14 ,  C01F17/00

    CPC分类号： C01G23/0536 ,  B01D9/0009 ,  B01F7/00775 ,  B01F7/00791 ,  B82Y30/00 ,  C01B13/36 ,  C01F5/02 ,  C01F5/14 ,  C01F5/20 ,  C01F17/0043 ,  C01G1/02 ,  C01G23/0532 ,  C01G25/02 ,  C01P2002/54 ,  C01P2004/04 ,  C01P2004/64

    摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.

    摘要翻译： 一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置 相对于另一个。 混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。 之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

    Stable Sub-Micron Titania Sols
    5.
    发明申请
    Stable Sub-Micron Titania Sols 有权
    稳定的亚微米级二氧化钛溶液

    公开(公告)号：US20120283092A1

    公开(公告)日：2012-11-08

    申请号：US13550954

    申请日：2012-07-17

    申请人： David M. Chapman

    发明人： David M. Chapman

    IPC分类号： B01J21/06 ,  B01J21/08

    CPC分类号： B01J21/063 ,  B01D53/885 ,  B01D53/9418 ,  B01D2255/20707 ,  B01D2259/804 ,  B01J23/22 ,  B01J23/30 ,  B01J35/002 ,  B01J35/004 ,  B01J35/023 ,  C01G23/047 ,  C01G23/0532 ,  C01P2004/04 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/22 ,  C09C1/3669

    摘要： The present invention is directed to compositions and processes for the production of stable, alkaline, high solids, low viscosity, low surface tension, low flammability, sub-micron titania sols that have minimal offensive odor and methods of their use. Compositions of the present invention include, for example, mixtures of strong and weak organic bases used as dispersants to stabilize the titania sols. The dispersant mixtures have been found to result in relatively high titania solids content, low surface tension, low viscosity suspensions that are low in flammability. Sols produced according to the present invention can be used, for example, in catalytic applications such as catalyst supports for diesel emission control, or in pollutant photocatalyst applications in which it is desirable to have the titania in sol form.

    摘要翻译： 本发明涉及用于生产稳定，碱性，高固体，低粘度，低表面张力，低可燃性，亚微米级二氧化钛溶胶的组合物和方法，其具有最小的令人反感的气味及其使用方法。 本发明的组合物包括例如用作分散剂的强和弱有机碱的混合物以稳定二氧化钛溶胶。 已经发现分散剂混合物导致相对高的二氧化钛固体含量，低表面张力，低粘度悬浮液，其易燃性低。 根据本发明生产的硫醇可用于例如催化应用，例如用于柴油机排放控制的催化剂载体，或者其中希望具有溶胶形式的二氧化钛的污染光催化剂应用中。

    Stable sub-micron titania sols
    6.
    发明授权
    Stable sub-micron titania sols 有权
    稳定的亚微米级二氧化钛溶胶

    公开(公告)号：US08247343B2

    公开(公告)日：2012-08-21

    申请号：US12618484

    申请日：2009-11-13

    申请人： David M. Chapman

    发明人： David M. Chapman

    IPC分类号： B01J31/02 ,  B01J21/08 ,  B01J23/10 ,  B23B5/16 ,  C01G23/053 ,  C01G23/08

    CPC分类号： B01J21/063 ,  B01D53/885 ,  B01D53/9418 ,  B01D2255/20707 ,  B01D2259/804 ,  B01J23/22 ,  B01J23/30 ,  B01J35/002 ,  B01J35/004 ,  B01J35/023 ,  C01G23/047 ,  C01G23/0532 ,  C01P2004/04 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/22 ,  C09C1/3669

    摘要： The present invention is directed to compositions and processes for the production of stable, alkaline, high solids, low viscosity, low surface tension, low flammability, sub-micron titania sols that have minimal offensive odor and methods of their use. Compositions of the present invention include, for example, mixtures of strong and weak organic bases used as dispersants to stabilize the titania sols. The dispersant mixtures have been found to result in relatively high titania solids content, low surface tension, low viscosity suspensions that are low in flammability. Sols produced according to the present invention can be used, for example, in catalytic applications such as catalyst supports for diesel emission control, or in pollutant photocatalyst applications in which it is desirable to have the titania in sol form.

    摘要翻译： 本发明涉及用于生产稳定，碱性，高固体，低粘度，低表面张力，低可燃性，亚微米级二氧化钛溶胶的组合物和方法，其具有最小的令人反感的气味及其使用方法。 本发明的组合物包括例如用作分散剂的强和弱有机碱的混合物以稳定二氧化钛溶胶。 已经发现分散剂混合物导致相对高的二氧化钛固体含量，低表面张力，低粘度悬浮液，其易燃性低。 根据本发明生产的硫醇可用于例如催化应用，例如用于柴油机排放控制的催化剂载体，或者其中希望具有溶胶形式的二氧化钛的污染光催化剂应用中。

    Method for producing high-active titanium dioxide hydrosol by using metatitanate as precursor
    7.
    发明授权
    Method for producing high-active titanium dioxide hydrosol by using metatitanate as precursor 有权
    以偏钛酸盐为前驱体制备高活性二氧化钛水溶胶的方法

    公开(公告)号：US07897137B2

    公开(公告)日：2011-03-01

    申请号：US11372874

    申请日：2006-03-10

    申请人： Fangbai Li ,  Tongxu Liu

    发明人： Fangbai Li ,  Tongxu Liu

    IPC分类号： C01G23/047 ,  C01G23/08

    CPC分类号： C01G23/053 ,  B01J21/063 ,  B01J23/10 ,  B01J23/50 ,  B01J23/745 ,  B01J35/004 ,  B01J37/033 ,  B01J37/036 ,  C01G23/00 ,  C01G23/0532 ,  C01P2002/72 ,  C01P2002/84 ,  C01P2004/03 ,  C01P2006/80 ,  H01L2924/0002 ,  H01L2924/00

    摘要： A method for producing high-active titanium dioxide anatase hydrosol by using metatitanate as precursor, is characterized in comprising the following steps in order: (1) Wash process: adding alkali to wash so as to remove sulfate ion; (2) Dispersion process: adding acid to disperse the filter cake and obtaining a uniform suspension; (3) Peptization process: peptizing the suspension obtained in dispersion process according to the method of (a), (b) or (c). When producing transition metal or rare earth doped anatase hydrosol, transition metal or rare earth salt solution with a predetermined concentration is first prepared, and then added into the metatitanate suspension which has not been washed by alkali. Subsequently, the resulting suspension is filtered and washed until no sulfate ion is present. When producing precious metal deposited anatase hydrosol, precious metal solution is added into prepared pure anatase hydrosol, and then, the resulting solution is irradiated with ultraviolet light for 0.5-10 hours under stirring continuously. The advantages and beneficial effects of the present invention are as follows: (1) the raw material has low price and little pollution as well as abundant source; (2) the hydrosol has excellent degree of dispersibility and higher anatase crystallization; (3) the hydrosol has higher activity under visible light irradiation owing to doping/depositing technique; (4) the properties and activity of the hydrosol can be further enhanced by using post disposal, such as microwave and ultrasonic technique; and (5) the hydrosol is a kind of nano-material with about 10 nm particle size. The anatase hydrosol can be applied for indoor air purification, crop disease control, odor control and so on.

    摘要翻译： 以钛酸锶为原料制备高活性二氧化钛锐钛矿型水溶胶的方法，其特征在于包括以下步骤：（1）洗涤方法：加碱洗涤以除去硫酸根离子; （2）分散工艺：加入酸分散滤饼并获得均匀的悬浮液; （3）胶溶过程：根据（a），（b）或（c）的方法对分散过程中获得的悬浮液进行胶溶。 当制备过渡金属或稀土掺杂的锐钛矿水溶胶时，首先制备预定浓度的过渡金属或稀土盐溶液，然后加入未经碱洗的偏钛酸盐悬浮液中。 随后，将所得悬浮液过滤并洗涤直至不存在硫酸根离子。 当制备贵金属沉积锐钛矿型水溶胶时，将贵金属溶液加入到制备的纯锐钛矿水溶胶中，然后将所得溶液在持续搅拌下用紫外线照射0.5-10小时。 本发明的优点和有益效果如下：（1）原料价格低，污染少，来源丰富; （2）水溶胶具有优异的分散性和较高的锐钛矿结晶度; （3）由于掺杂/沉积技术，水溶胶在可见光照射下具有较高的活性; （4）通过微波和超声波技术等后处理可以进一步提高水溶胶的性能和活性; 和（5）水溶胶是一种具有约10nm粒径的纳米材料。 锐钛型水溶胶可用于室内空气净化，作物病害控制，气味控制等。

    TITANIUM DIOXIDE
    8.
    发明申请
    TITANIUM DIOXIDE 有权
    二氧化钛

    公开(公告)号：US20110041726A1

    公开(公告)日：2011-02-24

    申请号：US12935600

    申请日：2009-05-01

    申请人： John Robb ,  John L. Edwards ,  John Temperley ,  Robert Bird ,  Paul C. Bradley ,  Anthony G. Jones

    发明人： John Robb ,  John L. Edwards ,  John Temperley ,  Robert Bird ,  Paul C. Bradley ,  Anthony G. Jones

    IPC分类号： C09D1/00 ,  C09D11/00

    CPC分类号： C09D5/032 ,  C01G23/0532 ,  C01P2004/03 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2006/62 ,  C01P2006/63 ,  C01P2006/64 ,  C08K3/22 ,  C09C1/3661 ,  C09D5/004 ,  C09D7/61 ,  C09D7/68 ,  C09D7/69 ,  C09D11/037

    摘要： A coloured composition comprising: a) NIR scattering TiO2 particulate material with an average crystal size of greater than 0.40 μm and a particle size distribution such that 30% or more of the particles are less than 1 μm; b) one or more non-white colorant; wherein the particulate material and the non-white colorant are dispersed within a vehicle. This material with a large crystal size has unusually high reflection of NIR radiation and, simultaneously, noticeably diminished reflectance of visible light. Also disclosed is a coated particulate TiO2 material, wherein the material has an average crystal size of greater than 0.40 μm, and the coating comprises one or more oxide material; this provides low levels of photocatalytic activity that were previously unattainable. This coated TiO2 material may be provided in a composition.

    摘要翻译： 一种着色组合物，其包含：a）平均晶体尺寸大于0.40μm的粒径分布为30％以上的NIR散射TiO 2粒状材料， b）一种或多种非白色着色剂; 其中所述颗粒材料和所述非白色着色剂分散在车辆内。 这种具有大晶体尺寸的材料具有非常高的NIR辐射反射，并且同时可见光的反射率明显降低。 还公开了一种涂覆的颗粒状TiO 2材料，其中该材料具有大于0.40μm的平均晶体尺寸，并且该涂层包含一种或多种氧化物材料; 这提供了以前无法实现的低水平的光催化活性。 该涂覆的TiO 2材料可以以组合物形式提供。

    Methods for production of titanium oxide particles, and particles and preparations produced thereby
    10.
    发明授权
    Methods for production of titanium oxide particles, and particles and preparations produced thereby 有权
    生产氧化钛颗粒的方法，以及由此制备的颗粒和制剂

    公开(公告)号：US07763232B2

    公开(公告)日：2010-07-27

    申请号：US12096143

    申请日：2006-12-21

    申请人： Asher Vitner ,  Aharon Eyal

    发明人： Asher Vitner ,  Aharon Eyal

    IPC分类号： C01G23/047 ,  C01G23/053 ,  C01G23/04

    CPC分类号： C01G23/053 ,  B82Y30/00 ,  C01G23/0532 ,  C01G23/0536 ,  C01G23/08 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12

    摘要： The invention provides a method for the formation of small-size titanium oxide particles, comprising the steps of a) preparing a starting aqueous solution comprising at least one of titanic ions and complexes thereof, at a concentration of at least 0.1% w/w titanium; b) maintaining the solution at a temperature lower than 70° C. for a retention time in which hydrolysis takes place, the extent of the hydrolysis being sufficient to produce O.i mmol protons per mmol of titanium present in solution, wherein the time does not exceed 14 days, to form a system containing a retained solution; and c) adjusting the conditions in the system by at least one of the steps of: i) heating the retained solution to elevate the temperature thereof by at least 1° C.; ii) changing the pH of the retained solution by at least 0.1 units; and iii) diluting the retained solution by at least 20% whereby there are formed particles, wherein the majority of the particles formed are between about 2 nm and about 500 nm in size.

    摘要翻译： 本发明提供一种形成小尺寸氧化钛颗粒的方法，包括以下步骤：a）制备含有至少0.1％w / w钛的钛离子及其配合物中的至少一种的起始水溶液 ; b）将溶液保持在低于70℃的温度下进行水解的停留时间，水解程度足以产生溶解在溶液中的每毫摩尔钛的O 1 mmol质子，其中时间不超过 14天，形成含有保留溶液的体系; 以及c）通过以下步骤中的至少一个步骤来调节所述系统中的条件：i）加热所述保留的溶液以将其温度升高至少1℃; ii）将保留溶液的pH值改变至少0.1单位; 和iii）将保留的溶液稀释至少20％，由此形成颗粒，其中形成的大部分颗粒的尺寸在约2nm和约500nm之间。