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公开(公告)号：US10309158B2
公开(公告)日：2019-06-04
申请号：US12961787
申请日：2010-12-07
Applicant: Debkumar Mukhopadhyay , Kenneth E. Bertagnolli , Jair J. Gonzalez
Inventor： Debkumar Mukhopadhyay , Kenneth E. Bertagnolli , Jair J. Gonzalez
IPC: E21B10/55 , B22F7/06 , B24D3/10 , C22C26/00 , E21B10/567 , E21B10/573 , B22F5/00
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact (“PDC”) includes forming a polycrystalline diamond (“PCD”) table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The PCD table includes bonded diamond grains defining interstitial regions, with the metal-solvent catalyst disposed therein. The method includes at least partially leaching the PCD table to remove at least a portion of the metal-solvent catalyst therefrom. The method includes subjecting the at least partially leached PCD table and a substrate to a second HPHT process under diamond-stable temperature-pressure conditions to partially infiltrate the at least partially leached PCD table with an infiltrant. A maximum temperature (T), a total process time (t), and a maximum pressure (P) of the second HPHT process are chosen so that β is about 2° Celsius·hours/gigapascals (“° C.·h/GPa”) to about 325° C.·h/GPa, with β represented as β=T·t/P.
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2.发明授权Polycrystalline diamond compacts, methods of making same, and applications therefor 有权多晶金刚石压块，其制造方法及其应用公开(公告)号：US08727045B1
公开(公告)日：2014-05-20
申请号：US13033436
申请日：2011-02-23
Applicant: Debkumar Mukhopadhyay , Kenneth E. Bertagnolli
Inventor： Debkumar Mukhopadhyay , Kenneth E. Bertagnolli
IPC: E21B10/36 , E21B10/567
CPC classification number: E21B10/573 , B22F7/062 , C22C26/00
Abstract: Embodiments of the invention relate to polycrystalline diamond compact (“PDC”) including a polycrystalline diamond (“PCD”) table that bonded to a cobalt-nickel alloy cemented carbide substrate. The cobalt-nickel alloy cemented carbide substrate provides both erosion resistance and corrosion resistance to the cemented carbide substrate. In an embodiment, a PDC includes a cemented carbide substrate including cobalt-nickel alloy cementing constituent. The PDC further includes a PCD table bonded to the cemented carbide substrate.
Abstract translation: 本发明的实施方案涉及包含结合到钴 - 镍合金硬质合金基底的多晶金刚石（“PCD”）表的多晶金刚石致密体（“PDC”）。 钴 - 镍合金硬质合金基体为硬质合金基体提供耐腐蚀性和耐腐蚀性。 在一个实施方案中，PDC包括包含钴 - 镍合金胶结成分的硬质合金基底。 PDC还包括结合到硬质合金基底的PCD台。
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3.发明申请POLYCRYSTALLINE DIAMOND COMPACTS, RELATED PRODUCTS, AND METHODS OF MANUFACTURE 有权多晶金刚石复合材料，相关产品及其制造方法公开(公告)号：US20130092451A1
公开(公告)日：2013-04-18
申请号：US13275372
申请日：2011-10-18
Applicant: Debkumar Mukhopadhyay , Jair J. Gonzalez
Inventor： Debkumar Mukhopadhyay , Jair J. Gonzalez
CPC classification number: B24D3/06 , B01J3/062 , B01J2203/062 , B01J2203/0655 , B01J2203/0685 , B24D18/0009 , B24D99/005 , E21B10/46 , E21B10/56
Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) and methods of manufacturing such PDCs in which an at least partially leached polycrystalline diamond (“PCD”) table is infiltrated with a low viscosity cobalt-based alloy infiltrant. In an embodiment, a method includes forming a PCD table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The method includes at least partially leaching the PCD table to remove at least a portion of the metal-solvent catalyst therefrom to form an at least partially leached PCD table. The method includes subjecting the at least partially leached PCD table and a substrate to a second HPHT process effective to at least partially infiltrate the at least partially leached PCD table with a cobalt-based alloy infiltrant having a composition at or near a eutectic composition of the cobalt-based alloy infiltrant.
Abstract translation: 实施例涉及多晶金刚石压块（“PDC”）以及制造这样的PDC的方法，其中至少部分浸出的多晶金刚石（“PCD”）工作台用低粘度钴基合金渗透剂渗透。 在一个实施方案中，一种方法包括在第一高压/高温（“HPHT”）方法中在金属溶剂催化剂存在下形成PCD表。 该方法包括至少部分浸出PCD表以从其中除去至少一部分金属 - 溶剂催化剂以形成至少部分浸出的PCD台。 该方法包括使至少部分浸出的PCD台和基板经受有效的至少部分浸渗的PCD台的第二HPHT方法，所述第二HPHT工艺具有钴基合金浸渗剂，所述钴基合金浸渗剂具有或接近共晶组成 钴基合金浸润剂。
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4.发明授权Polycrystalline diamond compacts, methods of making same, and applications therefor 有权多晶金刚石压块，其制造方法及其应用公开(公告)号：US08216677B2
公开(公告)日：2012-07-10
申请号：US12649784
申请日：2009-12-30
Applicant: Debkumar Mukhopadhyay , Kenneth E Bertagnolli , Jair J Gonzalez
Inventor： Debkumar Mukhopadhyay , Kenneth E Bertagnolli , Jair J Gonzalez
IPC: B32B9/00
CPC classification number: E21B10/573 , B01J3/062 , B01J2203/063 , B01J2203/0655 , B24D99/005 , C04B35/528 , C04B2235/3847 , C04B2237/36 , C04B2237/363 , C04B2237/555 , C22C19/07 , C22C29/08 , C22C2204/00 , E21B10/567 , E21B10/5735 , F16C33/043 , F16C2352/00 , Y10T428/30
Abstract: In an embodiment, a polycrystalline diamond compact (“PDC”) comprises a cemented carbide substrate including a first cemented carbide portion exhibiting a first concentration of chromium carbide and a second cemented carbide portion bonded to the first cemented carbide portion and exhibiting a second concentration of chromium carbide that is greater than the first concentration. The PDC further comprises a polycrystalline diamond (“PCD”) table bonded to the first cemented carbide portion. The PCD table includes a plurality of bonded diamond grains exhibiting diamond-to-diamond bonding therebetween, with the plurality of bonded diamond grains defining a plurality of interstitial regions. The PCD table includes chromium present in a concentration less than about 0.25 weight %.
Abstract translation: 在一个实施例中，多晶金刚石复合体（“PDC”）包括硬质合金基体，该硬质合金基体包括表现出第一浓度的碳化铬的第一硬质合金部分和与第一硬质合金部分结合的第二硬质合金部分， 大于第一浓度的碳化铬。 PDC还包括结合到第一硬质合金部分的多晶金刚石（“PCD”）台。 PCD表包括多个结合的金刚石晶粒，其间形成金刚石 - 金刚石结合，多个结合的金刚石晶粒限定多个间隙区域。 PCD表包括以小于约0.25重量％的浓度存在的铬。
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5.发明授权Polycrystalline diamond, polycrystalline diamond compacts, methods of making same, and applications 有权多晶金刚石，多晶金刚石压块，制造方法及应用公开(公告)号：US09315881B2
公开(公告)日：2016-04-19
申请号：US13486578
申请日：2012-06-01
Applicant: Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
Inventor： Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
CPC classification number: B24D3/10 , B22F2005/001 , C22C26/00 , E21B10/567 , F16C33/043 , F16C2352/00
Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDC”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, a PDC includes a polycrystalline diamond (“PCD”) table bonded to a substrate. At least a portion of the PCD table includes a plurality of diamond grains defining a plurality of interstitial regions. The plurality of interstitial regions includes a metal-solvent catalyst. The plurality of diamond grains exhibit an average grain size of about 30 μm or less. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit an average electrical conductivity of less than about 1200 S/m. Other embodiments are directed to PCD, employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
Abstract translation: 本发明的实施方案涉及显示增强的金刚石到金刚石结合的多晶金刚石压块（“PDC”）。 在一个实施例中，PDC包括结合到衬底的多晶金刚石（“PCD”）表。 PCD表的至少一部分包括限定多个间隙区域的多个金刚石晶粒。 多个间隙区域包括金属 - 溶剂催化剂。 多个金刚石晶粒的平均粒径为30μm以下。 多个金刚石晶粒和金属 - 溶剂催化剂共同表现出小于约1200S / m的平均导电率。 其他实施例涉及PCD，采用这种PCD，形成PCD和PDC的方法，以及用于旋转钻头，轴承装置和拉丝模具中的这种PCD和PDC的各种应用。
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Patent Agency Ranking
6.发明授权公开(公告)号：US09027675B1
公开(公告)日：2015-05-12
申请号：US13100388
申请日：2011-05-04
Applicant: Paul Douglas Jones , Kenneth E. Bertagnolli , Debkumar Mukhopadhyay , David P. Miess
Inventor： Paul Douglas Jones , Kenneth E. Bertagnolli , Debkumar Mukhopadhyay , David P. Miess
CPC classification number: E21B10/46 , B24D3/02 , B24D3/06 , B24D99/005 , E21B10/56 , E21B10/5676
Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDCs”) comprising a polycrystalline diamond (“PCD”) table including at least a portion having aluminum carbide disposed interstitially between bonded-together diamond grains thereof, and methods of fabricating such PDCs. In an embodiment, a PDC includes a substrate, and a PCD table bonded to the substrate. The PCD table includes a plurality of bonded-together diamond grains defining a plurality of interstitial regions. The PCD table further includes aluminum carbide disposed in at least a portion of the plurality of interstitial regions.
Abstract translation: 本发明的实施方案涉及包括多晶金刚石（“PCD”）台的多晶金刚石压块（“PDC”），其包括至少一部分具有间隙地设置在其结合的金刚石晶粒之间的碳化铝的部分和制造这种PDC的方法。 在一个实施例中，PDC包括基板和与基板结合的PCD台。 PCD表包括限定多个间隙区域的多个接合在一起的金刚石晶粒。 PCD表还包括设置在多个间隙区域的至少一部分中的碳化铝。
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7.发明授权Detection of one or more interstitial constituents in a polycrystalline diamond element by neutron radiographic imaging 有权通过中子射线成像检测多晶金刚石元件中的一个或多个间隙成分公开(公告)号：US08888879B1
公开(公告)日：2014-11-18
申请号：US13267026
申请日：2011-10-06
Applicant: Debkumar Mukhopadhyay , Kenneth E. Bertagnolli
Inventor： Debkumar Mukhopadhyay , Kenneth E. Bertagnolli
CPC classification number: G01N23/005 , B24D18/0009 , C04B41/009 , C04B41/5353 , C04B41/91 , G01N23/05 , G01N33/385 , G01N33/40 , C04B35/52
Abstract: In an embodiment, a method of non-destructively testing a polycrystalline diamond (“PCD”) element includes providing a PCD element including a plurality of bonded diamond grains defining a plurality of interstitial regions, at least a portion of the plurality of interstitial regions including one or more interstitial constituents disposed therein. The method further includes exposing the PCD element to neutron radiation from a neutron radiation source, receiving a portion of the neutron radiation that passes through the PCD element, and determining at least one characteristic of the PCD element at least partially based on the portion of the neutron radiation received. For example, the at least one characteristic may be the presence and distribution of metal-solvent catalyst, residual metal-solvent catalyst, an infiltrant, residual infiltrant, or other interstitial constituents within a PCD element.
Abstract translation: 在一个实施例中，一种非破坏性地测试多晶金刚石（“PCD”）元件的方法包括提供包括限定多个间隙区域的多个结合金刚石晶粒的PCD元件，所述多个间隙区域的至少一部分包括 设置在其中的一个或多个间质成分。 该方法还包括将PCD元件暴露于来自中子辐射源的中子辐射，接收穿过PCD元件的一部分中子辐射，以及至少部分地基于所述PCD元件的一部分来确定PCD元件的至少一个特性 收到中子辐射。 例如，至少一个特征可以是在PCD元件内金属溶剂催化剂，残余金属溶剂催化剂，浸润剂，残余浸润剂或其它间隙成分的存在和分布。
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公开(公告)号：US08764862B2
公开(公告)日：2014-07-01
申请号：US13457088
申请日：2012-04-26
Applicant: Brian Atkins , Seth G. Anderle , Robert W. Arfele , Ram L. Ladi , Brandon Paul Linford , Jason Keith Wiggins , Kevin Duy Nguyen , Jiang Qian , Kenneth Eugene Bertagnolli , Shawn Casey Scott , Debkumar Mukhopadhyay , Michael Alexander Vail
Inventor： Brian Atkins , Seth G. Anderle , Robert W. Arfele , Ram L. Ladi , Brandon Paul Linford , Jason Keith Wiggins , Kevin Duy Nguyen , Jiang Qian , Kenneth Eugene Bertagnolli , Shawn Casey Scott , Debkumar Mukhopadhyay , Michael Alexander Vail
CPC classification number: E21B10/5735
Abstract: The disclosure provides a super abrasive element containing a substantially catalyst-free thermally stable polycrystalline diamond (TSP) body having pores and a contact surface, a base adjacent the contact surface of the TSP body; and an infiltrant material infiltrated in the base and in the pores of the TSP body at the contact surface. The disclosure additionally provides earth-boring drill bits and other devices containing such super abrasive elements. The disclosure further provides methods and mold assemblies for forming such super abrasive elements via infiltration and hot press methods.
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9.发明申请POLYCRYSTALLINE DIAMOND, POLYCRYSTALLINE DIAMOND COMPACTS, METHODS OF MAKING SAME, AND APPLICATIONS 有权多晶金刚石，多晶金刚石复合材料，制备方法及应用公开(公告)号：US20120241226A1
公开(公告)日：2012-09-27
申请号：US13486578
申请日：2012-06-01
Applicant: Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
Inventor： Kenneth E. Bertagnolli , Jiang Qian , Jason K. Wiggins , Michael A. Vail , Debkumar Mukhopadhyay , Brandon P. Linford
CPC classification number: B24D3/10 , B22F2005/001 , C22C26/00 , E21B10/567 , F16C33/043 , F16C2352/00
Abstract: Embodiments of the invention relate to polycrystalline diamond compacts (“PDC”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, a PDC includes a polycrystalline diamond (“PCD”) table bonded to a substrate. At least a portion of the PCD table includes a plurality of diamond grains defining a plurality of interstitial regions. The plurality of interstitial regions includes a metal-solvent catalyst. The plurality of diamond grains exhibit an average grain size of about 30 μm or less. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit an average electrical conductivity of less than about 1200 S/m. Other embodiments are directed to PCD, employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.
Abstract translation: 本发明的实施方案涉及显示增强的金刚石到金刚石结合的多晶金刚石压块（“PDC”）。 在一个实施例中，PDC包括结合到衬底的多晶金刚石（“PCD”）表。 PCD表的至少一部分包括限定多个间隙区域的多个金刚石晶粒。 多个间隙区域包括金属 - 溶剂催化剂。 多个金刚石晶粒的平均粒径为30μm以下。 多个金刚石晶粒和金属 - 溶剂催化剂共同表现出小于约1200S / m的平均导电率。 其他实施例涉及PCD，采用这种PCD，形成PCD和PDC的方法，以及用于旋转钻头，轴承装置和拉丝模具中的这种PCD和PDC的各种应用。
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10.发明授权公开(公告)号：US08261858B1
公开(公告)日：2012-09-11
申请号：US13225134
申请日：2011-09-02
Applicant: Brian Atkins , Seth G. Anderle , Robert W. Arfele , Ram L. Ladi , Brandon Paul Linford , Jason Keith Wiggins , Kevin Duy Nguyen , Jiang Qian , Kenneth Eugene Bertagnolli , Shawn Casey Scott , Debkumar Mukhopadhyay , Michael Alexander Vail
Inventor： Brian Atkins , Seth G. Anderle , Robert W. Arfele , Ram L. Ladi , Brandon Paul Linford , Jason Keith Wiggins , Kevin Duy Nguyen , Jiang Qian , Kenneth Eugene Bertagnolli , Shawn Casey Scott , Debkumar Mukhopadhyay , Michael Alexander Vail
IPC: E21B10/46
CPC classification number: E21B10/5735
Abstract: The disclosure provides a super abrasive element containing a substantially catalyst-free thermally stable polycrystalline diamond (TSP) body having pores and a contact surface, a base adjacent the contact surface of the TSP body; and an infiltrant material infiltrated in the base and in the pores of the TSP body at the contact surface. The disclosure additionally provides earth-boring drill bits and other devices containing such super abrasive elements. The disclosure further provides methods and mold assemblies for forming such super abrasive elements via infiltration and hot press methods.
Abstract translation: 本公开提供了一种含有基本上无催化剂的热稳定多晶金刚石（TSP）体的超级研磨元件，其具有孔和接触表面，邻近TSP体的接触表面的基底; 以及在接触表面浸渍在TSP体的基体和孔中的渗透材料。 本公开另外提供了钻孔钻头和包含这种超级研磨元件的其它装置。 本公开进一步提供了通过渗透和热压法形成这种超级研磨元件的方法和模具组件。
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