REACTION TUBE AND METHOD FOR PRODUCING HYDROGEN CYANIDE
    4.
    发明申请
    REACTION TUBE AND METHOD FOR PRODUCING HYDROGEN CYANIDE 审中-公开
    反应管和生产氢氰化物的方法

    公开(公告)号:US20160263558A1

    公开(公告)日:2016-09-15

    申请号:US15028415

    申请日:2014-10-02

    摘要: The reaction tube for preparing hydrogen cyanide comprises a cylindrical tube composed of ceramic, a catalyst comprising platinum applied to the inner wall of the tube and also at least one insert composed of ceramic, having three or four fins pointing from the tube axis to the inner wall of the tube, which is inserted into the cylindrical tube, wherein the fins divide the tube interior space into substantially straight channels with substantially identical circle segment cross sections and wherein the mean gap between the ends of the fins and the inner wall of the tube is in the range of 0.1 to 3 mm. In the method for preparing hydrogen cyanide, ammonia and at least one aliphatic hydrocarbon having 1 to 4 carbon atoms are reacted in the reaction tube at 1000 to 1400° C.

    摘要翻译: 用于制备氰化氢的反应管包括由陶瓷构成的圆柱形管,包含铂的催化剂,其施加到管的内壁上,还包括至少一个由陶瓷组成的插入件,具有从管轴指向内部的三个或四个翅片 插入圆柱形管中的管的壁,其中翅片将管内部空间划分成具有基本相同的圆形截面的基本上直的通道,并且其中翅片的端部与管的内壁之间的平均间隙 在0.1〜3mm的范围内。 在制备氰化氢的方法中,氨和至少一种具有1至4个碳原子的脂族烃在反应管中在1000-1400℃下反应。

    PROCESS FOR OBTAINING METHIONINE
    7.
    发明申请
    PROCESS FOR OBTAINING METHIONINE 有权
    获得甲磺酸的方法

    公开(公告)号:US20160229799A1

    公开(公告)日:2016-08-11

    申请号:US15021541

    申请日:2014-09-10

    IPC分类号: C07C321/14

    摘要: The invention relates to a method for crystallizing D,L-methionine from aqueous solutions and/or suspensions containing D,L-methionine and D,L-methionine ammonium salts, having a Met content of 70-180 g/kg, an NH4+ content of 1-5 g/kg, in the presence of a crystallization additive, which comprises a nonionic or anionic surfactant or a mixture of various nonionic or anionic surfactants, in which the temperature of the solution and/or suspension is lowered directly or stepwise from T1=85-110° C. to T2=30-50° C., so that D,L-methionine precipitates as a solid.

    摘要翻译: 本发明涉及从含有D,L-甲硫氨酸和D,L-甲硫氨酸铵盐的水溶液和/或悬浮液中结晶D,L-甲硫氨酸的方法,其Met含量为70-180g / kg,NH4 +含量 在结晶添加剂存在下,其包含非离子或阴离子表面活性剂或各种非离子或阴离子表面活性剂的混合物,其中溶液和/或悬浮液的温度直接或逐步从 T1 = 85-110℃至T2 = 30-50℃,因此D,L-甲硫氨酸作为固体沉淀。