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    Granular poly(arylene sulfide) recovery using evaporation
    1.
    发明授权
    Granular poly(arylene sulfide) recovery using evaporation 失效
    颗粒状聚（亚芳基硫）采用蒸发回收

    公开(公告)号：US4524200A

    公开(公告)日：1985-06-18

    申请号：US611573

    申请日：1984-05-18

    申请人： Fred T. Sherk ,  Afif M. Nesheiwat ,  Guy Senatore

    发明人： Fred T. Sherk ,  Afif M. Nesheiwat ,  Guy Senatore

    IPC分类号： C08G75/02 ,  C08J3/12 ,  C08G75/14

    CPC分类号： C08J3/12 ,  C08G75/02 ,  C08J2381/02

    摘要： Granular poly(arylene sulfide) is recovered from a slurry comprising granular poly(arylene sulfide), polar organic solvent, alkali metal halide, poly(arylene sulfide) oligomers, untreated reactants in the water by heating the slurry under conditions to evaporate polar organic solvent, water and volatile impurities at a temperature below the normal boiling point of the polar organic solvent to produce a dry mixture containing poly(arylene sulfide), poly(arylene sulfide) oligomers and alkali metal halide which is then reslurried with water to produce a reslurried mixture containing aqueous alkali metal halide solution and dispersed poly(arylene sulfide) oligomers with the reslurried mixture being filtered through a coarse screen to recover granular poly(arylene sulfide) thereon and pass a filtrate containing poly(arylene sulfide) oligomers and aqueous alkali metal halide solution therethrough. The filtrate can be further treated by filtering through a filter aid coated vacuum filter to recover poly(arylene sulfide) oligomers thereon and pass an aqueous alkali metal halide solution therethrough as filtrate.

    摘要翻译： 从含有聚（亚芳基硫醚），极性有机溶剂，碱金属卤化物，聚（亚芳基硫醚）低聚物的浆料中回收颗粒状聚（亚芳基硫醚），在水中通过在蒸发极性有机溶剂的条件下加热浆料 ，水和挥发性杂质在低于极性有机溶剂的正常沸点的温度下产生含有聚（亚芳基硫醚），聚（亚芳基硫醚）低聚物和碱金属卤化物的干燥混合物，然后将其与水一起重新制备， 含有碱金属卤化物水溶液和分散的聚（亚芳基硫醚）低聚物的混合物，其中重新制备的混合物通过粗筛过滤，以在其上回收粒状聚（亚芳基硫醚），并通过含有聚（亚芳基硫醚）低聚物和碱金属卤化物水溶液的滤液 溶液通过。 可以通过过滤助滤剂真空过滤器进一步处理滤液，以在其上回收聚（亚芳基硫醚）低聚物，并通过作为滤液的碱金属卤化物水溶液。

    Production of arylene sulfide polymer beads
    2.
    发明授权
    Production of arylene sulfide polymer beads 失效
    生产亚芳基硫化物聚合物珠

    公开(公告)号：US4451643A

    公开(公告)日：1984-05-29

    申请号：US456185

    申请日：1983-01-06

    申请人： James T. Edmonds, Jr. ,  Fred T. Sherk

    发明人： James T. Edmonds, Jr. ,  Fred T. Sherk

    IPC分类号： C08G75/02 ,  C08G75/14

    CPC分类号： C08G75/0272 ,  C08G75/0281

    摘要： A method for producing a polymer in which lithium hydroxide, optionally also employing either lithium chloride or lithium acetate, is contacted with N-methyl-pyrrolidone in the presence of lithium halide to produce a reaction product mixture containing lithium N-methyl-4-aminobutyrate with this reaction mixture then being contacted with hydrogen sulfide and polyhalo aromatic compound in the presence of additional N-methyl-pyrrolidone under conditions to form a polymer. Lithium halide produced as a by-product is substantially recovered from the reaction mixture, converted to lithium hydroxide and can be recycled to the process.

    摘要翻译： 一种生产聚合物的方法，其中任选地还使用氯化锂或乙酸锂的氢氧化锂在卤化锂的存在下与N-甲基 - 吡咯烷酮接触以产生含有N-甲基-4-氨基丁酸锂的反应产物混合物 然后在另外的N-甲基吡咯烷酮的存在下，使该反应混合物与硫化氢和多卤代芳族化合物接触，形成聚合物。 作为副产物生产的卤化锂基本上从反应混合物中回收，转化成氢氧化锂并可循环使用。

    Hydrocarbon treating process
    4.
    发明授权
    Hydrocarbon treating process 失效
    烃处理工艺

    公开(公告)号：US4167472A

    公开(公告)日：1979-09-11

    申请号：US900390

    申请日：1978-04-26

    申请人： James E. Dick ,  Fred T. Sherk ,  Lewis E. Drehman

    发明人： James E. Dick ,  Fred T. Sherk ,  Lewis E. Drehman

    IPC分类号： C07C5/41 ,  C07C15/00 ,  C10G59/06 ,  C07C5/40 ,  C07C15/02 ,  C10G39/00

    CPC分类号： C07C15/00 ,  C07C5/417 ,  C10G2400/30

    摘要： A process for treating a hydrocarbon composition containing both straight chain and non-straight chain hydrocarbons in which said hydrocarbon composition is separated into a straight chain hydrocarbon-rich fraction and a non-straight chain hydrocarbon-rich fraction, non-aromatics in said non-straight chain hydrocarbon-rich fraction are converted to aromatics, and at least a portion of the straight chain hydrocarbon-rich fraction is passed in combination with steam over a steam active catalyst comprising at least one Group VIII metal and a tin modified Group II metal aluminate under conditions such that aromatics are produced.

    摘要翻译： 一种用于处理含有直链烃和非直链烃的烃组合物的方法，其中所述烃组合物分离成直链富烃馏分和非直链富烃馏分，所述非芳族烃在所述非 - 将直链富烃馏分转化成芳族化合物，并将至少一部分直链富烃馏分与蒸汽结合通过包含至少一种第Ⅷ族金属和锡改性的第II族金属铝酸盐的蒸汽活性催化剂 在产生芳族化合物的条件下。

    Continuous process for the production of alkali metal n-methylaminobutyrate
    7.
    发明授权
    Continuous process for the production of alkali metal n-methylaminobutyrate 失效
    生产碱金属正甲基氨基丁酸酯的连续工艺

    公开(公告)号：US4529818A

    公开(公告)日：1985-07-16

    申请号：US502032

    申请日：1983-06-07

    申请人： Afif M. Nesheiwat ,  Fred T. Sherk

    发明人： Afif M. Nesheiwat ,  Fred T. Sherk

    IPC分类号： C07C101/04

    CPC分类号： C07C227/22

    摘要： A process for producing alkali metal aminobutyrate or alkali metal aminobutyrate-alkali metal bisulfide complex by contacting an aqueous alkali metal hydroxide with NMP and optionally alkali metal bisulfide in a stirred reactor under reaction conditions to produce a predominantly one-phase system and maintaining these reaction conditions while passing the one-phase system through a disrupted flow tube reactor to complete the reaction. Dehydrating the reaction product in a two-stage dehydration process using a higher temperature in the second stage.

    摘要翻译： 通过在搅拌反应器中在反应条件下使碱金属氢氧化物水溶液与NMP和任选的碱金属二硫化物接触来制备氨基丁酸碱金属或碱金属氨基丁酸盐 - 碱金属二硫化物络合物的方法，以产生主要的一相体系并维持这些反应条件 同时使单相系统通过破碎的流管反应器完成反应。 在第二阶段使用较高温度的两步脱水过程中使反应产物脱水。

    Hydrocarbon wash liquid for catalyst separation
    8.
    发明授权
    Hydrocarbon wash liquid for catalyst separation 失效
    用于催化分离的烃洗液

    公开(公告)号：US4436901A

    公开(公告)日：1984-03-13

    申请号：US350851

    申请日：1982-02-22

    申请人： Fred T. Sherk

    发明人： Fred T. Sherk

    IPC分类号： B01J19/18 ,  C08F6/02 ,  C08F6/10 ,  C08F6/06

    CPC分类号： B01J19/1837 ,  B01J19/245 ,  C08F6/02 ,  B01J2219/00094

    摘要： An improved polymerization process wherein vapors from a flash zone are condensed and used as wash liquid in a polymer washing zone and optionally a sidestream from a monomer fractionation zone is also used as wash liquid.

    摘要翻译： 改进的聚合方法，其中来自闪蒸区域的蒸气被冷凝并用作聚合物洗涤区域中的洗涤液体，并且任选地来自单体分馏区域的侧流也用作洗涤液体。

    Washing arylene sulfide polymers with water plus a reducing agent
    10.
    发明授权
    Washing arylene sulfide polymers with water plus a reducing agent 失效
    用水加还原剂洗涤亚芳基硫醚聚合物

    公开(公告)号：US4882418A

    公开(公告)日：1989-11-21

    申请号：US284169

    申请日：1988-12-13

    申请人： Guy Senatore ,  Afif M. Nesheiwat ,  Fred T. Sherk

    发明人： Guy Senatore ,  Afif M. Nesheiwat ,  Fred T. Sherk

    IPC分类号： C08G75/02

    CPC分类号： C08G75/0231 ,  C08G75/0281 ,  C08G75/0286

    摘要： A process is provided for removing solid and liquid impurities from a particulate arylene sulfide polymer recovered from a polymerization reaction mixture slurry, without significantly discoloring the resulting washed polymer. The process of this invention comprises the steps of: (a) preparing a first slurry, wherein the solid component thereof comprises a particulate arylene sulfide polymer recovered from a reaction mixture slurry, and wherein the liquid component thereof comprises a mixture of water and a reducing agent; (b) heating the first slurry to a temperature of at least about 185.degree. C. (365.degree. F.) but below the melting point of the particulate polymer, to wash the polymer contained therein; (c) cooling the first slurry to a temperature below about 100.degree. C. (212.degree. F.), to form a second slurry, wherein the solid component thereof comprises a washed particulate arylene sulfide polymer; and (d) recovering the washed particulate arylene sulfide polymer from the second slurry.

    摘要翻译： 提供一种从聚合反应混合物浆料中回收的颗粒状亚芳基硫醚聚合物中除去固体和液体杂质的方法，而不会使得到的洗涤聚合物显着变色。 本发明的方法包括以下步骤：（a）制备第一浆料，其中其固体组分包含从反应混合物浆料中回收的颗粒状亚芳基硫醚聚合物，并且其中其液体组分包括水和还原剂的混合物 代理人 （b）将第一浆料加热到至少约185℃（365°F）但低于颗粒状聚合物熔点的温度，以洗涤其中所含的聚合物; （c）将第一浆料冷却至低于约100℃（212°F）的温度，以形成第二浆料，其中其固体组分包含经洗涤的颗粒亚芳基硫醚聚合物; 和（d）从第二浆料中回收洗涤的颗粒状亚芳基硫醚聚合物。