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55 条记录 (耗时 0.013 秒)

    Manufacturing method of nitrile compound
    43.
    发明授权
    Manufacturing method of nitrile compound 有权

    公开(公告)号：US11795137B2

    公开(公告)日：2023-10-24

    申请号：US17431284

    申请日：2020-03-25

    申请人： Mitsubishi Gas Chemical Company, Inc.

    发明人： Masayoshi Ueno

    IPC分类号： C07C253/28

    CPC分类号： C07C253/28

    摘要： A manufacturing method of a nitrile compound comprising a first step of introducing a raw material gas containing a cyclic compound having an organic substituent, ammonia, and air into a reactor and reacting the raw material gas in the presence of a catalyst to generate the nitrile compound, a second step of discharging a reacted gas from the reactor and separating the nitrile compound from the reacted gas, and a third step of collecting mist from a first residual gas obtained by separating the nitrile compound from the reacted gas to remove water and ammonium carbonate in the first residual gas.

    Method for producing alkyl and/or cycloalkyl-substituted cyclic nitrile
    45.
    发明申请
    Method for producing alkyl and/or cycloalkyl-substituted cyclic nitrile 有权
    制备烷基和/或环烷基取代的环腈的方法

    公开(公告)号：US20050124823A1

    公开(公告)日：2005-06-09

    申请号：US10951592

    申请日：2004-09-29

    申请人： Kentaro Kataoka ,  Yoshikazu Shima ,  Kenji Inamasa

    发明人： Kentaro Kataoka ,  Yoshikazu Shima ,  Kenji Inamasa

    IPC分类号： C07B43/08 ,  C07C253/28 ,  C07C255/50 ,  C07C253/00

    CPC分类号： C07C253/28 ,  C07C255/50

    摘要： In the production method of the invention, a cyclic aldehyde having an alkyl group and/or a cycloalkyl group directly bonded to a skeletal ring and a formyl group directly bonded to the skeletal ring is brought into contact with ammonia and oxygen in vapor phase in the presence of a catalyst. As a result thereof, the formyl group is selectively ammoxidized into a cyano group to convert the cyclic aldehyde into a corresponding cyclic nitrile. The method enables a long-term, high-yield production of the cyclic nitrile using a reduced amount of ammonia.

    摘要翻译： 在本发明的制造方法中，将与骨架环直接键合的具有烷基和/或环烷基的环醛和与骨架环直接结合的甲酰基与气相中的氨和氧接触， 存在催化剂。 作为其结果，甲酰基被选择性氨氧化成氰基以将环醛转化为相应的环腈。 该方法能够使用氨的量减少量的长期高产率的环腈。

    Preparation of vanadium antimonate based catalysts using SnO.sub.2 .multidot.xH.sub.2 O
    47.
    发明授权
    Preparation of vanadium antimonate based catalysts using SnO.sub.2 .multidot.xH.sub.2 O 失效
    使用SnO2xxH2O制备锑酸锑基催化剂

    公开(公告)号：US5972833A

    公开(公告)日：1999-10-26

    申请号：US151463

    申请日：1998-11-09

    申请人： James Frank Brazdil, Jr. ,  Joseph Peter Bartek

    发明人： James Frank Brazdil, Jr. ,  Joseph Peter Bartek

    IPC分类号： B01J23/20 ,  B01J23/14 ,  B01J23/16 ,  B01J23/18 ,  B01J23/22 ,  B01J23/24 ,  B01J23/26 ,  B01J23/28 ,  B01J23/30 ,  B01J23/34 ,  B01J23/847 ,  B01J27/057 ,  B01J37/04 ,  C07B61/00 ,  C07C51/265 ,  C07C253/00 ,  C07C253/24 ,  C07C253/26 ,  C07C253/28 ,  C07C255/08 ,  C07C255/51 ,  C07D213/84 ,  B01J23/00 ,  B01J21/08

    CPC分类号： C07D213/84 ,  B01J23/18 ,  B01J23/22 ,  C07C253/24 ,  C07C253/26 ,  Y02P20/52

    摘要： A method of preparing a catalyst having the elements and the proportions indicated by the following empirical formula:VSb.sub.m A.sub.a D.sub.d O.sub.xwhereA is one or more Ti, Sn, where Sn is always presentD is one or more Li, Mg, Ca, Sr, Ba, Co, Fe, Cr, Ga, Ni, Zn, Ge, Nb, Zr, Mo, W, Cu, Te, Ta, Se, Bi, Ce, In, As, B, Al and Mn whereinm is 0.5 to 10a is greater than zero to 10d is zero to 10x is determined by the oxidation state of the cations present,comprising making an aqueous slurry of a mixture of source batch materials comprising compounds of said elements to be included in the final catalyst, followed by drying and heat calcining the mixture to an active catalyst, wherein the source batch material for the tin is a solution which comprises SnO.sub.2.xH.sub.2 O wherein x.gtoreq.0 dispersed in tetraalkyl ammonium hydroxide wherein the tetraalkyl ammonium hydroxide is defined by the following formula:C.sub.n H.sub.2n+1 NOHwherein 5.gtoreq.n.gtoreq.1,drying said slurry and calcining the mixture to an upper calcination temperature of at least 500.degree. C.

    摘要翻译： 制备具有以下经验式所示元素和比例的催化剂的方法：VSbmAaDdOx其中A是一种或多种Ti，Sn，其中Sn总是存在D是一种或多种Li，Mg，Ca，Sr，Ba，Co ，Fe，Cr，Ga，Ni，Zn，Ge，Nb，Zr，Mo，W，Cu，Te，Ta，Se，Bi，Ce，In，As，B，Al和Mn，其中m为0.5〜 大于0至10天是零至10倍，由存在的阳离子的氧化态确定，包括制备包含待包含在最终催化剂中的所述元素化合物的源批料的混合物的含水浆料，然后干燥 以及将所述混合物煅烧为活性催化剂，其中所述锡的所述源批料为包含SnO 2·xH 2 O的溶液，其中x 2 = 0分散在四烷基氢氧化铵中，其中所述四烷基氢氧化铵由下式定义：C n H 2n + 1NOH其中5> / = n> / = 1，干燥所述浆料并将混合物煅烧至上煅烧温度o f至少500℃

    Method for preparing acrylonitrile
    48.
    发明授权
    Method for preparing acrylonitrile 失效
    制备丙烯腈的方法

    公开(公告)号：US5907053A

    公开(公告)日：1999-05-25

    申请号：US894136

    申请日：1997-07-30

    申请人： Katsuhiko Sakai

    发明人： Katsuhiko Sakai

    IPC分类号： C07C253/24 ,  C07C253/26 ,  C07C253/28 ,  C07C255/08

    CPC分类号： C07C253/28 ,  C07C253/24 ,  C07C253/26

    摘要： This invention relates to a method for preparing acrylonitrile by ammoxydation using a multi-story quenching tower. The method comprises the steps of supplying the reacted gas into the first quenching chamber of the multi-story quenching tower, said first quenching chamber has a water supply pipe equipped with spray nozzles at a two-dimensional density of more than 2 nozzles/m.sup.2 for the sectional area of the multi-story quenching tower and contacting the reacted gas with 5 T or more of water per 1 T of the reacted gas fed from the nozzles.

    摘要翻译： PCT No.PCT / JP96 / 00133 Sec。 371日期1997年7月30日 102（e）日期1997年7月30日PCT提交1996年1月25日PCT公布。 第WO96 / 23765号公报 日期：1996年8月8日本发明涉及使用多层骤冷塔通过氨氧化制备丙烯腈的方法。 该方法包括以下步骤：将反应的气体供应到多层骤冷塔的第一淬火室中，所述第一淬火室具有供水管，该供水管具有二维密度大于2个喷嘴/ m2的喷嘴，用于 多层淬火塔的截面积，并使反应气体与每喷嘴喷射的每1升反应气体中的5T或更多的水接触。

    Preparation of vanadium antimonate based catalysts using SnO.sub.2 .multidot.xH.sub.2 O
    50.
    发明授权
    Preparation of vanadium antimonate based catalysts using SnO.sub.2 .multidot.xH.sub.2 O 失效
    使用SnO2xxH2O制备锑酸锑基催化剂

    公开(公告)号：US5854172A

    公开(公告)日：1998-12-29

    申请号：US785543

    申请日：1997-01-17

    申请人： James Frank Brazdil, Jr. ,  Joseph Peter Bartek

    发明人： James Frank Brazdil, Jr. ,  Joseph Peter Bartek

    IPC分类号： B01J23/20 ,  B01J23/14 ,  B01J23/16 ,  B01J23/18 ,  B01J23/22 ,  B01J23/24 ,  B01J23/26 ,  B01J23/28 ,  B01J23/30 ,  B01J23/34 ,  B01J23/847 ,  B01J27/057 ,  B01J37/04 ,  C07B61/00 ,  C07C51/265 ,  C07C253/00 ,  C07C253/24 ,  C07C253/26 ,  C07C253/28 ,  C07C255/08 ,  C07C255/51 ,  C07D213/84 ,  B01J23/00 ,  B01J21/08

    CPC分类号： C07D213/84 ,  B01J23/18 ,  B01J23/22 ,  C07C253/24 ,  C07C253/26 ,  Y02P20/52

    摘要： A method of preparing a catalyst having the elements and the proportions indicated by the following empirical formula: VSb.sub.m A.sub.a D.sub.d O.sub.x where A is one or more Ti, Sn, where Sn is always present D is one or more Li, Mg, Ca, Sr, Ba, Co, Fe, Cr, Ga, Ni, Zn, Ge, Nb, Zr, Mo, W, Cu, Te, Ta, Se, Bi, Ce, In, As, B, Al and Mn wherein m is 0.5 to 10 a is greater than zero to 10 d is zero to 10 x is determined by the oxidation state of the cations present, comprising making an aqueous slurry of a mixture of source batch materials comprising compounds of said elements to be included in the final catalyst, followed by drying and heat calcining the mixture to an active catalyst, wherein the source batch material for the tin is a solution which comprises SnO.sub.2.xH.sub.2 O wherein x.gtoreq.0 dispersed in tetraalkyl ammonium hydroxide wherein the tetraalkyl ammonium hydroxide is defined by the following formula: C.sub.n H.sub.2n+1 NOH wherein 5.gtoreq.n.gtoreq.1, drying said slurry and calcining the mixture to an upper calcination temperature of at least 500.degree. C.

    摘要翻译： 制备具有以下经验式所示元素和比例的催化剂的方法：VSbmAaDdOx其中A是一种或多种Ti，Sn，其中Sn总是存在D是一种或多种Li，Mg，Ca，Sr，Ba，Co ，Fe，Cr，Ga，Ni，Zn，Ge，Nb，Zr，Mo，W，Cu，Te，Ta，Se，Bi，Ce，In，As，B，Al和Mn，其中m为0.5〜 大于0至10天是零至10倍，由存在的阳离子的氧化态确定，包括制备包含待包含在最终催化剂中的所述元素化合物的源批料的混合物的含水浆料，然后干燥 以及将所述混合物煅烧为活性催化剂，其中所述锡的所述源批料为包含SnO 2·xH 2 O的溶液，其中x 2 = 0分散在四烷基氢氧化铵中，其中所述四烷基氢氧化铵由下式定义：C n H 2n + 1NOH其中5> / = n> / = 1，干燥所述浆料并将混合物煅烧至上煅烧温度 至少500℃