Method of sintering materials with microwave radiation
    2.
    发明授权
    Method of sintering materials with microwave radiation 失效
    用微波辐射烧结材料的方法

    公开(公告)号:US5321223A

    公开(公告)日:1994-06-14

    申请号:US781781

    申请日:1991-10-23

    IPC分类号: H05B6/64

    CPC分类号: H05B6/64

    摘要: A method of sintering ceramic materials following: A compacted article comprising inorganic particles coated with carbon is provided, the carbon providing improved microwave coupling. The compacted article is then heated by microwave radiation to a temperature and for a period of time sufficient to sinter the compacted article.

    摘要翻译: 烧结陶瓷材料的方法如下:提供包含碳覆盖的无机颗粒的压实制品,所述碳提供改进的微波耦合。 然后将压实制品通过微波辐射加热到足以烧结压实制品的温度和一段时间。

    Water-insoluble high temperature ink
    3.
    发明授权
    Water-insoluble high temperature ink 失效
    水不溶性高温油墨

    公开(公告)号:US5055137A

    公开(公告)日:1991-10-08

    申请号:US448510

    申请日:1989-12-11

    摘要: A composition to produce an adherent and water insoluble deposit on substrate surfaces. A coating material for these surfaces is described which can be applied at any temperature up to at least 2000 degrees F., with the resultant deposit being highly adherent and water insoluble after short drying times. This coating has a liquid phase formed from at least water, a pre-reacted lithium silicate, and a pre-reacted potassium silicate. It can also contain a sodium silicate. This coating can be expressed as being about 69 to about 79 wt. % water and about 21 to about 31 wt. % a mixture of R.sub.2 O and SiO.sub.2. The R.sub.2 O is selected from either a mixture of Li.sub.2 O and K.sub.2 O or from a mixture of Li.sub.2 O, K.sub.2 O and Na.sub.2 O. The R.sub.2 O and SiO.sub.2 typically have a molar ratio of about 0.24 to about 0.29, and the K.sub.2 O is about 35 to 85% of the total molar amount of the R.sub.2 O. When Na.sub.2 O is present, it is up to about 10% of the total molar amount of the R.sub.2 O. To this liquid phase is added a suitable pigment or other refractory material, at about 6-80 wt. % based upon the liquid phase. A range of compositions is discussed as well as typical results.

    摘要翻译: 在基材表面上产生粘附和水不溶性沉积物的组合物。 描述了用于这些表面的涂料,其可以在至多2000华氏度的任何温度下施用,所得沉积物在短时间后具有高粘附性和水不溶性。 该涂层具有由至少水,预反应的硅酸锂和预反应的硅酸钾形成的液相。 它也可以含有硅酸钠。 该涂层可以表示为约69-约79wt。 %水和约21至约31wt。 %是R2O和SiO2的混合物。 R2O选自Li2O和K2O的混合物或Li2O,K2O和Na2O的混合物。 R 2 O和SiO 2通常具有约0.24至约0.29的摩尔比,K 2 O为R 2 O的总摩尔量的约35至85%。 当存在Na 2 O时,其高达R 2 O的总摩尔量的约10%。 向该液相中加入合适的颜料或其它耐火材料,约6-80wt。 基于液相的%。 讨论了一系列组成以及典型的结果。

    Binder/suspension composition yielding water insolubility alone or with
additives
    4.
    发明授权
    Binder/suspension composition yielding water insolubility alone or with additives 失效
    粘合剂/悬浮液组合物单独或与添加剂产生水不溶性

    公开(公告)号:US4810300A

    公开(公告)日:1989-03-07

    申请号:US189352

    申请日:1988-05-02

    IPC分类号: C09D11/16 C09D1/00

    CPC分类号: C09D11/16

    摘要: A composition to produce an adherent and water insoluble deposit on substrate surfaces. A coating material for these surfaces is described which can be applied at any temperature up to at least 2,000 degrees Fahrenheit, with the resultant deposit (after drying) being highly adherent and water insoluble. This coating has a liquid phase formed from at least water, a pre-reacted lithium silicate, and unreacted lithium hydroxide monohydrate. Preferably, the liquid phase contains a dispersent in the form of a clay, for example. Typically the pre-reacted Li.sub.2 O-SiO.sub.2 has a SiO.sub.2 :Li.sub.2 O molar ratio of about 4.6:1, and the unreacted LiOH.H.sub.2 O provides from 1/3 to 2/3 the total lithium oxide content, giving a final SiO:Li.sub.2 O molar ratio of the composition of from about 1.71:1 to about 2.97:1. To this liquid phase is added a suitable pigment or other refractory material, at about 6-80 wt % based upon the liquid phase. A range of compositions is discussed as well as typical results. This includes graphite, oxides, borides, nitrides, carbides, sulfides, metals and mixtures thereof. The particular refractory material must be stable in the highly basic condition of the liquid phase.

    摘要翻译: 在基材表面上产生粘附和水不溶性沉积物的组合物。 描述了用于这些表面的涂层材料,其可以在至多2000华氏度的任何温度下施加,所得沉积物(干燥后)具有高粘附性和水不溶性。 该涂层具有由至少水,预反应的硅酸锂和未反应的氢氧化锂一水合物形成的液相。 优选地,液相例如含有粘土形式的分散体。 通常,预反应的Li 2 O-SiO 2的SiO 2 :Li 2 O摩尔比为约4.6:1,未反应的LiOH·H 2 O的总氧化锂含量为1/3〜2/3,得到最终的SiO:Li 2 O摩尔比 的组成为约1.71:1至约2.97:1。 在该液相中加入合适的颜料或其它耐火材料,其量约为基于液相的约6-80重量%。 讨论了一系列组成以及典型的结果。 这包括石墨,氧化物,硼化物,氮化物,碳化物,硫化物,金属及其混合物。 特定的耐火材料必须在液相的高碱性条件下是稳定的。

    Binder/suspension composition and method of preparation thereof
    5.
    发明授权
    Binder/suspension composition and method of preparation thereof 失效
    粘合剂/悬浮液组合物及其制备方法

    公开(公告)号:US4769074A

    公开(公告)日:1988-09-06

    申请号:US128808

    申请日:1987-12-04

    摘要: A binder/suspension liquid for use with refractory compounds and the like. Oxidation prevention coatings for up to at least 1000 degrees Centigrade are described. Both a graphite non-conductive and a conductive coating are described for use in coating graphite crucibles, graphite electrodes, and the like. Typical compositions utilize a binder/suspension liquid phase in an amount from about 40 to about 55 wt. % of the total paintable mixture. This binder/suspension liquid phase is formed by intimately mixing colloidal silica solution, mono-aluminum phosphate solution and alcohol. The non-conducting embodiment of the graphite coating is produced by mixing finely divided boric acid and silicon carbide with the binder/suspension liquid phase. The preferred conductive coating substitutes a mixed TiC-SiC for the SiC of the non-conductive embodiment. The resultant material is very stable (i.e., does not settle), is paintable upon the graphite, and is easily dried at or near room temperature. A few thin coats, with drying between applications, totaling only about 0.15 to about 0.23 mm prevents detrimental oxidation through several cycles to at least 1000 degrees C. Other applications of the binder/suspension agent are discussed.

    摘要翻译: 用于耐火化合物等的粘合剂/悬浮液。 描述了高达至少1000摄氏度的防氧化涂层。 描述了石墨非导电和导电涂层,用于涂覆石墨坩埚,石墨电极等。 典型的组合物使用约40至约55重量%的量的粘合剂/悬浮液相。 总可涂漆混合物的%。 该粘合剂/悬浮液相通过将胶态二氧化硅溶液,一磷酸铝溶液和醇充分混合而形成。 通过将细碎的硼酸和碳化硅与粘合剂/悬浮液相混合来制造石墨涂层的非导电性实施方案。 优选的导电涂层代替混合的TiC-SiC用于非导电实施例的SiC。 所得材料非常稳定(即不沉降),可在石墨上涂漆,并且容易在室温或室温下干燥。 在涂覆之间干燥的几层薄涂层,总共只有约0.15至约0.23毫米,防止有害氧化几个循环至至少1000摄氏度。讨论了粘合剂/悬浮剂的其他应用。

    Process for removing carbon from uranium
    6.
    发明授权
    Process for removing carbon from uranium 失效
    从铀中除去碳的工艺

    公开(公告)号:US3985551A

    公开(公告)日:1976-10-12

    申请号:US660907

    申请日:1976-02-24

    IPC分类号: C22B60/02

    CPC分类号: C22B60/0286

    摘要: Carbon contamination is removed from uranium and uranium alloys by heating in inert atmosphere to 700.degree.-1900.degree.C in effective contact with yttrium to cause carbon in the uranium to react with the yttrium. The yttrium is either in direct contact with the contaminated uranium or in indirect contact by means of an intermediate transport medium.

    摘要翻译: 通过在惰性气氛中加热至700°-1900℃,与钇有效接触,从铀和铀合金中除去碳污染物,使铀中的碳与钇反应。 钇与污染的铀直接接触或通过中间运输介质间接接触。

    Directly susceptible, noncarbon metal ceramic composite crucible
    7.
    发明授权
    Directly susceptible, noncarbon metal ceramic composite crucible 失效
    直接易受非碳金属陶瓷复合坩埚

    公开(公告)号:US5997802A

    公开(公告)日:1999-12-07

    申请号:US199313

    申请日:1998-11-25

    IPC分类号: B22D41/00 F27B14/06 F27B14/10

    摘要: A sintered metal ceramic crucible suitable for high temperature induction melting of reactive metals without appreciable carbon or silicon contamination of the melt. The crucible comprises a cast matrix of a thermally conductive ceramic material; a perforated metal sleeve, which serves as a susceptor for induction heating of the crucible, embedded within the ceramic cast matrix; and a thermal-shock-absorber barrier interposed between the metal sleeve and the ceramic cast matrix to allow for differential thermal expansions between the matrix and the metal sleeve and to act as a thermal-shock-absorber which moderates the effects of rapid changes of sleeve temperature on the matrix.

    摘要翻译: 一种适用于高温感应熔化反应性金属的烧结金属陶瓷坩埚,而熔体无明显的碳或硅污染。 坩埚包括导热陶瓷材料的铸造基体; 穿孔金属套筒,其用作嵌入在陶瓷浇铸基体内的用于坩埚感应加热的基座; 以及插入在金属套管和陶瓷浇铸基体之间的热冲击吸收器屏障,以允许基体和金属套筒之间的热膨胀差异,并且作为减轻套筒快速变化影响的热冲击吸收器 基体上的温度。

    Boron nitride-containing bodies and method of making the same
    8.
    发明授权
    Boron nitride-containing bodies and method of making the same 失效
    含氮化硼的体及其制造方法

    公开(公告)号:US5320989A

    公开(公告)日:1994-06-14

    申请号:US986548

    申请日:1992-12-07

    IPC分类号: C04B38/00 C04B35/58

    CPC分类号: C04B38/00

    摘要: A relatively chemically inert ceramic material produced from a clay-like mixture of boron nitride powder and aluminum oxide, where the aluminum oxide is derived from colloidal aluminum oxide, peptized aluminum oxide, or a dissolved aluminum salt. The clay-like mixture can be dried in a near net shape without cracking and then pressure-less sintered, or bulk dried. Alternatively, pressure-less sintered bodies can be easily machined to a given shape. The ceramic has properties very similar to those of boron nitride in that it resists damage from molten materials, has a high electrical resistance, has high strength at ambient and elevated temperatures, etc. A typical pressure-less sintered body is formed from a clay made with finely-divided boron nitride mixed with at least one of the listed sources of aluminum oxide such that the final sintered composition contains about 85 wt. % boron nitride.

    摘要翻译: 由氮化硼粉末和氧化铝的粘土状混合物制备的相对化学惰性的陶瓷材料,其中氧化铝源自胶体氧化铝,胶溶的氧化铝或溶解的铝盐。 粘土状混合物可以以近净形状干燥而不破裂,然后无压烧结或大量干燥。 或者,无压烧结体可以容易地加工成给定的形状。 该陶瓷具有与氮化硼非常相似的性质,因为它抵抗熔融材料的损伤,具有高电阻,在环境温度和高温下具有高强度等。典型的无压烧结体由粘土制成 其中细碎的氮化硼与所列出的氧化铝源中的至少一个混合,使得最终的烧结组合物含有约85wt。 %氮化硼。

    N-propyl bromide solvent systems
    9.
    发明授权
    N-propyl bromide solvent systems 有权
    N-丙基溴溶剂体系

    公开(公告)号:US09260595B1

    公开(公告)日:2016-02-16

    申请号:US14468443

    申请日:2014-08-26

    摘要: A solvent composition and system is disclosed having a composition including n-propyl bromide and a propionate containing liquid and/or a butyrate containing liquid. The solvent system may include approximately 35 to 92.5 weight percent propionate containing liquid and approximately 7.5 to 65 weight percent n-propyl bromide. Alternatively, the solvent system may include approximately 40 to 85 weight percent butyrate containing liquid and 15 to 60 weight percent n-propyl bromide. The solvent system may incorporate a polymer, such as a synthetic rubber polymer. Further the solvent system preferably has high solvency while maintaining desirable evaporation rates and is preferably nonflammable, combustible, or minimally a class IC flammable liquid.

    摘要翻译: 公开了具有包含正丙基溴和含有液体和/或含丁酸酯的液体的丙酸酯的组合物的溶剂组合物和体系。 溶剂系统可以包含约35至92.5重量%的含丙酸酯的液体和约7.5至65重量%的正丙基溴。 或者,溶剂系统可以包括约40至85重量%的含丁酸的液体和15至60重量%的正丙基溴。 溶剂系统可以加入聚合物,例如合成橡胶聚合物。 此外,溶剂体系优选具有高溶解性,同时保持理想的蒸发速率,并且优选是不可燃,可燃或最低限度的IC类可燃性液体。