摘要:
Alkylene oxide polymers and copolymers of excellent thermal stability are prepared by reacting (1) alkylene oxides, (2) amines, (3) organozinc compounds and (4) water, at an elevated temperature. In the process
摘要:
1. A PROCESS FOR PREPARING METHACRYLATE ESTER OF MULTIBROMINATED PHENOL DERIVATIVE, WHICH COMPRISES REACTING A COMPOUND OF THE FORMULA:
((H)K-),((BR)N-),((H3C)M-)-PHENOL
WHEREIN N IS INTEGER 3, 4 OR 5M M IS AN INTEGER 0, 1 OR 2, K IS AN INTEGER 0, 1 OR 2, AND N+N+K=5, WITH METHACRYLIC ACID CHLORIDE IN THE PRESENCE OF A PYRIDINE BASE AT A TEMPERATURE IN THE RANGE OF 100 TIO 160*C.
摘要:
PROPANESULTONE IS STABILIZED BY ADDING AT LEAST ONE COMPOUND SELECTED FROM THE GROUP CONSISTING OF ALIPHATIC AMINES, ALICYCLIC AMINES, ARALKYLAMINES, NON-AROMATIC CYCLIC AMINES, N-ALKYL-SUBSTITUTED AROMATIC AMINES, AMINOALCOHOLS AMINE CHARACTER NITROGEN CONTAINING CARBOXYLIC ACIDS HAVING 2 TO 10 CARBON ATOMS AND THEIR ESTERS, AMIDES, PYRIDINES, QUINOLINES, AND REACTION PRODUCTS OF THESE COMPOUNDS WITH PROPANESULTONE.
摘要:
A PROCESS FOR PREPARING PROPANE SULTONE FROM A HYDROXYPROPANE SULFONIC ACID CONTAINING SOLUTION WHICH IS CHARACTERIZED BY CONCENTRATING THE SOLUTION UNTIL THE CONCENTRATION RATIO WITHIN A SPECIFIC RANGE IS REACHED AND THEN SUBJECTING THE OBTAINED CONCENTRATED SOLUTION TO A CONTINUOUS DISTILLATION IN AN AGITATED-FILM EVAPORATOR UNDER A HIGH VACUUM OF LOWER THAN 15 MM. HG TO DISTILL AND RECOVER PROPANE SULTONE.
摘要:
A process for modifying cellulose acetate by treating an object made of a mixed ester of cellulose and (1) acetic acid and (2) a polybasic carboxylic acid, i.e., a dibasic carboxylic acid and/or tribasic carboxylic acid, with a divalent or higher metal salt to impart solvent resistance to the object.
摘要:
A SURFACTANT IS ADDED TO AN AQUEOUS PROTEIN SOLUTION UNDERGOING PURIFICATION OR CONCENTRATION USING A SEMIPERMEABLE MEMBRANE, IN ORDER TO IMPROVE THE WATER PERMEATION RATE OF THE MEMBRANE.
摘要:
SUSPENSION POLYMERIZATION OF A STYRENE-ACRYLONITRILE POLYMERIZATION MIXTURE IS CARRIED OUT WHILE ADDING STYRENE TO THE POLYMERIZATION MIXTURE UNTIL THE CONVERSION OF MONOMERS TO COPOLYMER REACHES 40 TO 70%. AN INERT GAS IS PASSED THROUGH THE POLYMERIZATION SYSTEM AFTER THE CONVERSION HAS REACHED 75 TO 85% TO REMOVE EXCESS ACRYLONITRILE, WHEREBY THERE IS OBTAINED A STYRENE-ACRYLONITRILE COPOLYMER HAVING A UNIFORM HOMOGENOUS COMPOSITION.
摘要:
A process for manufacturing 3,3,5-trimethylcyclohexyl mandelate in which mandelic acid is esterified with 3,3,5trimethylcyclohexanol in an inert solvent in the presence of an acid catalyst, in which a metal (Zn, Sn, Mg, Ni or Pb) is added to the reaction system at the beginning of or during the reaction, or afterwards, to generate ketone-reductive hydrogen in situ in order to minimize formation of 3,3,5trimethylcyclohexylphenylglyoxylate.
摘要:
3-HYDROXY-2-METHYL-4-PYRONE (MALTOL) IS PREPARED BY (1) REACTING Beta , delta -DIOXOCAPROALDEHYDE DIALKYL ACETAL WITH LEAD TETRAACETATE, (2) EITHER (A) PYROLYZING THE PRODUCT OF STEP (1), OR (B) TREATING THE SAME WITH AN ACID CONDENSING AGENT, AND (3) HYDROLYZING THE PRODUCT OF STEP (2) EITHER SIMULTANEOUSLY THEREWITH OR SUBSEQUENTLY. Beta , delta -DIOXOCAPROALDEHYDE IS PREPARED BY REACTING LOWER ALKYL Beta -DIALKOXYPROPIONATES WITH ACETONE UNDER CONDITIONS SUITABLE TO EFFECT THE Claisen condensation reaction.