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    Porous anodic aluminum oxide membranes for nanofarication
    2.
    发明申请
    Porous anodic aluminum oxide membranes for nanofarication 有权
    多孔阳极氧化铝膜用于纳米法

    公开(公告)号：US20070151850A1

    公开(公告)日：2007-07-05

    申请号：US11606310

    申请日：2006-11-28

    申请人： Hsien-Hau Wang ,  Jianjiang Lu ,  Shufang Yu

    发明人： Hsien-Hau Wang ,  Jianjiang Lu ,  Shufang Yu

    IPC分类号： G01N27/26 ,  B01J23/44 ,  C01F7/02

    CPC分类号： G01N27/40 ,  C23C18/08 ,  C25D11/12 ,  C25D11/24

    摘要： A hydrogen detector with a porous layer of alumina. Pores with average pore diameters in the range of from about 10 to about 200 nanometers (nms) and average pore depths in the range of from about 10 to about 1000 nms have Pd nanoparticles in the pores forming a film. Electrodes on the Pd film measure changes in electrical resistance of the Pd film in the presence of hydrogen. Pd may be in the form of nanotubes. The alumina is anodized for various times to form the nanowalls or pores and vary the pore depths.

    摘要翻译： 具有多孔氧化铝层的氢探测器。 平均孔径在约10至约200纳米（nms）范围内且平均孔深度在约10至约1000nms范围内的孔具有形成膜的孔中的Pd纳米颗粒。 Pd膜上的电极测量Pd存在下Pd膜的电阻变化。 Pd可以是纳米管的形式。 将氧化铝阳极氧化多次以形成纳米壁或孔，并改变孔深。

    Ambient-pressure organic superconductor
    3.
    发明授权
    Ambient-pressure organic superconductor 失效
    环境压力有机超导体

    公开(公告)号：US4632776A

    公开(公告)日：1986-12-30

    申请号：US853324

    申请日：1986-04-18

    申请人： Jack M. Williams ,  Hsien-Hau Wang ,  Mark A. Beno

    发明人： Jack M. Williams ,  Hsien-Hau Wang ,  Mark A. Beno

    IPC分类号： H01L39/12 ,  H01B1/06

    CPC分类号： H01L39/121 ,  Y10S505/802

    摘要： A new class of organic superconductors having the formula (ET).sub.2 MX.sub.2 wherein ET represents bis(ethylenedithio)-tetrathiafulvalene, M is a metal such as Au, Ag, In, Tl, Rb, Pd and the like and X is a halide. The superconductor (ET).sub.2 AuI.sub.2 exhibits a transition temperature of 5 K which is high for organic superconductors.

    摘要翻译： 具有式（ET）2MX2的新一类有机超导体，其中ET表示双（亚乙基二硫） - 四硫富瓦烯，M是金属如Au，Ag，In，Tl，Rb，Pd等，X是卤化物。 超导体（ET）2AuI2的转变温度为5K，对于有机超导体而言是高的。

    High-Performance Flexible Hydrogen Sensors
    5.
    发明申请
    High-Performance Flexible Hydrogen Sensors 有权
    高性能柔性氢传感器

    公开(公告)号：US20090084159A1

    公开(公告)日：2009-04-02

    申请号：US11862341

    申请日：2007-09-27

    申请人： Yugang Sun ,  Hsien-Hau Wang

    发明人： Yugang Sun ,  Hsien-Hau Wang

    IPC分类号： G01N7/00 ,  B28B1/20

    CPC分类号： G01N33/005 ,  G01N27/127 ,  Y10S977/748 ,  Y10S977/957

    摘要： Single-walled carbon nanotubes (SWNTs) are decorated with metal nanoparticles to form high-performance flexible hydrogen sensors. The special process to form the high-performance flexible hydrogen sensors can combine a dry transfer printing technique and modification of SWNTs with palladium (Pd) nanoparticles to provide high-performance hydrogen sensors with excellent mechanical flexibility on plastic substrates. Two approaches can be used to decorate the SWNTs. One is physical deposition, such as electron beam evaporation (EBE) and the other is electrochemical deposition which can selectively grow palladium nanoparticles on the surface of the SWNTs, resulting in significantly decreasing the use of palladium. Preferably, the Pd nanoparticles are deposed on the SWNTs in a discontinuous arrangement so that the Pd nanoparticles are spaced away from each other to form individual discontinuous Pd nanoparticles rather a continuous Pd film. Advantageously, the SWNTs are arranged with substantial semiconducting pathways. Desirably, the high-performance flexible hydrogen sensors have an excellent response and recovery time, provide superior sensitivity for detecting hydrogen, and are bendable to conform to the contours of other structures.

    摘要翻译： 单壁碳纳米管（SWNT）用金属纳米粒子装饰以形成高性能柔性氢传感器。 形成高性能柔性氢传感器的特殊工艺可以结合干法转印技术和将单壁碳纳米管与钯（Pd）纳米粒子进行改性，以提供高性能的氢传感器，在塑料基板上具有出色的机械灵活性。 可以使用两种方法来装饰SWNT。 一种是物理沉积，例如电子束蒸发（EBE），另一种是电化学沉积，其可以选择性地在单壁奈米碳管的表面上生长钯纳米颗粒，导致钯的使用显着降低。 优选地，Pd纳米颗粒以不连续的排列被置于SWNT上，使得Pd纳米颗粒彼此间隔开以形成单独的不连续的Pd纳米颗粒而不是连续的Pd膜。 有利地，SWNT布置有大量的半导体通路。 理想地，高性能柔性氢传感器具有优异的响应和恢复时间，为检测氢提供优异的灵敏度，并且可弯曲以符合其他结构的轮廓。

    Porous anodic aluminum oxide membranes for nanofabrication
    6.
    发明授权
    Porous anodic aluminum oxide membranes for nanofabrication 有权
    多孔阳极氧化铝膜用于纳米制造

    公开(公告)号：US07820587B2

    公开(公告)日：2010-10-26

    申请号：US11606310

    申请日：2006-11-28

    申请人： Hsien-Hau Wang ,  Jianjiang Lu ,  Shufang Yu

    发明人： Hsien-Hau Wang ,  Jianjiang Lu ,  Shufang Yu

    IPC分类号： B01J23/44

    CPC分类号： G01N27/40 ,  C23C18/08 ,  C25D11/12 ,  C25D11/24

    摘要： A hydrogen detector with a porous layer of alumina. Pores with average pore diameters in the range of from about 10 to about 200 nanometers (nms) and average pore depths in the range of from about 10 to about 1000 nms have Pd nanoparticles in the pores forming a film. Electrodes on the Pd film measure changes in electrical resistance of the Pd film in the presence of hydrogen. Pd may be in the form of nanotubes. The alumina is anodized for various times to form the nanowalls or pores and vary the pore depths.

    摘要翻译： 具有多孔氧化铝层的氢探测器。 平均孔径在约10至约200纳米（nms）范围内且平均孔深度在约10至约1000nms范围内的孔具有形成膜的孔中的Pd纳米颗粒。 Pd膜上的电极测量Pd存在下Pd膜的电阻变化。 Pd可以是纳米管的形式。 将氧化铝阳极氧化多次以形成纳米壁或孔，并改变孔深。

    High-performance flexible hydrogen sensors
    7.
    发明授权
    High-performance flexible hydrogen sensors 有权
    高性能柔性氢传感器

    公开(公告)号：US07818993B2

    公开(公告)日：2010-10-26

    申请号：US11862341

    申请日：2007-09-27

    申请人： Yugang Sun ,  Hsien-Hau Wang

    发明人： Yugang Sun ,  Hsien-Hau Wang

    IPC分类号： G01N7/00

    CPC分类号： G01N33/005 ,  G01N27/127 ,  Y10S977/748 ,  Y10S977/957

    摘要： Single-walled carbon nanotubes (SWNTs) are decorated with metal nanoparticles to form high-performance flexible hydrogen sensors. The special process to form the high-performance flexible hydrogen sensors can combine a dry transfer printing technique and modification of SWNTs with palladium (Pd) nanoparticles to provide high-performance hydrogen sensors with excellent mechanical flexibility on plastic substrates. Two approaches can be used to decorate the SWNTs. One is physical deposition, such as electron beam evaporation (EBE) and the other is electrochemical deposition which can selectively grow palladium nanoparticles on the surface of the SWNTs, resulting in significantly decreasing the use of palladium. Preferably, the Pd nanoparticles are deposed on the SWNTs in a discontinuous arrangement so that the Pd nanoparticles are spaced away from each other to form individual discontinuous Pd nanoparticles rather a continuous Pd film. Advantageously, the SWNTs are arranged with substantial semiconducting pathways. Desirably, the high-performance flexible hydrogen sensors have an excellent response and recovery time, provide superior sensitivity for detecting hydrogen, and are bendable to conform to the contours of other structures.

    摘要翻译： 单壁碳纳米管（SWNT）用金属纳米粒子装饰以形成高性能柔性氢传感器。 形成高性能柔性氢传感器的特殊工艺可以结合干法转印技术和将单壁碳纳米管与钯（Pd）纳米粒子进行改性，以提供高性能的氢传感器，在塑料基材上具有出色的机械灵活性。 可以使用两种方法来装饰SWNT。 一种是物理沉积，例如电子束蒸发（EBE），另一种是电化学沉积，其可以选择性地在单壁奈米碳管的表面上生长钯纳米颗粒，导致钯的使用显着降低。 优选地，Pd纳米颗粒以不连续的排列被置于SWNT上，使得Pd纳米颗粒彼此间隔开以形成单独的不连续的Pd纳米颗粒而不是连续的Pd膜。 有利地，SWNT布置有大量的半导体通路。 理想地，高性能柔性氢传感器具有优异的响应和恢复时间，为检测氢提供优异的灵敏度，并且可弯曲以符合其他结构的轮廓。

    Spatially controlled, in situ synthesis of polymers
    8.
    发明授权
    Spatially controlled, in situ synthesis of polymers 失效
    空间控制，聚合物的原位合成

    公开(公告)号：US06869983B2

    公开(公告)日：2005-03-22

    申请号：US10458344

    申请日：2003-06-10

    申请人： Gerard T. Caneba ,  Vijaya Raghavan Tirumala ,  Derrick C. Mancini ,  Hsien-Hau Wang

    发明人： Gerard T. Caneba ,  Vijaya Raghavan Tirumala ,  Derrick C. Mancini ,  Hsien-Hau Wang

    IPC分类号： C08F2/46

    CPC分类号： C08F2/46 ,  Y10S522/91

    摘要： An in situ polymer microstructure formation method. The monomer mixture is polymerized in a solvent/precipitant through exposure to ionizing radiation in the absence any chemical mediators. If an exposure mask is employed to block out certain regions of the radiation cross section, then a patterned microstructure is formed. The polymerization mechanism is based on the so-called free-radical retrograde-precipitation polymerization process, in which polymerization occurs while the system is phase separating above the lower critical solution temperature. This method was extended to produce a crosslinked line grid-pattern of poly (N-isopropylacrylamide), which has been known to have thermoreversible properties.

    摘要翻译： 原位聚合物微观结构形成方法。 在没有任何化学介质的情况下，通过暴露于电离辐射，单体混合物在溶剂/沉淀剂中聚合。 如果使用曝光掩模来阻挡辐射截面的某些区域，则形成图案化的微结构。 聚合机理基于所谓的自由基逆行沉淀聚合方法，其中在系统在较低临界溶解温度以上分相时发生聚合。 该方法被扩展以产生已知具有热可逆性质的聚（N-异丙基丙烯酰胺）的交联线栅格图案。

    SPATIALLY CONTROLLED, IN SITU SYNTHESIS OF POLYMERS
    10.
    发明申请
    SPATIALLY CONTROLLED, IN SITU SYNTHESIS OF POLYMERS 失效
    空间控制，聚合物的合成

    公开(公告)号：US20050043428A1

    公开(公告)日：2005-02-24

    申请号：US10458344

    申请日：2003-06-10

    申请人： Gerard Caneba ,  Vijaya Tirumala ,  Derrick Mancini ,  Hsien-Hau Wang

    发明人： Gerard Caneba ,  Vijaya Tirumala ,  Derrick Mancini ,  Hsien-Hau Wang

    IPC分类号： C08F2/46 ,  C08G2/00

    CPC分类号： C08F2/46 ,  Y10S522/91

    摘要： An in situ polymer microstructure formation method. The monomer mixture is polymerized in a solvent/precipitant through exposure to ionizing radiation in the absence any chemical mediators. If an exposure mask is employed to block out certain regions of the radiation cross section, then a patterned microstructure is formed. The polymerization mechanism is based on the so-called free-radical retrograde-precipitation polymerization process, in which polymerization occurs while the system is phase separating above the lower critical solution temperature. This method was extended to produce a crosslinked line grid-pattern of poly (N-isopropylacrylamide), which has been known to have thermoreversible properties.

    摘要翻译： 原位聚合物微观结构形成方法。 在没有任何化学介质的情况下，通过暴露于电离辐射，单体混合物在溶剂/沉淀剂中聚合。 如果使用曝光掩模来阻挡辐射截面的某些区域，则形成图案化的微结构。 聚合机理基于所谓的自由基逆行沉淀聚合方法，其中在系统在较低临界溶解温度以上分相时发生聚合。 该方法被扩展以产生已知具有热可逆性质的聚（N-异丙基丙烯酰胺）的交联线栅格图案。