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公开(公告)号：US5458955A
公开(公告)日：1995-10-17
申请号：US140340
申请日：1993-10-21
CPC分类号： C23C18/1879 , C23C18/1865 , C23C18/2033 , C23C18/206 , C23C18/30 , Y10T428/24942
摘要： Metal/polymer laminates prepared from essentially insoluble anionomeric polymer film layer with catalytic metal, e.g. palladium, exchanged into surface acid groups which can be reduced to provide catalytic metal clusters for catalyzing electroless deposition of metal which is resistant to removal by adhesive tape. Anionomeric polymer films are coated from solutions, emulsions or dispersions of sulfonated or carboxylated polyesters or sulfonated, phosphonated or carboxylated perfluorocarbon polymer, dried and heat treated, e.g. at 120.degree.-180.degree. C., to render the coating insoluble.
摘要翻译： 由基本不溶的阴离子聚合物膜层与催化金属制备的金属/聚合物层压体 钯，交换成表面酸基团，其可以还原以提供催化金属簇，用于催化金属的无电沉积，其耐胶粘剂去除。 由磺化或羧化的聚酯或磺化，膦酸化或羧化的全氟化碳聚合物的溶液，乳液或分散体涂覆阴离子聚合物膜，干燥和热处理。 在120°-180℃下，使涂层不溶。
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公开(公告)号：US5275861A
公开(公告)日：1994-01-04
申请号：US820450
申请日：1992-01-09
申请人： George D. Vaughn
发明人： George D. Vaughn
CPC分类号： H01M8/1004 , C23C18/30 , H05K3/182 , H05K3/387 , Y10T428/239
摘要： Electromagnetic radiation shielding textile material comprising metal-coated fabric adapted to be applied with overlapping seams at least 4 cm wide to provide at least 80 dB of far-field shielding against electromagnetic radiation between 0.1 and 10 gigahertz. Fabric, e.g. non-woven nylon fabric, coated with at least one layer of electrolessly-deposited metal, e.g. at least 15 g/m.sup.2 copper, is useful as backing for wallpaper which can provide effective far-field shielding of electromagnetic radiation.
摘要翻译： 电磁辐射屏蔽纺织材料包括金属涂层织物，其适用于至少4cm宽的重叠接缝，以提供至少80dB的远场屏蔽，防止0.1至10千兆赫兹之间的电磁辐射。 织物，例如 无纺布尼龙织物，涂覆有至少一层无电沉积金属，例如无纺布。 至少15克/平方米的铜，可用作壁纸背衬，可提供有效的远场屏蔽电磁辐射。
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公开(公告)号：US5517338A
公开(公告)日：1996-05-14
申请号：US963650
申请日：1992-10-20
摘要： Composite mirrors on a substrate comprising a mixture of up to 20 percent of polymer and at least 80 percent of metal clusters, e.g. of gold, palladium or silver, which have a nominal diameter less than 100 nanometers and which are agglomerated in a layer conforming to the surface of the substrate. Composite mirrors are produced by coating a substrate with a solution comprising at least 80 percent solvent, e.g. water and alcohol, and up to 20 percent of a mixture of up to 20 percent polymer, e.g. methylcellulose, and at least 80 percent metal, present as a salt of volatiles-forming anion, e.g. silver lactate or palladium acetate; dry films of polymer and salt are exposed to heat or ultraviolet light to convert the salt to metal clusters. Polymeric mirrors are especially useful for making reflection holograms on polymeric surfaces embossed with a latent holographic image in a relief pattern.
摘要翻译： 基底上的复合反射镜，其包含高达20％的聚合物和至少80％的金属簇的混合物，例如， 金，钯或银，其具有小于100纳米的标称直径，并且在与基材表面相符的层中聚集。 复合反射镜通过用包含至少80％溶剂的溶液涂布基材来制备，例如， 水和醇，以及高达20％的高达20％的聚合物的混合物，例如。 甲基纤维素和至少80％的金属，以形成挥发物的阴离子的盐形式存在，例如， 乳酸银或乙酸钯; 将聚合物和盐的干膜暴露于热或紫外光以将盐转化为金属簇。 聚合反射镜特别适用于在浮雕图案中用潜像全息图像压印的聚合物表面上制作反射全息图。
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公开(公告)号：US5403649A
公开(公告)日：1995-04-04
申请号：US91145
申请日：1993-07-13
申请人： Albert W. Morgan , George D. Vaughn
发明人： Albert W. Morgan , George D. Vaughn
IPC分类号： B60B3/00 , C23C18/28 , C23C18/30 , C23C18/31 , H01G13/00 , H01L21/288 , H01M8/10 , H01Q15/14 , H01R43/16 , H05K3/18 , H05K3/38 , B32B9/00
CPC分类号： C23C18/30 , C23C18/28 , H01M8/1004 , H05K3/182 , B41M1/10 , B41M3/006 , B41M7/009 , B41N1/20 , H05K3/387 , Y10S428/901 , Y10T428/24917 , Y10T428/249921 , Y10T428/26 , Y10T428/31678
摘要： Methods for fabricating two-dimensional imaged metal articles on webs by electroless deposition of metal onto a catalytic pattern rotogravurely printed onto moving webs travelling at linear speeds of up to 500 meters/minute using low viscosity catalytic ink comprising polymer and compound, complex or colloid of a Group 1B or Group 8 metal. Such two-dimensional imaged metal articles comprise areas or fine lines, e.g. less than 100 micrometers wide, which are useful as electrical devices such as circuit connectors, antennas and the like or as mechanical devices such as levers, gears and the like. With modification of the metal component or addition of other materials, such two-dimensional imaged metal articles can be useful a electronic devices such as diodes, resistors, capacitors and the like or as energy conversion devices such as batteries, sensors or fuel cells. The catalytic inks have appropriate rheological properties of viscosity and surface tension that permit non-sagging, non-spreading images to be printed onto a web which can travel vertically into a drying zone.
摘要翻译： 通过将金属无电沉积到催化图案上的催化图案上制造二维成像金属制品的方法，所述催化图案通过使用包含聚合物和化合物，复合物或胶体的低粘度催化油墨以高达500米/分钟的直线速度行进的移动幅材上印刷 第1B组或第8组金属。 这样的二维成像金属制品包括区域或细线，例如。 小于100微米宽，其可用作诸如电路连接器，天线等的电气装置，或作为诸如杠杆，齿轮等的机械装置。 通过改变金属组分或添加其它材料，这种二维成像的金属制品可用于诸如二极管，电阻器，电容器等的电子设备，或者作为诸如电池，传感器或燃料电池的能量转换装置。 催化油墨具有适当的粘度和表面张力的流变性质，其允许不下垂，不扩散的图像被印刷到可垂直移动到干燥区域的幅材上。
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公开(公告)号：US5227223A
公开(公告)日：1993-07-13
申请号：US713246
申请日：1991-06-07
申请人： Albert W. Morgan , George D. Vaughn
发明人： Albert W. Morgan , George D. Vaughn
IPC分类号： B60B3/00 , C23C18/28 , C23C18/30 , C23C18/31 , H01G13/00 , H01L21/288 , H01M8/10 , H01Q15/14 , H01R43/16 , H05K3/18 , H05K3/38
CPC分类号： C23C18/30 , C23C18/28 , H01M8/1004 , H05K3/182 , B41M1/10 , B41M3/006 , B41M7/009 , B41N1/20 , H05K3/387 , Y10S428/901 , Y10T428/24917 , Y10T428/249921 , Y10T428/26 , Y10T428/31678
摘要： Methods for fabricating two-dimensional imaged metal articles on webs by electroless deposition of metal onto a catalytic pattern rotogravurely printed onto moving webs travelling at linear speeds of up to 500 meters/minute using low viscosity catalytic ink comprising polymer and compound, complex or colloid of a Group 1B or Group 8 metal. Such two-dimensional imaged metal articles comprise areas or fine lines, e.g. less than 100 micrometers wide, which are useful as electrical devices such as circuit connectors, antennas and the like or as mechanical devices such as levers, gears and the like. With modification of the metal component or addition of other materials, such two-dimensional imaged metal articles can be useful a electronic devices such as diodes, resistors, capacitors and the like or as energy conversion devices such as batteries, sensors or fuel cells. The catalytic inks have appropriate rheological properties of viscosity and surface tension that permit non-sagging, non-spreading images to be printed onto a web which can travel vertically into a drying zone.
摘要翻译： 通过将金属无电沉积到催化图案上的催化图案上制造二维成像金属制品的方法，所述催化图案通过使用包含聚合物和化合物，复合物或胶体的低粘度催化油墨以高达500米/分钟的直线速度行进的移动幅材上印刷 第1B组或第8组金属。 这样的二维成像金属制品包括区域或细线，例如。 小于100微米宽，其可用作诸如电路连接器，天线等的电气装置，或作为诸如杠杆，齿轮等的机械装置。 通过改变金属组分或添加其它材料，这种二维成像的金属制品可用于诸如二极管，电阻器，电容器等的电子设备，或者作为诸如电池，传感器或燃料电池的能量转换装置。 催化油墨具有适当的粘度和表面张力的流变性质，其允许不下垂，不扩散的图像被印刷到可垂直移动到干燥区域的幅材上。
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公开(公告)号：US5158604A
公开(公告)日：1992-10-27
申请号：US724093
申请日：1991-07-01
IPC分类号： C23C18/31
CPC分类号： C23C18/31
摘要： Viscous aqueous electroless plating solutions comprising ionic depositable metal species such as copper or nickel, metal complexing agent such as EDTA, metal reducing agent such as formaldehyde or hypophosphite and thickener such as xantham gum, silica or carboxymethylcellulose have a viscosity greater than 50 cp, for instance up to 20,000 cp. The viscous solutions are useful for electrolessly depositing metal onto moving or inclined catalytic substrates and as a component of kits for applying electrolessly deposited metal images to such surfaces.
摘要翻译： 包含离子沉积金属物质如铜或镍的粘性含水化学镀溶液，诸如EDTA的金属络合剂，诸如甲醛或次磷酸盐的金属还原剂和黄原胶，二氧化硅或羧甲基纤维素等增稠剂的粘度大于50cp，对于 实例高达20,000 cp。 粘性溶液可用于将金属无电沉积到移动或倾斜的催化底物上，并且作为用于将无电沉积金属图像施加到这些表面的试剂盒的组分。
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公开(公告)号：US5082734A
公开(公告)日：1992-01-21
申请号：US609718
申请日：1990-11-13
申请人： George D. Vaughn
发明人： George D. Vaughn
CPC分类号： C23C18/30 , H01M8/1004 , H05K3/182 , H05K3/387 , Y10S428/901 , Y10T428/24917 , Y10T428/25 , Y10T428/256 , Y10T428/31504 , Y10T428/31678 , Y10T442/2418 , Y10T442/339 , Y10T442/3407
摘要： Metal coated articles where the metal is electrolessly deposited onto catalytic films prepared by thermally activating catalytically inert films formed from an aqueous solution comprising polymer, e.g. cellulosic, vinyl alcohol or oxyolefin polymers, and catalytic metal of Group 8, e.g. palladium. Copper electrolessly deposited on activated films exhibits high ductility similar to electrolytic copper, e.g. at least about 8 percent ductility.
摘要翻译： 金属涂层制品，其中金属被无电沉积到通过热活化由包含聚合物的水溶液形成的催化惰性膜制备的催化膜上。 纤维素，乙烯醇或氧烯烃聚合物，以及第8组的催化金属，例如。 钯。 无电沉积在活化膜上的铜显示出类似于电解铜的高延展性，例如。 至少约8％的延展性。
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公开(公告)号：US5087510A
公开(公告)日：1992-02-11
申请号：US497960
申请日：1990-03-22
IPC分类号： G03H1/02
CPC分类号： G03H1/0252 , G03H1/0244 , G03H2250/36 , Y10S428/913 , Y10T428/24802 , Y10T428/24917 , Y10T428/31678
摘要： Electrolessly deposited metal holograms comprising a polymeric substrate having a holographic relief-patterned surface and a metal reflective layer electrolessly deposited to conform to and reproduce the holographic relief patterned. Light incident to the metal surface is reflected to provide an holographic reproduction of an holographic image inherent in said relief-patterned polymeric substrate.
摘要翻译： 无电沉积的金属全息图包括具有全息凸版图案表面的聚合物基材和无电沉积以符合并再现图案化的全息图案的金属反射层。 入射到金属表面的光被反射以提供所述浮雕图案化聚合物基底中固有的全息图像的全息再现。
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