摘要:
A charged particle beam adjustment apparatus for tilting an electron beam by a tilt deflector is disclosed. The tilt angle adjustment of the electron beam and the distortion adjustment for correcting the image distortion generated when the electron beam is tilted are conducted on a specified. sample such as a pyramidal sample. The images before and after the tilting are acquired and processed to determine the tilt angle value and the distortion amount. The tilt angle adjustment and the adjustment for correction of the distortion are automated in accordance with a predetermined processing flow.
摘要:
A charged particle beam apparatus produces little reduction in resolution when the beam is inclined with respect to a sample. The trajectory of a primary beam 4 is deflected by a deflector or changed by a movable aperture such that the beam is incident on a plurality of lenses 6 and 7 off the axes thereof. A means is provided to control the off-axis trajectory of the beam such than an aberration produced by the objective lens 7 when the beam is inclined can be canceled by an aberration produced by the other lens 6.
摘要:
A cyclododecanone compound is continuously produced by an isomerization reaction of a corresponding epoxycyclododecane compound in the presence of a catalyst including lithium bromide and/or lithium iodide, the isomerization reaction being carried out by passing a reaction mixture containing the epoxycyclododecane compound and the catalyst through a continuous reaction apparatus including at least one tubular reactor preferably at a temperature of 100 to 350° C.
摘要:
A cyclododecanone compound is produced in a high reaction rate, with a high conversion of the starting compound, and with a high selectivity to and a high yield of the target compound by isomerizing an epoxycyclododecane compound in the presence of a catalyst comprising lithium bromide and/or lithium iodide, without using a solvent or in a non-polar solvent, in an inert gas atmosphere, while substantially no polymeric compounds having a high boiling temperature is produced.
摘要:
In tandem copy, an external controller assigns a minimum print copy number to a slave image forming apparatus from a total print copy number. The external controller assigns a remainder print copy number, which is obtained by subtracting the minimum print copy number assigned to the slave image forming apparatus from the total print copy number, to a master image forming apparatus, and instructs starting of printing out. When detecting that printing of all assigned copy number is completed in the slave and a new interrupt print job (other job print request) has come in, the external controller starts a new print job in the slave. When detecting that the interrupt printing in the slave is completed, the external controller suspends printing in the master and inquires of the master about a non-output copy number. Similarly with the print start time, the external controller redistributes a minimum print copy number to the slave and also redistributes a remainder of the non-output copy number, from which the minimum print copy number redistributed to the slave has been subtracted, to the master. The external controller thus resumes the tandem copy.
摘要:
A catalyst composed of an organic phosphorus compound having a trivalent or pentavalent phosphorus atom and at least one carbon-phosphorus bonding or a combination of the organic phosphorus compound and a halogen atom-containing compound is effective for decarbonylation, that is, for releasing carbon monoxide from a compound containing a moiety of --CO--CO--O-- in its molecular structure.
摘要:
A diaryl carbonate with a high degree of purity is produced at a high yield by (A) subjecting (a) a diaryl oxalate and a phenol compound or (b) an alkylaryl oxalate to transesterification reaction in one or two stages in the presence of a catalyst to prepare a diaryl oxalate, while removing a by-product from the reaction system; (B) collecting the diaryl oxalate from the resultant reaction product mixture of the step (A); (C) subjecting the diaryl oxalate to a decarbonylation reaction, preferably in the presence of a phosphorous compound-containing catalyst, to convert the diaryl oxalate to a corresponding diaryl carbonate, while removing a reaction by-product comprising carbon monoxide from the reaction system; and (D) collecting the diaryl carbonate from the reaction product mixture of the step (C).
摘要:
An improved process for preparing a diaryl carbonate from a diaryl oxalate in a liquid phase by decarbonylation utilizes a reaction vessel composed of two or more reaction chambers which are connected in series. The process is composed of the steps of continuously introducing the diaryl oxalate and an organic phosphorus compound having a trivalent or pentavalent phosphorus atom and at least one carbon-phosphorus bonding into the first chamber and continuously recovering a reaction mixture mainly containing the diaryl carbonate from the last chamber under the condition that a mixture of the diaryl oxalate and the organic phosphorus compound is heated in the reaction chambers, while discharging carbon monoxide released from the mixture.
摘要:
An information medium storage and management system includes storage compartments for storing a plurality of information media; a plurality of recording/reproducing apparatus each capable of accessing each of a plurality of information media, each capable of recording at least one file; handling apparatus for mounting a mount information medium on a mount recording/reproducing apparatus and demounting a demount information medium from a demount recording/reproducing apparatus; and a controller for controlling the handling apparatus to select as the mount information medium one of the plurality of information media in accordance with the use history data of each information medium, to select as the mount recording/reproducing apparatus one of unoccupied recording/reproducing apparatus of the plurality of recording/reproducing apparatus, and to cause the mount information medium to use the mount recording/reproducing apparatus for a predetermined time period.
摘要:
When the mount and demount operation of information media are achieved between an information medium storage shelf and a plurality of recording/playback apparatuses by use of a plurality of handling devices, in order to execute the operations in a concurrent fashion without causing an interference between the handling devices for an increased operation efficiency, the area of the storage shelf and at least one of the recording/playback apparatuses are respectively subdivided into a plurality of subareas so as to process the obtained subareas by the plurality devices respectively associated therewith.