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    Dispersant Comprising Copolymer Mixture
    61.
    发明申请
    Dispersant Comprising Copolymer Mixture 有权
    分散剂包含共聚物混合物

    公开(公告)号：US20120041104A1

    公开(公告)日：2012-02-16

    申请号：US13133043

    申请日：2009-11-25

    申请人： Klaus Lorenz ,  Mario Vierle ,  Barbara Wimmer ,  Petra Wagner ,  Christian Schôlz

    发明人： Klaus Lorenz ,  Mario Vierle ,  Barbara Wimmer ,  Petra Wagner ,  Christian Schôlz

    IPC分类号： C04B16/04 ,  C08L35/08 ,  C08L41/00 ,  C04B28/02 ,  C08L35/00 ,  C08L33/02 ,  C08L37/00 ,  C08J3/07 ,  C08L39/04 ,  C08L43/02

    CPC分类号： C04B24/2647 ,  C04B24/2658 ,  C04B24/267 ,  C04B40/0039 ,  C04B2103/32 ,  C04B2103/408 ,  C08G65/2609 ,  C08L29/10 ,  C08L33/02 ,  C08L33/066 ,  C08L33/14 ,  C08L33/26 ,  C08L35/08 ,  C08L43/02 ,  C08L71/02 ,  C08L2205/02 ,  C08L2666/04 ,  C08L2666/22

    摘要： The invention relates to a polymer composition containing 3 to 95% by weight of a copolymer H and 3 to 95% by weight of a copolymer K, the copolymers H and K each having polyether macromonomer structural units and acid monomer structural units, which are present in the copolymers H and K in each case in a molar ratio of 1:20 to 1:1, and at least 20 mol % of all structural units of the copolymer H and at least 25 mol % of all structural units of the copolymer K being present in each case in the form of acid monomer structural units, the polyether macromonomer structural units of the copolymers H and K having side chains containing in each case at least 5 ether oxygen atoms, the number of ether oxygen atoms per side chain of the polyether macromonomer structural units of the copolymers H and K varying in each case in such a way that the corresponding frequency distribution diagrams, in which the number of ether oxygen atoms per side chain of a polyether macromonomer structural unit is plotted in each case along the abscissae and the respectively associated frequencies for the copolymers H or K are plotted in each case along the ordinates, contain in each case at least 2 maxima whose abscissa values differ in each case by more than 7 ether oxygen atoms from one another, the frequency distribution diagrams of the copolymers H and K differing from one another in that the abscissa value of at least one maximum of the copolymer H differs in each case by more than 5 ether oxygen atoms from the abscissa values of all maxima of the copolymer K and/or that the arithmetic means of the ether oxygen atoms of the polyether macromonomer structural units of the copolymers H and K differ from one another by more than 5 ether oxygen atoms.

    摘要翻译： 本发明涉及含有3〜95重量％共聚物H和3〜95重量％共聚物K的聚合物组合物，共聚物H和K各自具有聚醚大分子单体结构单元和酸单体结构单元，其存在 在共聚物H和K中的摩尔比为1:20至1:1的共聚物中，共聚物H的全部结构单元的至少20摩尔％和共聚物K的所有结构单元的至少25摩尔％ 在各种情况下以酸单体结构单元的形式存在，共聚物H和K的聚醚大分子单体结构单元具有侧链，每种情况下含有至少5个醚氧原子，每个侧链的醚氧原子数 共聚物H和K的聚醚大分子单体结构单元在每种情况下变化，使得相应的频率分布图，其中聚醚大分子单体结构单元每侧链的醚氧原子数为pl 在每个情况下沿着横坐标分别表示，并且在每种情况下沿着纵坐标绘制共聚物H或K的分别相关联的频率，每种情况下包含至少2个最大值，其横坐标值在每种情况下不同于7个以上的醚氧原子 另一方面，共聚物H和K的频率分布图彼此不同，因为共聚物H的至少一个最大值的横坐标值在每种情况下都不同于5个以上的醚氧原子，从所有最大值的横坐标值 共聚物K和/或共聚物H和K的聚醚大分子单体结构单元的醚氧原子的算术手段彼此间隔超过5个醚氧原子。

    ANTI-FOAMING AGENT FOR THE PAPER INDUSTRY
    63.
    发明申请
    ANTI-FOAMING AGENT FOR THE PAPER INDUSTRY 审中-公开
    造纸行业的反泡剂

    公开(公告)号：US20100212847A1

    公开(公告)日：2010-08-26

    申请号：US12680456

    申请日：2008-10-13

    申请人： Christoph Hamers ,  Klaus Lorenz

    发明人： Christoph Hamers ,  Klaus Lorenz

    IPC分类号： D21C3/28 ,  B01D19/04

    CPC分类号： D21H21/12 ,  B01D19/0404 ,  D21H17/14

    摘要： Antifoams for the paper industry, based on oil-in-water emulsions in which the oil phase comprises(a) at least one alcohol having at least 12 carbon atoms, fatty acid esters of alcohols having at least 22 carbon atoms and C1- to C36-carboxylic acids, distillation residues which are obtainable in the preparation of alcohols having a carbon number of at least 8 by oxo synthesis or by the Ziegler process and which, if appropriate, are alkoxylated, mixtures of said compounds and/or(b) at least one fatty acid ester of C12- to C22-carboxylic acids with monohydric to trihydric C1- to C18-alcohols and, if appropriate,(c) at least one hydrocarbon having a boiling point above 200° C. or a fatty acid having 12 to 22 carbon atoms and(d) from 1 to 80% by weight of polyglyceryl esters which are obtainable by at least 20% esterification of polyglycerol mixtures comprising from 0 to 10% by weight of monoglycerol, from 15 to 40% by weight of diglycerol, from 30 to 55% by weight of triglycerol, from 10 to 25% by weight of tetraglycerol, from 0 to 15% by weight of pentaglycerol, from 0 to 10% by weight of hexaglycerol and from 0 to 5% by weight of polyglycerols having a higher degree of condensation with at least one fatty acid having 12 to 36 carbon atoms, more than 50 to 80% by weight of the oil phase being involved in the production of the oil-in-water emulsions.

    摘要翻译： 用于造纸工业的消泡剂，其基于水包油乳液，其中油相包含（a）至少一种具有至少12个碳原子的醇，具有至少22个碳原子的醇的脂肪酸酯和C 1 -C 36 - 羧酸，可通过氧代合成或通过齐格勒方法制备碳原子数至少为8的醇而得到的蒸馏残余物，如果合适的话，其可以被烷氧基化，所述化合物和/或（b）的混合物在 至少一种C 12〜C 22羧酸与一元至三元C 1至C 18醇的脂肪酸酯，如果合适，（c）至少一种沸点高于200℃的烃或具有12 至22个碳原子和（d）1至80重量％的聚甘油酯，其可通过至少20％的聚甘油混合物酯化获得，所述聚甘油混合物包含0至10重量％的单甘油，15至40重量％的双甘油 ，30至55重量％的三甘油 10至25重量％的四甘油，0至15重量％的五甘油，0至10重量％的六甘油和0至5重量％的与至少一种脂肪具有较高缩合度的聚甘油 具有12至36个碳原子的酸，大于50至80重量％的油相参与水包油乳液的生产。

    Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde
    69.
    发明授权
    Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde 失效
    苯二酚酸，二羟基二苯基硫醚，尿素和甲醛的浓缩产物

    公开(公告)号：US5155164A

    公开(公告)日：1992-10-13

    申请号：US696912

    申请日：1991-05-08

    申请人： Hermann Graf ,  Adolf Stuebinger ,  Klaus Lorenz ,  Ortwin Schaffer ,  Karl Stork

    发明人： Hermann Graf ,  Adolf Stuebinger ,  Klaus Lorenz ,  Ortwin Schaffer ,  Karl Stork

    IPC分类号： C08G14/02

    CPC分类号： C08G14/02

    摘要： Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde can be obtained by(A) preparing a homogeneous reaction mixture in sulfuric acid from the phenolmonosulfonic acid and dihydroxydiphenyl sulfone in the molar ratio of from 3:1 to 10:1, with the proviso that the water content of the mixture is not more than 10% of the total weight of the components, and the mixture contains from 0.3 to 1.5 moles of sulfuric acid per mole of dihydroxydiphenyl sulfone, at from 100.degree. to 180.degree. C.,(B) subsequently, at from 40.degree. to 90.degree. C., carrying out a precondensation with 1 to 2 moles of formaldehyde and 0.5 to 1.5 moles of urea per mole of phenol units present in aqueous medium,(C) partially neutralizing the reaction mixture,(D) adding to the partially neutralized reaction mixture 0 to 0.5 mole of phenol per mole of phenol units present and then 0.1 to 0.8 mole of formaldehyde per mole of phenol units then present,(E) further condensing at from 40.degree. to 90.degree. C.,(F) shifting the pH of the reaction mixture into the neutral range and(G) subsequently acidifying with a weak acid.

    摘要翻译： 苯酚磺酸，二羟基二苯基砜，脲和甲醛缩合的产物可以通过以下方法获得：（A）在苯磺酸和二羟基二苯基砜的硫酸中以3:1至10:1的摩尔比制备均匀的反应混合物， 条件是混合物的水含量不超过组分总重量的10％，并且混合物含有0.3至1.5摩尔硫酸/摩尔二羟基二苯基砜，在100至180℃ （B）随后在40℃至90℃下，每1摩尔含水介质中的苯酚单元进行1至2摩尔甲醛和0.5至1.5摩尔脲的预缩合，（C）部分中和 反应混合物中，（D）向部分中和的反应混合物中加入每摩尔苯酚单元0至0.5摩尔苯酚，然后存在每摩尔苯酚单元0.1至0.8摩尔甲醛，（E）进一步冷凝 在40℃至90℃下，（F）将反应混合物的pH转移到中性范围，（G）随后用弱酸酸化。