METHOD OF REFINING RAFFINATE-2
    53.
    发明申请

    公开(公告)号:US20210363075A1

    公开(公告)日:2021-11-25

    申请号:US16625333

    申请日:2018-07-20

    Applicant: LG CHEM, LTD.

    Abstract: A method for separating and refining 1-butene with a high purity and a high yield from a raffinate-2 stream. The method includes: feeding raffinate-2 to a first distillation column; obtaining heavy raffinate-3 from a lower part of the first distillation column; recovering an upper part fraction containing 1-butene from an upper part of the first distillation column; feeding the upper part fraction containing 1-butene to a second distillation column; recovering a first lower part fraction rich in 1-butene from a lower part of the second distillation column and light raffinate-3 from an upper part of the second distillation column. Heat of the upper part fraction recovered from the upper part of the first distillation column is fed to the lower part of the second distillation column through a first heat exchanger. Thus, 1-butene is obtained with high purity and high yield while maximizing an energy recovery amount by double-effect distillation.

    A METHOD FOR MANUFACTURING TEREPHTHALATE-BASED COMPOSITION COMPRISING APPLYING PRESSURE

    公开(公告)号:US20210317063A1

    公开(公告)日:2021-10-14

    申请号:US17273279

    申请日:2019-09-18

    Applicant: LG CHEM, LTD.

    Abstract: Provided is a method for manufacturing a terephthalate-based composition, the method comprising: a step (S1) of flowing in a dialkyl terephthalate in which alkyl has 7 to 10 carbon atoms and a primary alcohol with a low boiling point having 4 or 5 carbon atoms into a reactor and performing transesterification of the dialkyl terephthalate and the primary alcohol with a low boiling point and a step (S2) of extracting in a reduced pressure an unreacted material and a by-product from the reactor after finishing the transesterification, wherein the step S1 comprises a pressure-applying step in which the pressure of the reactor is 1.5 to 2.5 bar.

    ESTER COMPOSITION PREPARATION SYSTEM AND ESTER COMPOSITION PREPARATION METHOD USING SAME

    公开(公告)号:US20190263745A1

    公开(公告)日:2019-08-29

    申请号:US16343988

    申请日:2018-09-05

    Applicant: LG CHEM, LTD.

    Abstract: Provided are an ester composition preparation system, including an integrated reactor, a gas-liquid separation column, a purification unit, an alcohol storage tank, and a mixed alcohol separation column, which is an efficient, economical, and simplified ester composition preparation system, and an ester composition preparation method using the same. The ester composition preparation system is a simplified system which can reduce facility space, drastically remove reaction equipment, and reduce transfer time through the introduction of the integrated reactor in which the reaction preparing an ester compound and the reaction preparing an ester composition are carried out in one space, the mixed alcohol separation column and the gas-liquid separation column.

    DISTALLATION DEVICE (AMENDED)
    58.
    发明申请

    公开(公告)号:US20180169542A1

    公开(公告)日:2018-06-21

    申请号:US15580393

    申请日:2016-07-01

    Applicant: LG CHEM, LTD

    Abstract: The present application relates to a distillation device. When a feedstock containing acetone and methanol is separated using a distillation device according to the present application, a methanol removal distillation column may be located at a position for easily separating methanol to solve a problem due to accumulation of methanol in the process and to lower the methanol content in the acetone product, and thus the lifetime of catalysts can be extended, and moreover, methanol can be removed with good efficiency from a flow of the lower part of the distillation column obtaining the final acetone product by using only the conventional phase separator and one methanol removal distillation column further installed, so that the acetone product obtained from the upper part of the distillation column obtaining the acetone product can be obtained in high purity and the operating cost and the equipment cost of equipments can be greatly reduced.

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