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    Process of producing cyclohexylbenzene
    44.
    发明授权
    Process of producing cyclohexylbenzene 有权
    生产环己基苯的方法

    公开(公告)号：US09382172B2

    公开(公告)日：2016-07-05

    申请号：US14375996

    申请日：2012-12-05

    Applicant: ExxonMobil Chemical Patents Inc.

    Inventor： Christopher L. Becker ,  James R. Lattner ,  Keith H. Kuechler ,  Hari Nair

    IPC: C07C2/74 ,  C07C2/54 ,  C07C7/04 ,  C07C5/367

    CPC classification number: C07C2/74 ,  C07C5/367 ,  C07C2529/08 ,  C07C2529/18 ,  C07C2529/70 ,  C07C2529/89 ,  C07C13/28 ,  C07C15/04

    Abstract: In a process for producing cyclohexylbenzene, benzene is contacted with hydrogen in the presence of a hydroalkylation catalyst under hydroalkylation conditions effective to form a first effluent stream comprising cyclohexylbenzene, cyclohexane, and benzene. At least a portion of the cyclohexane from the first effluent stream is then contacted with hydrogen in the presence of a dehydrogenation catalyst under dehydrogenation conditions effective to convert at least some of the cyclohexane into benzene contained in a second effluent stream. At least some of the hydrogen is supplied to the process so as to contact the dehydrogenation zone (e.g., the dehydrogenation catalyst) before contacting the hydroalkylation catalyst.

    Abstract translation: 在生产环己基苯的方法中，苯在氢化烷基化催化剂存在下，在有效形成包含环己基苯，环己烷和苯的第一流出物流的加氢烷基化条件下与氢气接触。 然后，在脱氢催化剂存在下，将有效将至少一些环己烷转化为第二流出物流中所含的苯的脱氢催化剂存在下，将来自第一流出物流的至少一部分环己烷与氢气接触。 在与加氢烷基化催化剂接触之前，将至少一些氢气供给到该方法中以与脱氢区（例如，脱氢催化剂）接触。

    Process for Producing Phenol and/or Cyclohexanone from Cyclohexylbenzene
    45.
    发明申请
    Process for Producing Phenol and/or Cyclohexanone from Cyclohexylbenzene 有权
    从环己基苯生产苯酚和/或环己酮的方法

    公开(公告)号：US20150218075A1

    公开(公告)日：2015-08-06

    申请号：US14422444

    申请日：2013-09-12

    Applicant: ExxonMobil Chemical Patents Inc.

    Inventor： Keith H. Kuechler ,  Jihad M. Dakka ,  James R. Lattner ,  Christopher L. Becker ,  Edmund J. Mozeleski

    IPC: C07C45/53 ,  C07C1/24 ,  C07C37/08 ,  C07C407/00 ,  C07C29/60

    CPC classification number: C07C45/53 ,  C07C1/24 ,  C07C2/66 ,  C07C2/74 ,  C07C5/03 ,  C07C29/60 ,  C07C29/80 ,  C07C37/08 ,  C07C407/00 ,  C07C2529/70 ,  C07C2601/14 ,  C07C409/14 ,  C07C39/04 ,  C07C49/403 ,  C07C35/21 ,  C07C13/28

    Abstract: In a process for producing phenol and/or cyclohexanone, cyclohexylbenzene is contacted with an oxygen-containing gas to produce an oxidation effluent containing cyclohexylbenzene hydroperoxide. At least a portion of the cyclohexylbenzene hydroperoxide is then contacted with a cleavage catalyst to produce a cleavage effluent containing phenol and cyclohexanone and by-products including phenylcyclohexanol. The cleavage effluent or a neutralized product thereof also comprises at least one compound comprising an atom not being carbon, hydrogen or oxygen, which is separated from the cleavage effluent and/or the neutralized product thereof to leave a cleavage fraction lean in the compound comprising an atom not being carbon, hydrogen or oxygen and containing at least a portion of the phenylcyclohexanol. At least a portion of the phenylcyclohexanol is then contacted with a dehydration catalyst comprising a molecular sieve of the MCM-22 type to convert at least a portion of the phenylcyclohexanol to phenyl cyclohexene.

    Abstract translation: 在生产苯酚和/或环己酮的方法中，使环己基苯与含氧气体接触以产生含有环己基苯氢过氧化物的氧化流出物。 然后将至少一部分环己基苯氢过氧化物与裂解催化剂接触，以产生包含苯酚和环己酮的裂解流出物以及包括苯基环己醇在内的副产物。 裂解流出物或其中和产物还包含至少一种包含不是碳，氢或氧的原子的化合物，其从裂解流出物和/或其中和产物中分离出来，以在含有 原子不是碳，氢或氧并且含有至少一部分苯基环己醇。 然后至少一部分苯基环己醇与包含MCM-22型分子筛的脱水催化剂接触，以将至少一部分苯基环己醇转化成苯基环己烯。

    Process for Producing Phenol and Cyclohexanone
    46.
    发明申请
    Process for Producing Phenol and Cyclohexanone 有权
    酚和环己酮的制备方法

    公开(公告)号：US20150094495A1

    公开(公告)日：2015-04-02

    申请号：US14394455

    申请日：2013-04-09

    Applicant: ExxonMobil Chemical Patents Inc.

    Inventor： Keith H. Kuechler ,  Francisco M. Benitez ,  Krystle J. Chavez ,  Christopher L. Becker ,  John L. Heidman

    IPC: C07C49/403 ,  C07C37/58 ,  B01D3/40 ,  C07C37/80

    CPC classification number: C07C49/403 ,  B01D3/40 ,  C07C37/08 ,  C07C37/58 ,  C07C37/80 ,  C07C45/53 ,  C07C45/83 ,  C07C2601/14 ,  C07C39/04

    Abstract: In a process for separating a mixture comprising cyclohexanone and phenol, at least a portion of the mixture is distilled in the presence of a solvent including at least two alcoholic hydroxyl groups attached to non-adjacent saturated carbon atoms, water, and in the presence or absence of a hemiketal defined by the formula (I) or the formula (II): wherein R1, the same or different at each occurrence, is independently an alkylene group having from 2 to 10 carbon atoms, R2 is an alkylene group having from 4 to 10 carbon atoms and/or R3 is hydrogen or the following group: and in the presence or absence of an enol-ether derived from the hemiketal defined by the formula (I) or the formula (II), wherein the total concentration of the hemiketal and enol-ether, expressed in term of weight percentage of the total weight of the feed to the distilling step, is at most 0.01%.

    Abstract translation: 在分离包含环己酮和苯酚的混合物的方法中，至少一部分混合物在溶剂存在下蒸馏，所述溶剂包括至少两个连接到不相邻饱和碳原子上的醇羟基，水和存在或不存在 不存在由式（I）或式（II）定义的半缩酮化合物：其中每次出现相同或不同的R 1独立地为具有2至10个碳原子的亚烷基，R 2为具有4 至10个碳原子和/或R 3为氢或以下基团：并且在存在或不存在衍生自由式（I）或式（II）定义的半缩酮的烯醇 - 醚的情况下，其中， 半缩酮和烯醇醚，以蒸馏步骤的进料总重量的重量百分比表示，至多为0.01％。

    Process for Producing Phenol
    48.
    发明申请
    Process for Producing Phenol 有权
    生产苯酚的方法

    公开(公告)号：US20150018583A1

    公开(公告)日：2015-01-15

    申请号：US14375983

    申请日：2012-12-04

    Applicant: ExxonMobil Chemical Patents Inc.

    Inventor： Christopher L. Becker ,  James R. Lattner ,  Keith H. Kuechler ,  Hari Nair

    IPC: C07C37/08 ,  C07C2/66 ,  C07C407/00

    CPC classification number: C07C37/08 ,  C07C2/66 ,  C07C2/74 ,  C07C5/03 ,  C07C7/11 ,  C07C37/80 ,  C07C45/53 ,  C07C407/00 ,  C07C2601/14 ,  C07C409/14 ,  C07C39/04 ,  C07C49/403 ,  C07C13/28

    Abstract: In a process for producing phenol, benzene is reacted with a source of hydrogen containing methane in the presence of a hydroalkylation catalyst under conditions effective to produce a hydroalkylation reaction effluent comprising cyclohexylbenzene, benzene, hydrogen, and methane. A first stream comprising hydrogen, methane, and benzene is removed from the hydroalkylation reaction effluent and the first stream is washed with a second stream containing cyclohexylbenzene to produce a benzene-depleted hydrogen stream containing hydrogen and methane and a wash stream containing cyclohexylbenzene and benzene.

    Abstract translation: 在生产苯酚的方法中，在有效产生包含环己基苯，苯，氢和甲烷的加氢烷基化反应流出物的条件下，在加氢烷基化催化剂存在下，使苯与含氢甲烷源反应。 从加氢烷基化反应流出物中除去包含氢气，甲烷和苯的第一流，并将第一流用含有环己基苯的第二料流洗涤以产生含有氢和甲烷的贫苯氢气流，以及含有环己基苯和苯的洗涤流。

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