Process for preparation of polytrimethylene ether glycols
    71.
    发明授权
    Process for preparation of polytrimethylene ether glycols 失效
    聚三亚甲基醚二醇的制备方法

    公开(公告)号:US07074969B2

    公开(公告)日:2006-07-11

    申请号:US10871622

    申请日:2004-06-18

    IPC分类号: C07C41/34

    摘要: There is disclosed a process for preparing polytrimethylene ether glycol by acid catalyzed polycondensation, neutralization and contact with filter aid. The process avoids hydrolysis and yet provides product substantially free of catalyst derived end groups.

    摘要翻译: 公开了通过酸催化缩聚,中和和与助滤剂接触来制备聚三亚甲基醚二醇的方法。 该方法避免水解,并提供基本上不含催化剂衍生的端基的产物。

    Process for the production of polyamides from dinitriles and diamines
    74.
    发明授权
    Process for the production of polyamides from dinitriles and diamines 有权
    从二腈和二胺生产聚酰胺的方法

    公开(公告)号:US06509439B1

    公开(公告)日:2003-01-21

    申请号:US09549330

    申请日:2000-04-14

    IPC分类号: C08G6900

    CPC分类号: C08G69/04 C08G69/28

    摘要: A process for producing polyamides from dinitriles and diamines in a continuous reaction using subsequent heating steps. In particular, the process involves contacting a dinitrile, a diamine, water, and optionally a catalyst to form a reaction mixture; heating the reaction mixture to a first elevated temperature of between about 180 to about 240° C., maintaining said temperature for about 0.10 to about 20 hours, and optionally controlling the pressure in this heating step by venting; heating the reaction mixture to a second elevated temperature of between about 250 to about 350° C., adding water to the reaction mixture before or after the second elevated temperature is reached, maintaining the pressure in the second heating step above atmospheric pressure by venting at least some of the water, and maintaining the second elevated temperature for a period of about 0.10 to about 10 hours; and recovering the polyamide.

    摘要翻译: 使用随后的加热步骤在连续反应中由二腈和二胺生产聚酰胺的方法。 特别地,该方法包括使二腈,二胺,水和任选的催化剂接触以形成反应混合物; 将反应混合物加热至约180至约240℃的第一升高温度,将所述温度保持约0.10至约20小时,并且可选地通过排气控制该加热步骤中的压力; 将反应混合物加热至约250至约350℃的第二升高温度,在达到第二升高温度之前或之后向反应混合物中加入水,将第二加热步骤中的压力通过排气在 至少一些水,并保持第二升高温度约0.10至约10小时; 并回收聚酰胺。

    Copolyether composition and processes therefor and therewith
    75.
    发明授权
    Copolyether composition and processes therefor and therewith 失效
    共聚醚组合物及其工艺及其

    公开(公告)号:US06316586B1

    公开(公告)日:2001-11-13

    申请号:US09638356

    申请日:2000-08-15

    IPC分类号: C08G6366

    CPC分类号: C08G63/6886 C08G63/672

    摘要: A copolyether composition that can be used to produce a dyeable polyester is provided. The composition can comprise repeat units derived from a first diol such as, for example, 1,3-propanediol and a sulfonated dicarboxylic acid such as, for example, 5-sulfo-isophthalic acid. The dyeable polyester composition can comprise repeat units derived from the copolyether composition, an acid such as, for example, terephthalic acid, and a second diol such as, for example, 1,3-propanediol. Also disclosed is a process that can be used for producing the copolyether composition. The process comprises contacting the first diol with the sulfonated dicarboxylic acid. Further disclosed is a process that can be used for producing the dyeable composition in which the process comprises (1) contacting, in the presence of a catalyst, the copolyether composition with a diol such as, for example, 1,3-propanediol, and a dicarboxylic ester such as, for example, dimethylterephthalate or (2) contacting an acid such as for example, terephthalic acid and a diol such as, for example, 1,3-propanediol to produce an intermediate and thereafter contacting the intermediate with the copolyether.

    摘要翻译: 提供了可用于生产可染色聚酯的共聚醚组合物。 组合物可以包含衍生自第一二醇的重复单元,例如1,3-丙二醇和磺化二羧酸,例如5-磺基间苯二甲酸。 可染性聚酯组合物可以包含衍生自共聚醚组合物的重复单元,酸例如对苯二甲酸,和第二二醇,例如1,3-丙二醇。 还公开了可用于制备共聚醚组合物的方法。 该方法包括使第一二醇与磺化二羧酸接触。 进一步公开的是可用于生产可染组合物的方法,其中该方法包括(1)在催化剂存在下使共聚醚组合物与二醇例如1,3-丙二醇接触,和 二羧酸酯,例如对苯二甲酸二甲酯或(2)使酸例如对苯二甲酸与二醇例如1,3-丙二醇接触以制备中间体,然后使中间体与共聚醚接触 。

    Wellbore fluids comprising poly(trimethylene ether) glycol polymers
    78.
    发明授权
    Wellbore fluids comprising poly(trimethylene ether) glycol polymers 失效
    井筒流体包含聚(三亚甲基醚)乙二醇聚合物

    公开(公告)号:US08288324B2

    公开(公告)日:2012-10-16

    申请号:US13075447

    申请日:2011-03-30

    申请人: Hari Babu Sunkara

    发明人: Hari Babu Sunkara

    IPC分类号: C09K8/24 C09K8/28

    摘要: Wellbore fluids containing poly(trimethylene ether)glycols are provided. The wellbore fluids can provide enhanced functionality, improved cost effectiveness, and reduced environmental impact as compared to conventional wellbore fluids.

    摘要翻译: 提供含有聚(三亚甲基醚)二醇的井筒流体。 与常规井眼流体相比,井筒流体可以提供增强的功能,改善的成本效益和减少的环境影响。

    BLENDS COMPRISING BRANCHED POLY(TRIMETHYLENE ETHER) POLYOLS
    79.
    发明申请
    BLENDS COMPRISING BRANCHED POLY(TRIMETHYLENE ETHER) POLYOLS 审中-公开
    包含分支聚(三甲苯醚)多元醇的共混物

    公开(公告)号:US20120228546A1

    公开(公告)日:2012-09-13

    申请号:US13220052

    申请日:2011-08-29

    申请人: Hari Babu Sunkara

    发明人: Hari Babu Sunkara

    IPC分类号: C08G18/32 C09K3/00

    摘要: Disclosed are blends comprising branched poly(trimethylene ether)polyols prepared from the acid catalyzed polycondensation reaction of 1,3-propanediol, and at least one triol comonomer selected from 1,1,1-tris(hydroxymethyl)ethane and 1,1,1-tris(hydroxymethyl)propane. The blends are useful in the preparation of polyurethane rigid and flexible foams.

    摘要翻译: 公开了包含由1,3-丙二醇的酸催化缩聚反应制备的支化聚(三亚甲基醚)多元醇和至少一种选自1,1,1-三(羟甲基)乙烷和1,1,1-三羟甲基丙烷的三元共聚单体的共混物 - 三(羟甲基)丙烷。 该混合物可用于制备聚氨酯刚性和柔性泡沫。

    Deodorant compositions
    80.
    发明授权
    Deodorant compositions 有权
    除臭剂组合物

    公开(公告)号:US08114423B2

    公开(公告)日:2012-02-14

    申请号:US11869056

    申请日:2007-10-09

    CPC分类号: A61L9/01 A61K8/86 A61Q15/00

    摘要: This invention relates to deodorant compositions containing polytrimethylene ether glycol homo- and copolymers and/or polytrimethylene glycol ester(s) in a variety of physical forms. In at least one embodiment, the polytrimethylene ether glycol homo- and copolymers and/or polytrimethylene glycol ester(s) are derived predominantly from monomers (e.g., 1,3-propanediol) obtained from renewable resources, and are thus more environmentally friendly in terms of manufacture, use and disposal.

    摘要翻译: 本发明涉及含有各种物理形式的聚三亚甲基醚二醇均聚物和共聚物和/或聚三亚甲基二醇酯的除臭剂组合物。 在至少一个实施方案中,聚三亚甲基醚二醇均聚物和/或聚三亚甲基二醇酯主要衍生自从可再生资源获得的单体(例如,1,3-丙二醇),因此对环境友好 的制造,使用和处置。