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    Process for preparation of aromatic dimers
    61.
    发明授权
    Process for preparation of aromatic dimers 失效
    芳族二聚体的制备方法

    公开(公告)号：US4885423A

    公开(公告)日：1989-12-05

    申请号：US350667

    申请日：1989-05-11

    Applicant: Mark Rule

    Inventor： Mark Rule

    IPC: C07C17/26

    CPC classification number: C07C17/269

    Abstract: A process for preparation of an aromatic dimer compound corresponding to the structureIxAr-ArIxwherein x is 0, 1, 2, 3, 4, or 5 and Ar is a divalent aromatic radical containing 6 to 14 carbon atoms comprising contacting, at a sufficient temperature and pressure in the absence of carbon monoxide and in the absence of an alkali metal compound or an alkaline earth metal compound, platinum and an aromatic iodide compound corresponding to the structureAr-Ixwhere Ar is a monovalent aromatic radical and x is 1, 2, 3, 4, 5, or 6.

    Abstract translation: 制备对应于结构IxAr-ArIx的芳族二聚体化合物的方法，其中x为0,1,2,3,4或5，Ar为含有6至14个碳原子的二价芳基，包括以足够的 在不存在一氧化碳的情况下，在不存在碱金属化合物或碱土金属化合物的情况下，对应于结构Ar-Ix的铂和芳香族碘化合物，其中Ar是一价芳族基，x是1， 2，3，4，5或6。

    Process for the preparation of copoly(arylene sulfide)
    62.
    发明授权
    Process for the preparation of copoly(arylene sulfide) 失效
    共聚（亚芳基硫醚）的制备方法

    公开(公告)号：US4859762A

    公开(公告)日：1989-08-22

    申请号：US308924

    申请日：1989-02-13

    Applicant: Mark Rule ,  David R. Fagerburg ,  Joseph J. Watkins

    Inventor： Mark Rule ,  David R. Fagerburg ,  Joseph J. Watkins

    IPC: C08G75/02

    CPC classification number: C08G75/0263 ,  C08G75/0222

    Abstract: A process for preparing a copoly(arylene sulfide) corresponding to the structure[(--A--S--).sub.1-x (--A--S--S--).sub.x ].sub.nwherein x is in the range of 0.5 to 0.001 by reacting a mixture of a diiodoaromatic compound and elemental sulfur in the absence of a basic material and in the presence of a catalytic amount of an organic amine-containing compound.

    Abstract translation: 制备对应于[（-AS-）1-x（-ASS-）x] n结构的共聚（亚芳基硫醚）的方法，其中x为0.5至0.001的范围内，通过使二碘代芳族化合物和 在不存在碱性物质的情况下和在催化量的含有机胺化合物存在下的元素硫。

    Oxidative iodination of phenol
    63.
    发明授权
    Oxidative iodination of phenol 失效
    酚的氧化碘化

    公开(公告)号：US4855514A

    公开(公告)日：1989-08-08

    申请号：US232964

    申请日：1988-08-17

    Applicant: Mark Rule ,  Regina M. Moncier

    Inventor： Mark Rule ,  Regina M. Moncier

    IPC: C07C29/38 ,  C07C37/62

    CPC classification number: C07C37/62

    Abstract: A process for producing iodophenols which comprises contacting phenol, a source of iodine and molecular oxygen in an aqueous medium to produce an iodophenol.

    Abstract translation: 一种生产碘酚的方法，其包括使苯酚，碘源和分子氧在水性介质中接触以产生碘苯酚。

    Carbonylation process for the production of aromatic acids
    66.
    发明授权
    Carbonylation process for the production of aromatic acids 失效
    用于生产芳香酸的羰基化方法

    公开(公告)号：US4705890A

    公开(公告)日：1987-11-10

    申请号：US26916

    申请日：1987-03-17

    Applicant: Guy R. Steinmetz ,  Mark Rule

    Inventor： Guy R. Steinmetz ,  Mark Rule

    IPC: C07C51/10

    CPC classification number: C07C51/10

    Abstract: Disclosed is a process for production of aromatic carboxylic acids by the carbonylation of aromatic iodides in the presence of a ruthenium catalyst, a Bronsted base, and an iodide promoter.

    Abstract translation: 公开了在钌催化剂，Bronsted碱和碘化物促进剂的存在下通过芳族碘化物的羰基化生产芳族羧酸的方法。

    Infrared radiation absorbent anthraquinone derivatives in polyester compositions
    67.
    发明授权
    Infrared radiation absorbent anthraquinone derivatives in polyester compositions 失效
    聚酯组合物中的红外辐射吸收蒽醌衍生物

    公开(公告)号：US4481314A

    公开(公告)日：1984-11-06

    申请号：US509112

    申请日：1983-06-29

    Applicant: Mark Rule

    Inventor： Mark Rule

    IPC: C08K5/18 ,  C08K5/42 ,  C09K15/24

    CPC classification number: C08K5/18 ,  Y10S430/145 ,  Y10S430/146

    Abstract: Disclosed are novel anthraquinone compounds containing tetra-p-phenylenediamine substituents, particularly useful in molding type polyester compositions and possessing strong infrared absorptivity. This property renders these compounds attractive as additives for increasing the infrared energy absorptivity of polyesters either from high intensity quartz lamps or from certain laser systems. These compounds are particularly useful in bottle polyester material for increasing the blow-mold parison reheat rate, and in the printing of plastic articles with lasers.

    Abstract translation: 公开了含有四对苯二胺取代基的新型蒽醌化合物，特别适用于成型型聚酯组合物并且具有强的红外吸收性。 这种性质使得这些化合物作为增加聚酯的红外能量吸收性的添加剂是有吸引力的，或者来自高强度石英灯或来自某些激光系统。 这些化合物特别适用于瓶聚酯材料，用于增加吹模型坯再加热速率，以及在用激光打印塑料制品时。

    Process for preparing high molecular weight polyesters
    68.
    发明授权
    Process for preparing high molecular weight polyesters 失效
    制备高分子量聚酯的方法

    公开(公告)号：US4446303A

    公开(公告)日：1984-05-01

    申请号：US517485

    申请日：1983-07-26

    Applicant: Louis D. Moore ,  Mark Rule ,  Thomas H. Wicker

    Inventor： Louis D. Moore ,  Mark Rule ,  Thomas H. Wicker

    IPC: C08G63/80 ,  C08G63/26 ,  C08G63/70

    CPC classification number: C08G63/80

    Abstract: Disclosed is a process for the manufacture of high molecular weight polyesters, particularly poly(ethylene terephthalate) (PET) and modified PET, having inherent viscosities (I.V.) for example, above about 0.6, and up to about 1.3 or higher. Such polymers are useful, for example, as structural moldings, self-supporting sheets and films, and blow-molded bottles. The process involves one or more recrystallizations of the polymer incident to solid-state polycondensation, which recrystallizations, it has been discovered, restores the high polycondensation activity of the polymer experienced in the early stages thereof and allows greatly increased overall build-up rate and higher final I.V. for the total polycondensation period. The process is particularly applicable to crystallizable polyesters in general which lend to solid-state build-up.

    Abstract translation: 公开了一种用于制造高分子量聚酯，特别是聚对苯二甲酸乙二醇酯（PET）和改性PET的方法，其具有例如高于约0.6且高达约1.3或更高的特性粘度（I.V）。 这样的聚合物可用作例如结构模制品，自支撑片材和薄膜以及吹塑瓶子。 该方法包括进入固态缩聚反应的聚合物的一次或多次重结晶，已经发现重结晶可恢复在其早期阶段遇到的聚合物的高缩聚活性，并允许大大提高总体累积速率和更高的 最后四 用于总缩聚期。 该方法特别适用于可结晶聚酯，其通常能够固化成固态聚合物。

    SCAVENGING OXYGEN
    70.
    发明申请
    SCAVENGING OXYGEN 审中-公开

    公开(公告)号：US20150129454A1

    公开(公告)日：2015-05-14

    申请号：US14535593

    申请日：2014-11-07

    Applicant: Mark Rule ,  Ronald J. Valus ,  Steven Burgess Tattum

    Inventor： Mark Rule ,  Ronald J. Valus ,  Steven Burgess Tattum

    IPC: B65D81/26

    CPC classification number: B65D81/26 ,  A23L3/3436 ,  B65D51/244 ,  B65D81/266 ,  C01B3/065 ,  C08K3/014 ,  C08K3/10 ,  C08K5/098 ,  Y02E60/362

    Abstract: A container 22 includes a shell 24 made from a polymer, for example PET, and incorporating a catalyst, for example a palladium catalyst. A closure 40 incorporates a plug which includes a source of hydrogen, for example a hydride. In use, with container 22 including a beverage and closure 40 in position, the headspace in the container will be saturated with water vapor. This vapor contacts the hydride associated with plug 42 and as a result the hydride produces molecular hydrogen which migrates into the polymer matrix of shell 24 and combines with oxygen which may have entered the container through its permeable walls. A reaction between the hydrogen and oxygen takes place, catalysed by the catalyst, and water is produced. Thus, oxygen which may ingress the container is scavenged and the contents of the container are protected from oxidation.

    Abstract translation: 容器22包括由聚合物例如PET制成的壳体24，并且加入催化剂，例如钯催化剂。 封闭件40包括一个包括氢源的插塞，例如氢化物。 在使用中，对于包括饮料和封闭件40在内的容器22，容器中的顶部空间将被水蒸气饱和。 该蒸汽接触与塞42相关的氢化物，结果氢化物产生分子氢，其迁移到壳24的聚合物基质中，并与可能通过其渗透壁进入容器的氧结合。 氢和氧之间发生反应，催化剂催化，产生水。 因此，可能进入容器的氧气被清除，容器的内容物被保护免受氧化。

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