Method and Atmosphere for Extending Belt Life in Sintering Furnace
    401.
    发明申请
    Method and Atmosphere for Extending Belt Life in Sintering Furnace 有权
    烧结炉延长皮带寿命的方法和气氛

    公开(公告)号:US20110318216A1

    公开(公告)日:2011-12-29

    申请号:US12966440

    申请日:2010-12-13

    Abstract: Disclosed herein is a method and gas atmosphere for a metal component in a continuous furnace. In one embodiment, the method and gas atmosphere comprises the use of an effective amount, or about 1 to about 10 percent volume of endo-gas, into an atmosphere comprising nitrogen and hydrogen. In another embodiment, there is provided a method sintering metal components in a furnace at a one or more operating temperatures comprising: providing a furnace comprising a belt comprising a wire mesh material wherein the metal components are supported thereupon; and sintering the components in the furnace in an atmosphere comprising nitrogen, hydrogen, and effective amount of endothermic gas at the one or more operating temperatures ranging from about 1800° F. to about 2200° F. wherein the amount of endothermic gas in the atmosphere is such that it is oxidizing to the wire mesh material and reducing to the metal components.

    Abstract translation: 本文公开了连续炉中的金属成分的方法和气体气氛。 在一个实施方案中,所述方法和气体气氛包括使用有效量(或约1至约10体积%的内含气体)到包含氮气和氢气的气氛中。 在另一个实施方案中,提供了一种在一个或多个操作温度下在炉中烧结金属组分的方法,包括:提供包括包含金属丝网材料的带的炉子,其中金属组分被支撑在其上; 以及在约1800°F至约2200°F的一个或多个操作温度下,在包括氮气,氢气和有效量的吸热气体的气氛中烧结炉中的组分。其中吸入气体在大气中的量 使得其对金属丝网材料氧化并且还原成金属成分。

    Soft magnetic composite materials
    402.
    发明授权
    Soft magnetic composite materials 有权
    软磁复合材料

    公开(公告)号:US08075710B2

    公开(公告)日:2011-12-13

    申请号:US11921514

    申请日:2006-06-15

    Abstract: A process for the manufacture of soft magnetic composite components is provided including the steps of: die compacting a powder composition including a mixture of soft magnetic, iron or iron-based powder, core particles of which are surrounded by an electrically insulating, inorganic coating, and an organic lubricant in an amount of 0.05 to 1.5% by weight of the composition, the organic lubricant being free from metal and having a temperature of vaporization less than the decomposition temperature of the coating; ejecting the compacted body from the die; heating the compacted body in an inert atmosphere to a temperature above the vaporization temperature of the lubricant and below the decomposition temperature of the inorganic coating for removing the lubricant from the compacted body, and subjecting the body obtained after heating the compacted body in an inert atmosphere to heat treatment at a temperature between 300 and 600 in water vapor.

    Abstract translation: 提供了一种用于制造软磁性复合材料部件的方法,包括以下步骤:将包含软磁性,铁或铁基粉末的混合物的粉末组合物模压成型,其核心颗粒被电绝缘的无机涂层包围, 和组合物的0.05〜1.5重量%的有机润滑剂,有机润滑剂不含金属,其蒸发温度小于涂料的分解温度; 将压实体从模具中弹出; 将压实体在惰性气氛中加热至高于润滑剂蒸发温度的温度,并低于无机涂层的分解温度,以从压实体中除去润滑剂,并将经加压的本体在惰性气氛 在300〜600℃的水蒸气中进行热处理。

    METHOD FOR PRODUCING DUST CORE
    404.
    发明申请
    METHOD FOR PRODUCING DUST CORE 有权
    生产粉芯的方法

    公开(公告)号:US20110274576A1

    公开(公告)日:2011-11-10

    申请号:US13188638

    申请日:2011-07-22

    Abstract: An object of the present invention is to provide a method for producing a dust core wherein generation of iron oxide at grain boundaries in the dust core is unlikely to take place upon annealing of the dust core subjected to compaction, thus allowing excellent electromagnetic characteristics to be realized. Also, the following is provided: a method for producing a dust core, which comprises: a step of molding a magnetic powder comprising a powder for a dust core formed with an iron-based magnetic powder coated with a silicone resin into a dust core via compaction; and a step of annealing the dust core via heating so as to cause the silicone resin contained in the dust core to be partially formed into a silicate compound, wherein annealing of the dust core is carried out at a dew point of an inert gas of −40° C. or lower in an inert gas atmosphere in the annealing step.

    Abstract translation: 本发明的目的在于提供一种粉尘芯的制造方法,其特征在于,在经过压实的压粉芯退火后,在粉尘芯中产生铁氧化物不容易发生,从而使电磁特性优异 实现了 另外,提供以下内容:一种压粉芯的制造方法,其特征在于,包括以下步骤:将形成有由硅酮树脂涂覆的铁基磁性粉末形成的粉尘的粉末的磁性粉末成型为粉尘芯, 压实 以及通过加热对所述防尘芯体进行退火以使所述防尘芯体中包含的硅酮树脂部分地形成为硅酸盐化合物的步骤,其中所述防尘芯的退火在所述惰性气体的露点处进行, 在退火步骤中的惰性气体气氛中为40℃以下。

    Method for producing soft magnetic powdered core
    405.
    发明授权
    Method for producing soft magnetic powdered core 有权
    软磁粉芯的生产方法

    公开(公告)号:US08029626B2

    公开(公告)日:2011-10-04

    申请号:US12076336

    申请日:2008-03-17

    Abstract: A method for producing a soft magnetic powdered core comprises a mixing step for forming a raw powder by adding a thermoplastic resin powder to a soft magnetic powder and mixing them, a compacting step for forming a compact by compacting the raw powder into a predetermined shape, a melting and setting step for the resin in which the resin of the compact is melted by heating to at least the melting point of the thermoplastic resin and the melted resin is set by cooling to a room temperature, and a crystallizing step for the resin in which the set resin is heated to not less than the exothermic onset temperature and not more than the endothermic onset temperature, which are measured by DSC analysis of the thermoplastic resin, and is cooled to a room temperature.

    Abstract translation: 一种软磁性粉末芯的制造方法,其特征在于,包括:将热塑性树脂粉末添加到软磁性粉末并混合而形成原料粉末的混合工序;将所述原料粉末压制为规定形状的压实成形工序; 将通过加热到至少热塑性树脂和熔融树脂的熔点而使压块的树脂熔化的树脂的熔融和凝固步骤通过冷却至室温来设定,并且树脂的结晶步骤 将该树脂加热至不低于通过热塑性树脂的DSC分析测定的放热起始温度和不高于吸热开始温度,并冷却至室温。

    Particulate powder of silver and method of manufacturing same
    410.
    发明授权
    Particulate powder of silver and method of manufacturing same 有权
    银颗粒粉及其制造方法

    公开(公告)号:US07776442B2

    公开(公告)日:2010-08-17

    申请号:US11883344

    申请日:2006-02-01

    Applicant: Kimitaka Sato

    Inventor: Kimitaka Sato

    Abstract: A nanoparticle powder of silver has an average particle diameter measured by TEM observation (DTEM) of 30 nm or less, an aspect ratio of less than 1.5, an X-ray crystallite size (Dx) of 30 nm or less, a degree of single crystal grain {(DTEM)/(Dx)} of 5.0 or less, and a CV value {100×standard deviation (σ)/number average diameter (DTEM)} of less than 40%. The nanoparticle powder of silver has adhered to the particle surface thereof an organic protective agent having a molecular weight of 100 to 400. The nanoparticle powder is obtained by subjecting a silver salt to reduction treatment at a temperature of 85 to 150° C. in an alcohol having a boiling point of 85 to 150° C. and in the co-presence of an organic protective agent.

    Abstract translation: 银的纳米颗粒粉末通过TEM观察(DTEM)测量的平均粒径为30nm以下,纵横比小于1.5,X射线微晶尺寸(Dx)为30nm以下,单一度 晶粒{(DTEM)/(Dx)}为5.0以下,CV值{100×标准偏差(&Sgr)/数均粒径(DTEM)}小于40%。 银纳米颗粒粉末的粒子表面附着有分子量为100〜400的有机保护剂。通过在85〜150℃的温度下对银盐进行还原处理,得到纳米粒子粉末 醇的沸点为85〜150℃,有机保护剂共存。

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