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公开(公告)号：US07323519B2
公开(公告)日：2008-01-29
申请号：US10501023
申请日：2003-01-21
Applicant: Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
Inventor： Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
CPC classification number: C08F8/26 , C08F8/16 , C08F8/48 , C08F2810/30 , C08F2810/40 , Y10T436/196666
Abstract: The present invention provides: a process for preparing a vinyl polymer containing a halogen in an amount of 1,000 mg or less per kilogram, in which a vinyl polymer containing the halogen produced by atom transfer radical polymerization of a vinyl monomer is heated at a temperature in the range of 140 to 250° C. to dehalogenate the vinyl polymer; a vinyl polymer obtained by the process; and a hydrosilylation-reactive curable composition containing the vinyl polymer.
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公开(公告)号：US07276574B2
公开(公告)日：2007-10-02
申请号：US10491187
申请日：2002-10-17
Applicant: Akihisa Hirota , Kosuke Tanaka , Shigeru Hagimori , Yosuke Asai , Naoki Furukawa , Masanao Takeda , Nao Fujita , Yoshiki Nakagawa
Inventor： Akihisa Hirota , Kosuke Tanaka , Shigeru Hagimori , Yosuke Asai , Naoki Furukawa , Masanao Takeda , Nao Fujita , Yoshiki Nakagawa
CPC classification number: C08F6/02 , C08F8/06 , C08F2438/01 , C08F2810/30 , C08F2810/40 , C08F8/26 , C08F120/18 , C08F2220/1808 , C08F2220/1825 , C08F2220/281
Abstract: The present invention provides a method for producing a vinyl polymer including the steps of polymerizing a vinyl monomer by atom transfer radical polymerization with a transition metal complex as a polymerization catalyst, and bringing the resultant vinyl polymer into contact with an adsorbent in the presence of an oxidizing agent; the vinyl polymer produced by the method; and a reactive composition susceptible to hydrosilylation containing the vinyl polymer produced by the method and having at least one alkenyl group per molecule.
Abstract translation: 本发明提供一种乙烯基聚合物的制造方法，包括以下步骤：用过渡金属络合物作为聚合催化剂通过原子转移自由基聚合使乙烯基单体聚合，并使所得到的乙烯基聚合物与吸附剂接触， 氧化剂; 通过该方法制备的乙烯基聚合物; 以及易受含有通过该方法制备的乙烯基聚合物的氢化硅烷化的反应性组合物，并且每分子具有至少一个烯基。
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3.发明授权Process for producing vinyl polymer, vinyl polymer, and curable composition 有权制备乙烯基聚合物，乙烯基聚合物和可固化组合物的方法公开(公告)号：US07781534B2
公开(公告)日：2010-08-24
申请号：US11987469
申请日：2007-11-30
Applicant: Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
Inventor： Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
CPC classification number: C08F8/26 , C08F8/16 , C08F8/48 , C08F2810/30 , C08F2810/40 , Y10T436/196666
Abstract: The present invention provides: a process for preparing a vinyl polymer containing a halogen in an amount of 1,000 mg or less per kilogram, in which a vinyl polymer containing the halogen produced by atom transfer radical polymerization of a vinyl monomer is heated at a temperature in the range of 140 to 250° C. to dehalogenate the vinyl polymer; a vinyl polymer obtained by the process; and a hydrosilylation-reactive curable composition containing the vinyl polymer.
Abstract translation: 本发明提供了一种制备乙烯基聚合物的方法，该乙烯基聚合物含有每千克1,000mg以下的卤素，其中含有通过乙烯基单体的原子转移自由基聚合产生的卤素的乙烯基聚合物在温度为 范围为140至250℃，以使乙烯基聚合物脱卤; 通过该方法获得的乙烯基聚合物; 和含有乙烯基聚合物的氢化硅烷化反应性固化组合物。
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Patent Agency Ranking
公开(公告)号：US20050014912A1
公开(公告)日：2005-01-20
申请号：US10491187
申请日：2002-10-17
Applicant: Akihisa Hirota , Kosuke Tanaka , Shigeru Hagimori , Yosuke Asai , Naoki Furukawa , Masanao Takeda , Nao Fujita , Yoshiki Nakagawa
Inventor： Akihisa Hirota , Kosuke Tanaka , Shigeru Hagimori , Yosuke Asai , Naoki Furukawa , Masanao Takeda , Nao Fujita , Yoshiki Nakagawa
CPC classification number: C08F6/02 , C08F8/06 , C08F2438/01 , C08F2810/30 , C08F2810/40 , C08F8/26 , C08F120/18 , C08F2220/1808 , C08F2220/1825 , C08F2220/281
Abstract: The present invention provides a method for producing a vinyl polymer including the steps of polymerizing a vinyl monomer by atom transfer radical polymerization with a transition metal complex as a polymerization catalyst, and bringing the resultant vinyl polymer into contact with an adsorbent in the presence of an oxidizing agent; the vinyl polymer produced by the method; and a reactive composition susceptible to hydrosilylation containing the vinyl polymer produced by the method and having at least one alkenyl group per molecule.
Abstract translation: 本发明提供一种乙烯基聚合物的制造方法，包括以下步骤：用过渡金属络合物作为聚合催化剂通过原子转移自由基聚合使乙烯基单体聚合，并使所得到的乙烯基聚合物与吸附剂接触， 氧化剂; 通过该方法制备的乙烯基聚合物; 以及易受含有通过该方法制备的乙烯基聚合物的氢化硅烷化的反应性组合物，并且每分子具有至少一个烯基。
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公开(公告)号：US20070191589A1
公开(公告)日：2007-08-16
申请号：US10576895
申请日：2004-10-08
Applicant: Akihisa Hirota
Inventor： Akihisa Hirota
IPC: C08F6/00
CPC classification number: C08L53/00 , C08J3/12 , C08J3/122 , C08J2353/00 , C08L2666/02
Abstract: A simple method for producing a powder comprising a thermoplastic elastomer composition suitable for powder slush molding is provided. This is achieved by means of a method for producing powder for slush molding obtained by pulverization of a thermoplastic elastomer, characterized in that pulverization is performed by means of the shearing action of a fixed blade and a rotating blade. In particular, a specific acrylic block copolymer and a composition thereof can be favorably used for the thermoplastic elastomer composition.
Abstract translation: 提供了一种制备粉末的简单方法，其包括适用于粉末搪塑的热塑性弹性体组合物。 这是通过粉碎热塑性弹性体得到的搪塑成型粉末的方法实现的，其特征在于，通过固定刀片和旋转刀片的剪切作用进行粉碎。 特别地，特别的丙烯酸类嵌段共聚物及其组合物可有利地用于热塑性弹性体组合物。
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6.发明申请Process for producing vinyl polymer, vinyl polymer, and curable composition 有权制备乙烯基聚合物，乙烯基聚合物和可固化组合物的方法公开(公告)号：US20080160621A1
公开(公告)日：2008-07-03
申请号：US11987469
申请日：2007-11-30
Applicant: Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
Inventor： Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shigeki Ono , Nao Fujita
IPC: G01N33/00 , C08F130/08
CPC classification number: C08F8/26 , C08F8/16 , C08F8/48 , C08F2810/30 , C08F2810/40 , Y10T436/196666
Abstract: The present invention provides: a process for preparing a vinyl polymer containing a halogen in an amount of 1,000 mg or less per kilogram, in which a vinyl polymer containing the halogen produced by atom transfer radical polymerization of a vinyl monomer is heated at a temperature in the range of 140 to 250° C. to dehalogenate the vinyl polymer; a vinyl polymer obtained by the process; and a hydrosilylation-reactive curable composition containing the vinyl polymer.
Abstract translation: 本发明提供了一种制备乙烯基聚合物的方法，该乙烯基聚合物含有每千克1,000mg以下的卤素，其中含有通过乙烯基单体的原子转移自由基聚合产生的卤素的乙烯基聚合物在温度为 范围为140至250℃，以使乙烯基聚合物脱卤; 通过该方法获得的乙烯基聚合物; 和含有乙烯基聚合物的氢化硅烷化反应性固化组合物。
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7.发明申请Process for producing vinyl polymer, vinyl polymer, and curable composition 失效制备乙烯基聚合物，乙烯基聚合物和可固化组合物的方法公开(公告)号：US20050090622A1
公开(公告)日：2005-04-28
申请号：US10501023
申请日：2003-01-21
Applicant: Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shogeki Ono , Nao Fujita
Inventor： Kenichi Kitano , Akihisa Hirota , Masanao Takeda , Kosuke Tanaka , Yoshiki Nakagawa , Shigeru Hagimori , Naoki Furukawa , Shogeki Ono , Nao Fujita
CPC classification number: C08F8/26 , C08F8/16 , C08F8/48 , C08F2810/30 , C08F2810/40 , Y10T436/196666
Abstract: The present invention provides: a process for preparing a vinyl polymer containing a halogen in an amount of 1,000 mg or less per kilogram, in which a vinyl polymer containing the halogen produced by atom transfer radical polymerization of a vinyl monomer is heated at a temperature in the range of 140 to 250° C. to dehalogenate the vinyl polymer; a vinyl polymer obtained by the process; and a hydrosilylation-reactive curable composition containing the vinyl polymer.
Abstract translation: 本发明提供了一种制备乙烯基聚合物的方法，该乙烯基聚合物含有每千克1,000mg以下的卤素，其中含有通过乙烯基单体的原子转移自由基聚合产生的卤素的乙烯基聚合物在温度为 范围为140至250℃，以使乙烯基聚合物脱卤; 通过该方法获得的乙烯基聚合物; 和含有乙烯基聚合物的氢化硅烷化反应性固化组合物。
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公开(公告)号：US06187977B1
公开(公告)日：2001-02-13
申请号：US09300406
申请日：1999-04-27
Applicant: Takahiro Ohishi , Takeshi Kawamura , Akihisa Hirota , Takuya Maeda , Hiroshi Tsuneishi , Shun Wachi
Inventor： Takahiro Ohishi , Takeshi Kawamura , Akihisa Hirota , Takuya Maeda , Hiroshi Tsuneishi , Shun Wachi
IPC: C07C1700
CPC classification number: C07C17/392 , C07B39/00 , C07C17/10 , C07C17/14 , C07C22/04
Abstract: The present invention thus provides a process for producing (D) a chlorinated hydrocarbon compound of the general formula (2): CnR1mHk(CR2R3Cl)j (2) [wherein n is an integer of 1 to 12, m and k each independently is an integer of 0 to 25, j is an integer of 1 to 10; R1 represents an atom selected from the group consisting of chlorine, bromine, iodine, oxygen, nitrogen, sulfur and phosphorus and, when m is 2 or more, the two or more R1 groups may be the same or different, the group CnR1mHk having a valence of j does not contain any tertiary carbon-hydrogen bond; and R2 and R3 each independently represents a saturated aliphatic hydrocarbon group containing 1 to 5 carbon atoms or a group derived therefrom by substitution of a halogen atom or atoms for some hydrogen atom or atoms thereof and not containing a tertiary carbon-hydrogen bond],which process comprises adding (C) a protic acid to a mixture of (A) a compound of the general formula: CnR1mHk(CHR2R3)j (1) [wherein m, n, k, j, R1, R2 and R3 are as defined above] and (B) an aqueous solution of a metal hypochlorite.
Abstract translation: 因此，本发明提供了（D）通式（2）的氯化烃化合物的制备方法：[其中n为1〜12的整数，m和k各自独立地为0〜25的整数，j为 1〜10的整数; R1表示选自氯，溴，碘，氧，氮，硫和磷的原子，当m为2以上时，两个以上的R 1基可以相同或不同，具有 j的化合价不含任何叔碳 - 氢键; R 2和R 3各自独立地表示含有1〜5个碳原子的饱和脂肪族烃基或者通过卤素原子或原子取代一部分氢原子或不含叔碳氢键而衍生的基团]，其中 方法包括向（A）通式为[其中m，n，k，j，R1，R2和R3定义如上]的化合物的混合物中加入（C）质子酸，和（B）水溶液 的金属次氯酸盐。
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