Separation of molybdenum
    33.
    发明授权
    Separation of molybdenum 失效
    分离钼

    公开(公告)号:US5232559A

    公开(公告)日:1993-08-03

    申请号:US793902

    申请日:1991-11-18

    摘要: An organic solution of a soluble molybdenum compound is ammonated with ammonia, ammonium hydroxide and/or an ammonium salt in order to significantly reduce the electrical resistance of the solution and a direct electric current is passed therethrough in order to collect a significant amount of the molybdenum in solid form at the negative electrode. Preferably, an epoxidation reaction product formed by the molybdenum catalyzed reaction of propylene with tertiary butyl hydroperoxide to provide propylene oxide and tertiary butyl alcohol is separated by distillation into a propylene fraction, a propylene oxide fraction, a tertiary butyl alcohol fraction and a heavy liquid distillation fraction containing substantially all of the dissolved molybdenum catalyst, the heavy liquid distillation fraction is saturated with ammonia to precipitate the molybdenum therefrom, the precipitated molybdenum is removed from the ammonated heavy distillation fraction and a direct electric current is passed through the remaining liquid portion of the ammonated fraction in an electrolytic cell in order to collect a significant portion of the remaining molybdenum residually dissolved therein at the cathode.

    摘要翻译: 可溶性钼化合物的有机溶液用氨,氢氧化铵和/或铵盐氨化,以显着降低溶液的电阻,并且直流电流通过其中以收集显着量的钼 在固体形式的负极。 优选地,通过丙烯与叔丁基过氧化氢的钼催化反应形成环氧丙烷和叔丁醇形成的环氧化反应产物通过蒸馏分离成丙烯馏分,环氧丙烷馏分,叔丁醇馏分和重液体蒸馏 馏分含有基本上所有的溶解的钼催化剂,重液体蒸馏馏分用氨饱和,从中沉淀出钼,从氨化的重馏分中除去沉淀的钼,直流电流通过 在电解池中的氨化部分,以便在阴极收集残留的钼的很大部分。

    Sebum collection and monitoring means and method
    34.
    发明授权
    Sebum collection and monitoring means and method 失效
    皮脂采集和监测手段和方法

    公开(公告)号:US4532937A

    公开(公告)日:1985-08-06

    申请号:US555817

    申请日:1983-11-28

    申请人: David L. Miller

    发明人: David L. Miller

    摘要: Means for absorbing sebum screted by sebacious glands of a subject as well as providing semi-quantitative estimation of the rate of sebum production at various sites on the subject's skin and a record of excretion patterns on the skin, said means comprising a microporous hydrophobic polymeric film substrate coated on a major surface with a high molecular weight adhesive that is resistant to migration into the pores of the polymeric film. Said means may also be used to provide therapy by absorbing excess sebum or delivering medication to sites or abnormal sebum secretion. Method for ascertaining secretion patterns on the skin by applying to the skin for a preselected time a microporous, hydrophobic, polymeric film.

    摘要翻译: 用于吸收由受试者的海绵腺划伤的皮脂的方法,以及提供半定量估计受试者皮肤上各个部位的皮脂产生速率和皮肤上排泄模式的记录,所述方法包括微孔疏水性聚合物膜 基材涂覆在具有高分子量粘合剂的主表面上,其耐迁移到聚合物膜的孔中。 所述方法也可用于通过吸收多余皮脂或将药物递送至部位或异常皮脂分泌来提供治疗。 用于通过将微孔,疏水性聚合物膜施用于皮肤预选的时间来确定皮肤上的分泌模式的方法。