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公开(公告)号：US08682620B2
公开(公告)日：2014-03-25
申请号：US12949851
申请日：2010-11-19
CPC分类号： B29C47/0859 , B29C33/3835 , B29C47/0002 , B29C47/0009 , B29C47/0854 , B29C47/14 , B29C47/92 , B29C2947/92514 , B29C2947/926 , B29C2947/92666 , B29C2947/92904
摘要： A method of designing a die cavity that may include performing a flow analysis using characteristics of a predetermined die cavity, density and rheological properties of a material, and a flow rate of the material to calculate the pressure distribution exerted on the die cavity and cross-sectional flow profile. The method further includes a structural analysis using the calculated pressure distribution and structural characteristics of the die cavity to calculate a deformed die cavity. The flow analysis is repeated using the characteristics of the deformed die cavity to calculate a pressure distribution exerted on the die cavity and cross-sectional flow profile. The outcome is compared to determine if the pressure distributions and/or cross-sectional flow profiles converge. These steps are iteratively repeated until convergence of the pressure and/or cross-sectional flow profile is observed. The variation of the cross-sectional flow profile is analyzed to determine if it is below a predetermined tolerance.
摘要翻译： 设计模腔的方法，其可以包括使用预定模腔的特性，材料的密度和流变特性以及材料的流速来执行流动分析，以计算施加在模腔上的压力分布， 截面流动剖面图。 该方法还包括使用计算的压模分布和模腔的结构特征来计算变形模腔的结构分析。 使用变形模腔的特征重复流动分析，以计算施加在模腔上的压力分布和横截面流动分布。 比较结果以确定压力分布和/或横截面流动剖面是否收敛。 迭代地重复这些步骤，直到观察到压力和/或横截面流动分布的收敛。 分析横截面流动剖面的变化以确定其是否低于预定的公差。
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2.发明授权Synthesis of polyol fatty acid polyesters using column with inert gas stripping 失效使用惰性气体剥离柱合成多元醇脂肪酸聚酯
公开(公告)号：US5945529A
公开(公告)日：1999-08-31
申请号：US683899
申请日：1996-07-19
CPC分类号： C07H13/06
摘要： Processes for the synthesis of polyol fatty acid polyester by transesterification of a polyol comprise reacting polyol with a first portion of fatty acid lower alkyl ester to provide a first step reaction product in which substantially all of the polyol is reacted with at least one fatty acid lower alkyl ester. The processes then employ a multistage column providing substantial plug flow of liquid therein for further transesterification of the first step reaction product. Partially esterified polyol, a second portion of fatty acid lower alkyl ester and catalyst are fed to the column to form a mixture and cause further transesterification of the partially esterified polyol and fatty acid lower alkyl ester, with lower alkyl alcohol being formed as a by product. The resulting liquid mixture of reactants and product is passed in a first direction between adjacent stages through the column for further reaction of partially esterified polyol with fatty acid lower alkyl ester. An inert stripping or sparging gas is fed through the column in a second direction between adjacent stages, counter current to the flow of the liquid mixture between adjacent stages in the first direction, with radial shear agitation. The lower alkyl alcohol by-product of the polyol-fatty acid lower alkyl ester reaction is transferred from the liquid mixture to the inert gas.
摘要翻译： 通过多元醇酯交换合成多元醇脂肪酸聚酯的方法包括使多元醇与脂肪酸低级烷基酯的第一部分反应，以提供第一步反应产物，其中基本上所有的多元醇与至少一种脂肪酸较低 烷基酯。 然后，该方法使用多级柱，其中提供液体的大量活塞流，用于第一步反应产物的进一步酯交换。 将部分酯化的多元醇，第二部分的脂肪酸低级烷基酯和催化剂加入到塔中以形成混合物，并使部分酯化的多元醇和脂肪酸低级烷基酯进一步酯交换反应，形成低级烷基醇作为副产物 。 所得到的反应物和产物的液体混合物在相邻级之间的第一方向通过柱，用于部分酯化的多元醇与脂肪酸低级烷基酯的进一步反应。 惰性汽提或喷射气体在相邻级之间的第二方向通过柱体进料，与径向剪切搅拌相反，在相邻级之间的液体混合物流在第一方向上。 多元醇 - 脂肪酸低级烷基酯反应的低级烷基醇副产物从液体混合物转移到惰性气体中。
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3.发明申请Continuous Process of Making an Article of Dissolution Upon Use to Deliver Surfactants 审中-公开在使用表面活性剂时制作溶出物的连续过程公开(公告)号：US20120270029A1
公开(公告)日：2012-10-25
申请号：US13440475
申请日：2012-04-05
申请人： Robert Wayne GLENN, JR. , Eric Paul Granberg , Todd Ryan Thompson , Ke-ming Quan , John Phillip Hecht , Jason Donald McCarty , Raul Victorino Nunes , Aleksey Mikhailovich Pinyayev
发明人： Robert Wayne GLENN, JR. , Eric Paul Granberg , Todd Ryan Thompson , Ke-ming Quan , John Phillip Hecht , Jason Donald McCarty , Raul Victorino Nunes , Aleksey Mikhailovich Pinyayev
CPC分类号： A61K8/0216 , A61K8/046 , A61K8/345 , A61K8/731 , A61K8/8129 , A61K2800/805 , A61Q5/02 , A61Q19/10 , B29B7/46 , B29C41/28 , B29C48/0022 , B29C48/08 , B29C48/14 , B29C48/762 , B29C48/793 , B29C48/91 , B29C48/92 , B29C67/202 , B29C2948/92695 , B29C2948/92704 , B29C2948/92723 , B29K2105/04 , C08J9/30 , C08J2201/03 , C08J2205/05 , Y10T428/249921
摘要： A continuous process for making a flexible porous dissolvable solid structure with open celled foam. The continuous process has the steps of preparing a pre-mixture comprising surfactant, polymer, water, and optionally plasticizer; aerating the pre-mixture to form a wet aerated pre-mixture; extruding the wet aerated pre-mixture to form one or more sheets on a belt; and drying the sheets to form an Article having an open celled foam.
摘要翻译： 用开孔泡沫制造柔性多孔可溶性固体结构的连续方法。 连续方法具有制备包含表面活性剂，聚合物，水和任选的增塑剂的预混物的步骤; 对预混合物充气以形成湿式充气预混合物; 挤压湿气预混合物以在带上形成一个或多个片材; 并干燥片材以形成具有开孔泡沫的制品。
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公开(公告)号：US20120130684A1
公开(公告)日：2012-05-24
申请号：US12949851
申请日：2010-11-19
IPC分类号： G06F17/50
CPC分类号： B29C47/0859 , B29C33/3835 , B29C47/0002 , B29C47/0009 , B29C47/0854 , B29C47/14 , B29C47/92 , B29C2947/92514 , B29C2947/926 , B29C2947/92666 , B29C2947/92904
摘要： A method of designing a die cavity can include performing a flow analysis using characteristics of a predetermined die cavity design, density and rheological properties of a material to be extruded, and a flow rate of the material to calculate the pressure distribution exerted on the die cavity and cross-sectional flow profile. The method further includes performing a structural analysis using the calculated pressure distribution and structural characteristics of the die cavity to calculate a deformed die cavity. The flow analysis is then repeated using the characteristics of the deformed die cavity to calculate a pressure distribution exerted on the die cavity and cross-sectional flow profile. The calculated pressure distributions and/or cross-sectional flow profiles are compared to determine if the pressure distributions and/or cross-sectional flow profiles converge. These steps are iteratively repeated until convergence of the pressure and/or cross-sectional flow profile is observed. Once convergence is observed, the variation of the cross-sectional flow profile is analyzed to determine if it is less than a predetermined tolerance.
摘要翻译： 设计模具腔的方法可以包括使用预定模腔设计特性，要挤出的材料的密度和流变特性以及材料的流速来计算施加在模腔上的压力分布的流动分析 和截面流动剖面。 该方法还包括使用计算出的模腔的压力分布和结构特征进行结构分析以计算变形的模腔。 然后使用变形模腔的特征重复流动分析，以计算施加在模腔上的压力分布和横截面流动分布。 比较计算出的压力分布和/或横截面流动分布，以确定压力分布和/或横截面流动分布是否收敛。 迭代地重复这些步骤，直到观察到压力和/或横截面流动分布的收敛。 一旦观察到收敛，则分析横截面流动分布的变化以确定其是否小于预定的公差。
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公开(公告)号：US5648483A
公开(公告)日：1997-07-15
申请号：US481779
申请日：1995-06-07
摘要： Polyol polyesters can be made by a transesterification reaction of a polyol with a lower alkyl fatty acid ester. A by product of that reaction are the alcohols from the lower alkyl esters. These are usually removed from the transesterification reaction by inert gas stripping. The process herein links the transesterification reaction with a lower alkyl ester formation reaction. The transesterification reaction acts as a the source of the lower alkyl alcohols for the formation of the lower alkyl esters used in the polyol fatty acid polyester synthesis. A preferred method for both reactions uses a reactive absorption column.
摘要翻译： 多元醇聚酯可以通过多元醇与低级烷基脂肪酸酯的酯交换反应来制备。 该反应的副产物是来自低级烷基酯的醇。 这些通常通过惰性气体剥离从酯交换反应中除去。 本文的方法将酯交换反应与低级烷基酯形成反应连接。 酯交换反应作为用于形成多元醇脂肪酸聚酯合成中使用的低级烷基酯的低级烷基醇的来源。 两种反应的优选方法使用反应性吸收塔。
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公开(公告)号：US06121440A
公开(公告)日：2000-09-19
申请号：US022751
申请日：1998-02-12
申请人： Corey James Kenneally , Gary Allen Busch , Patrick Joseph Corrigan , Eric Paul Granberg , John Keeney Howie , Richard Gerard Schafermeyer , James Earl Trout
发明人： Corey James Kenneally , Gary Allen Busch , Patrick Joseph Corrigan , Eric Paul Granberg , John Keeney Howie , Richard Gerard Schafermeyer , James Earl Trout
CPC分类号： C07H13/06
摘要： A process for preparing esterified polyol fatty acid polyesters is provided, where the polyol has n hydroxyl groups. The process provides for independent control of the level of fully esterified polyols, on the one hand, and the level of n-3 and lower esters, on the other hand. The process is especially suited for preparing sucrose polyester, wherein the process provides for independent control of the level of octaesters, on the one hand, and penta and lower level esters, on the other hand. The process can be used to reduce the level of undesirable reaction byproducts, such as difatty ketone and beta ketoester.
摘要翻译： 提供了制备酯化多元醇脂肪酸聚酯的方法，其中多元醇具有n个羟基。 另一方面，该方法一方面独立地控制完全酯化的多元醇的水平，另一方面提供了n-3和低级酯的水平。 该方法特别适用于制备蔗糖聚酯，其中该方法一方面独立控制八酯水平，另一方面提供五酸和低级酯。 该方法可用于降低不希望的反应副产物的水平，例如二甲基酮和β-酮酯。
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公开(公告)号：US5844111A
公开(公告)日：1998-12-01
申请号：US486847
申请日：1995-06-07
IPC分类号： B01D53/18 , B01D53/72 , B01J19/18 , B01J31/12 , C07B61/00 , C07C67/03 , C07C69/30 , C11B3/00
摘要： A process for purifying an inert gas stream from a transesterification reaction wherein a lower alkyl alcohol is released during the reaction is claimed. A second use of the process is to make a lower alkyl, e.g., methyl, esters of fatty acids through a transesterification reaction using gaseous alcohols as a source of the lower alkyl alcohols. The alcohol is diluted with nitrogen or other inert gas carrier and reacted with a fatty acid ester, preferably a triglyceride, to form the corresponding methyl or lower alkyl fatty acid ester.
摘要翻译： 要求从反应中释放低级烷基醇的酯交换反应中纯化惰性气体流的方法。 该方法的第二个用途是通过使用气态醇作为低级烷基醇的来源，通过酯交换反应制备脂肪酸的低级烷基，例如甲基酯。 将醇用氮气或其它惰性气体载体稀释，并与脂肪酸酯，优选甘油三酯反应形成相应的甲基或低级烷基脂肪酸酯。
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