Abstract:
A spectrophotometer including: a) a light source switching mechanism for switching a plurality of light sources by swinging a light source mirror; b) a filter selecting mechanism; c) a diffraction grating rotating mechanism; and d) a controller for determining the operation origins of the three driving mechanisms using a rough origin sensor provided for the diffraction grating rotating mechanism and a photometer. The operation of the controller is to: i) determine an origin of the movement of the filter by making an end of the filter frame to touch a stopper; ii) determine a rough origin of the diffraction grating using the rough origin sensor; and iii) determine an origin of the movement of the light source mirror and a precise origin of the movement of the diffraction grating by detecting the position at which the photometer detects the maximum intensity of light.
Abstract:
An optical system and method comprising a diffraction grating which consists of diffracting elements spaced from one another by unequal distances. Correction of residual defocusing in the image produced by such a grating is accomplished by translating it along its surface. As one embodiment, a monochromator is constructed on which a self-focusing grating scans the value in wavelength which is transmitted between fixed slits by rotation of the grating about an axis fixed in space. Combined with a translation of the grating along its surface, such a monochromator produces a symmetrical image exactly in focus at the exit slit for all scanned wavelengths.
Abstract:
An apparatus for determining concentrations of mineral elements comprising an improved spectrometer wherein the spectrometer functions to diffract the light to be measured by means of a rotary grating and to determine the strength of light by using a single PM tube and further detects the wavelength of the diffracted light, by using a laser beam generator, reflective mirrors, photo diodes so as to analyze the composition and the concentration of mineral elements.
Abstract:
Each sample is analyzed for all desired elements before starting the next sample, using thermal or nonthermal atomizing devices fro liquid or solid samples. Other new features include the grating drive, lamp-carousel alignment, pulsed atom source, lamp-drift compensation, and dynamic range control. The grating is driven by an arm, the arm by a taut band wound on a drum, and the drum directly by a motor. The lamp carousel mounts on an "L"-shaped rocker with one horizontal and one vertical arm. The carousel rotates on a horizontal axis at the end of the vertical arm. The rocker itself pivots on a horizontal axis at the corner of the L; it is driven about its axis by a motor and screw at the other end of the L. Carousel rotation on its axis moves the right lamp into position and adjusts it accurately in a vertical direction. Pivoting of the rocker simultaneously on its corner axis positions the lamp accurately in a horizontal direction. The pulsed atom source is a combined angled-gas-jet-and-discharge unit. During pulses it yields high absorption with better detectability limits; average power is lower. The lamp-drift compensator makes double duty of the absorber pulsation to obtain a lamp-intensity reading between pulses. Dynamic range control is obtained by even further exploiting the pulsation, namely by taking measurements at a known delay (and decay) time after each pulse.
Abstract:
An improved mounting for a rotating diffraction grating assembly as used in a spectrophotometer directly connects the grating to the galvanometer that rotates the grating. The galvanometer is gimbally mounted on a plate so that its position, and that of the grating, can be adjusted so that the plane of dispersion of the grating passes through a desired point when the grating is rotated.
Abstract:
A manual device for the detection of photometric data which includes a measuring head to illuminate a measuring surface and to detect the light reflected. The measuring light captured by the measuring head is spectrally decomposed by a monochromator containing a diffraction grating. The intensity of the light exiting through an outlet diaphragm is detected by a photodetector. The spectral position of the measuring light is set by a drive motor rotating a grating shaft connected with the holder of the diffraction grating. From the spectra detected, densitometric and colorimetric data are calculated by a computer, which together with the spectra determined, may be displayed on a display field.
Abstract:
A photodiode array spectrometer for determining the spectral composition of a plychromatic beam of radiation comprises diffraction means (10) which generate from the polychromatic beam a diffracted beam with a plurality of spatially separated diffracted rays of different wavelengths (.lambda..sub.1, .lambda..sub.2, .lambda..sub.3). A photodiode array (11) receives the diffracted beam whereby each photodiode intercepts a different spectral portion of the beam. A rotatable transparent plate (8) is provided in the beam path in front of the diffraction means (10) which, due to refraction of the beam upon entering and leaving the plate (8), permits to vary the direction of the beam impinging on the diffraction means (10) and therefore the direction of the diffracted beam in small steps depending on the angle of rotation of the plate (8). By the stepwise displacement of the diffracted beam across the photodiode array (11), a better sampling of the diffracted beam and therefore an improved spectral resolution is achieved. The invention can be used in the spectrometric analysis of a sample contained in a sample cell ( 5), whereby the sample cell is irradiated with polychromatic light from a light source (1).
Abstract:
A scanning monochromator system comprises a housing, structure defining entrance and exit apertures, and a radiation dispersing component in the housing arranged to disperse radiation passing through the entrance aperture into a spectrum for transmission towards the exit aperture. The dispersing element is directly coupled to an electromagnetic drive transducer with the assembly of a rotary component of the drive transducer and the dispersing component being mounted for rotation as a unit about a stationary axis that is perpendicular to the optical axis of the system so that a selected portion of the radiation dispersed by the dispersing component is passed through the exit aperture. The drive transducer is arranged to move a selected portion of dispersed radiation at the exit aperture over a wavelength range of at least 3000 angstroms with a reproducible accuracy of better than 0.03 angstroms in less than one second.
Abstract:
Disclosed herein is a spectrophotometer which includes a source of radiation; an optical system for forming a beam of radiation from the source and directing it along a sample path and along a reference path, which paths come together at a location to form a combined path that impinges on a detector; a chopper mounted at said location for successively directing one or the other of the beams along the combined path or providing a blank chopper area for blocking radiation from the combined path; a monochromator having a grating and slits disposed in the combined path, the angular position of the grating being adjustable for passing selected successive wavelengths of radiant energy through the optical system; and controls are provided for controlling the movement of the grating and/or slits so that movement only occurs when the blank chopper area is blocking the combined path.
Abstract:
A method of identifying an operating position of a multiple-position filter changing mechanism situated in an optical path of a spectrophotometer by detecting and measuring a spectral characteristic(s) of light passed along the optical path to the spectrophotometer detector for one or more operating positions of the filter mechanism and comparing the measured spectral characteristic(s) with stored spectral characteristic information for one or more operating positions of the filter mechanism.