Abstract:
Production process of chlorine dioxide stable solution that occurs in two phases of pH control, the first phase being an acid one and the second phase a basic one, with two distinct reactors, one for generation of chlorine dioxide and the other for stabilization, the first one being operated under vacuum and the second one under atmospheric pressure. The resulting solution then contains up to 6% chlorine dioxide that becomes active when pH is reduced to a range of 6.5 to 7.5 at the application moment.
Abstract:
An apparatus is provided to generate a gas by mixing chemicals with water. Typically, the production of gas, particularly oxygen, by combining water with powders and other dry chemicals has not been widely employed. There have existed a number of preexisting barriers such as undesirable flow rates and yields. However, by utilizing multiple reaction chambers the flow rates and yields can be more precisely tailored for a variety of situations that may call for particular flow rates and yields. Additionally, the use of the dry chemicals would allow for a long self-life allowing the apparatus to be particularly useful in emergency situations.
Abstract:
A chemical generator having inlets for receiving multiple reactant and water streams; a dilution chamber; a reaction chamber operably connected to the inlets and to the dilution chamber; an eductor operably receiving the water stream from the one of the inlets and communicating with the reaction chamber for drawing first and second reactant streams into the reaction chamber for mixing. Float control valves interrupt the water stream to the eductor when desired amounts of the first and second reactant streams have entered the reaction chamber, the eductor drawing the activated solution of first and second reactant streams from the reaction chamber into the dilution chamber. The float control valves limit the residence time of the first and second reactants in the reaction chamber and selectively interrupt flow of the water stream into the dilution chamber.
Abstract:
A dosing device for liquid fuels, in particular for input into a chemical reformer in order to recover hydrogen or into a post-combustion device in order to generate heat, comprises at least one metering device for metering fuel into a metering conduit and a nozzle body, adjoining the metering conduit, having spray discharge openings which open into a metering chamber, the dosing device comprising at least one heating element made up of a wire braid networked in mesh fashion and/or a tubular hollow element, with which heat can be delivered to the fuel.
Abstract:
A system and method for providing process chemicals. The system includes a housing comprising a functional component positioned in a first compartment, a control module positioned in a second compartment and at least one connecting line positioned in a third compartment. At least one compartment is positioned in a defined location in the housing. Modules may be removable received in their respective compartments.
Abstract:
A controlled-flow microwave instrument for chemical synthesis that includes heterogeneous or highly viscous materials includes a fluid reservoir for supplying or receiving fluids, a fluid pump in fluid communication with the reservoir for pumping fluids to or from the reservoir, a microwave transparent reaction vessel in fluid communication with the pump for supplying or receiving fluids to or from the pump and the reservoir, a pressure sensor in fluid communication with the reservoir and the vessel for measuring the pressure of fluids in the instrument at the sensor, and a processor in signal communication with the pressure sensor and the pump for controlling the pump and the flow of fluids in the instrument based at least in part on the pressure measured at the sensor.
Abstract:
A controlled-flow microwave instrument for chemical synthesis using heterogeneous or highly viscous starting materials includes a microwave source for generating electromagnetic radiation in the microwave frequencies, a microwave cavity in wave communication with the source for exposing compositions placed therein to microwave radiation, a microwave-transparent pressure resistant reaction vessel in the cavity, a source reservoir for starting materials and related compositions, a pump in communication with the source reservoir for pumping heterogeneous or highly viscous materials from the source reservoir to the reaction vessel, and a pressure-resistant valve between the pump and the reaction vessel for isolating the reaction vessel from the pump and the source reservoir during application of microwave energy to compositions in the vessel and from any resulting high pressures generated therein.
Abstract:
A controlled-flow microwave instrument is disclosed for chemical synthesis that includes heterogeneous or highly viscous materials. The instrument includes a fluid reservoir for supplying or receiving fluids, a fluid pump in fluid communication with the reservoir for pumping fluids to or from the reservoir, a microwave transparent reaction vessel in fluid communication with the pump for supplying or receiving fluids to or from the pump and the reservoir, a pressure sensor in fluid communication with the reservoir and the vessel for measuring the pressure of fluids in the instrument at the sensor, and a processor in signal communication with the pressure sensor and the pump for controlling the pump and the flow of fluids in the instrument based at least in part on the pressure measured at the sensor. The instrument also includes a magnetic stirrer bar inside the vessel for agitating reactants in the vessel during exposure to microwave radiation, a first rotating magnet positioned external to and adjacent the cavity to minimize any interaction between the magnetic field of the magnet and microwave propagation in the cavity, and a second rotating magnet inside the cavity for being driven by the first rotating magnet and for driving the rotation of the stirrer bar in the reaction vessel.
Abstract:
A gas supply system for pulse-wise feeding a reactant gas to a reactor, the gas supply system comprising: a first valve being a four-port diaphragm valve; a second valve which in an open state brings the first port into fluid communication with an exhaust and in a closed state closes off said fluid communication; wherein the gas supply system provides a reactant flow state in which the first valve is in an open state and the second valve is in a closed state, and wherein the gas supply system provides a purge state in which the first valve is closed and the second valve is in a open state. Also disclosed are a method of switching a process fluid by operating a gas supply system according to the invention and a valve assembly for use in such a gas supply system.
Abstract:
The production and selection of precursor mixtures used to produce fine powders and methods for making fine powders using the selected precursor. The precursor mixture comprises at least one metal containing precursor, the metal containing precursor has an average molecular weight of less than 2000 grams per unit mol of the metal, the metal containing precursor has a normal boiling point greater than 350K, and the viscosity of the precursor mixture is between 0.1 to 250 cP. The precursor mixture is processed under conditions that produce a fine powder from the precursor mixture. Fine powders produced are of size less than 100 microns, preferably less than 10 micron, more preferably less than 1 micron, and most preferably less than 100 nanometers.