Process for synthesis of 11C-labeled methyl iodide and apparatus
    1.
    发明授权
    Process for synthesis of 11C-labeled methyl iodide and apparatus 失效
    合成11C标记甲基碘的方法及仪器

    公开(公告)号:US5278875A

    公开(公告)日:1994-01-11

    申请号:US913696

    申请日:1992-07-16

    IPC分类号: C07B59/00 G21G1/10

    CPC分类号: C07B59/001

    摘要: In a process for the synthesis of .sup.11 C-labeled methyl iodide which comprises producing .sup.11 CO.sub.2 by the irradiation of a proton beam, supplying .sup.11 CO.sub.2 gas to a collector of .sup.11 CO.sub.2 gas, bubbling .sup.11 CO.sub.2 gas into a reducing agent solution to reduce .sup.11 CO.sub.2, removing the reducing agent solution by evaporation, synthesizing .sup.11 CH.sub.3 I from the reduced product of .sup.11 CO.sub.2, and recovering .sup.11 CH.sub.3 I by distillation, the termination point of the .sup.11 CO.sub.2 gas supply, the termination point of the bubbling, the termination point of the evaporation of the reducing agent solution or the termination point of the distillation of .sup.11 CH.sub.3 I is decided by a radiation sensor provided in the vicinity of the reaction vessel or a transfer tube connecting the target box wherein .sup.11 CO.sub.2 gas is generated or a temperature sensor provided in an exhaust tube of the reaction vessel. The synthesizing time is shortened, and the yield of .sup.11 CH.sub.3 I is improved by improving the utilization of .sup.11 CO.sub.2 gas and the recovery of .sup.11 CH.sub.3 I of which the half-life is very short.

    摘要翻译: 在合成11C标记的甲基碘的方法中,其包括通过照射质子束产生11CO 2,向11CO 2气体的收集器提供11CO 2气体,将11CO 2气体鼓泡到还原剂溶液中以还原11CO2,除去还原剂 通过蒸发合成11CH3I,通过蒸馏合成11CH3I,通过蒸馏回收11CH 3 I,11CO 2气体供应的终止点,起泡终止点,还原剂溶液的蒸发终止点或终止点 11CH3I的蒸馏由设置在反应容器附近的辐射传感器或连接其上产生11CO 2气体的目标箱的转移管或设置在反应容器的排气管中的温度传感器决定。 合成时间缩短,提高11CO2气的利用率和11CH3I的半衰期非常短的11CH3I的回收率提高了11CH3I的产率。

    Data transfer between disk storage and host device under the control of
file control device employing cache and associated batch write-back
operation
    2.
    发明授权
    Data transfer between disk storage and host device under the control of file control device employing cache and associated batch write-back operation 失效
    在文件控制设备的控制下,使用缓存和关联的批量回写操作,磁盘存储和主机设备之间的数据传输

    公开(公告)号:US5727183A

    公开(公告)日:1998-03-10

    申请号:US615434

    申请日:1996-03-14

    申请人: Naoko Takahashi

    发明人: Naoko Takahashi

    IPC分类号: G06F3/06 G06F12/00 G06F12/08

    CPC分类号: G06F12/0804 G06F12/0866

    摘要: A file control apparatus and a data transferring method that are capable of accessing data within a disk storage device at a much higher speed. The file control apparatus, when there arises a necessity for writing track data within a cache memory back to a disk storage device, writes a series of track data containing that piece of track data and to be written back to the consecutive tracks back to the disk storage device from within the cache memory and stores the effect that each piece of track data that has been written back is data requiring no necessity for the write-back process.

    摘要翻译: 一种文件控制装置和数据传送方法,能够以更高的速度访问磁盘存储装置内的数据。 文件控制装置当需要将高速缓冲存储器内的轨迹数据写回磁盘存储装置时,写入包含该条轨道数据的一系列轨道数据,并将其写回到连续轨道回到盘 存储装置,并且存储已经被写回的每条磁道数据的数据是不需要回写处理的数据的效果。

    Process for synthesis of .sup.11 C-labeled methyl iodide and apparatus
    3.
    发明授权
    Process for synthesis of .sup.11 C-labeled methyl iodide and apparatus 失效
    合成11C标记的甲基碘和装置的方法

    公开(公告)号:US5217675A

    公开(公告)日:1993-06-08

    申请号:US716868

    申请日:1991-06-18

    IPC分类号: C07B59/00

    CPC分类号: C07B59/001

    摘要: In a process for the synthesis of .sup.11 C-labeled methyl iodide which comprises producing .sup.11 CO.sub.2 by the irradiation of a proton beam, supplying .sup.11 CO.sub.2 gas to a collector of .sup.11 CO.sub.2 gas, bubbling .sup.11 CO.sub.2 gas into a reducing agent solution to reduce .sup.11 CO.sub.2, removing the reducing agent solution by evaporation, synthesizing .sup.11 CH.sub.3 I from the reduced product of .sup.11 CO.sub.2, and recovering .sup.11 CH.sub.3 I by distillation, the termination point of the .sup.11 CO.sub.2 gas supply, the termination point of the bubbling, the termination point of the evaporation of the reducing agent solution or the termination point of the distillatin of .sup.11 CH.sub.3 I is decided by a radiation sensor provided in the vicinity of the reaction vessel or a transfer tube connecting the target box wherein .sup.11 CO.sub.2 gas is generated or a temperature sensor provide in an exhaust tube of the reaction vessel. The synthesizing time is shortened, and the yield of .sup.11 CH.sub.3 I is improved by improving the utilization of .sup.11 CO.sub.2 gas and the recovery of .sup.11 CH.sub.3 I of which the half-life is very short.

    SILICA MEMBRANE AND METHOD FOR MANUFACTURING THE SAME
    5.
    发明申请
    SILICA MEMBRANE AND METHOD FOR MANUFACTURING THE SAME 有权
    二氧化硅膜及其制造方法

    公开(公告)号:US20120018370A1

    公开(公告)日:2012-01-26

    申请号:US13182589

    申请日:2011-07-14

    IPC分类号: B01D71/02 B05D3/02

    摘要: There is provided a silica membrane 1 formed on a porous substrate. A desorbed ionic strength of water having a temperature of 500° C. in a temperature-programmed desorption analysis of water of the silica membrane is 2,000,000/g. The silica membrane 1 is manufactured by allowing a silica sol having a water concentration of 0.03 to 3 mass % to adhere to a porous substrate by an ethanol solvent, drying the silica sol by sending air having a dew point of −70 to 0° C., and firing the dried silica sol at 200 to 400° C.

    摘要翻译: 提供了形成在多孔基材上的二氧化硅膜1。 在二氧化硅膜的水的温度程序解吸分析中,温度为500℃的水的解吸离子强度为2,000,000 / g。 二氧化硅膜1通过使水浓度为0.03〜3质量%的硅溶胶通过乙醇溶剂粘附到多孔质基材上来制造,通过将露点为-70〜0℃的空气干燥, 在200〜400℃下烧干硅溶胶。

    Absorbent article and production process therefor
    10.
    发明授权
    Absorbent article and production process therefor 失效
    吸收制品及其生产工艺

    公开(公告)号:US06150582A

    公开(公告)日:2000-11-21

    申请号:US82923

    申请日:1998-05-21

    摘要: The invention clarifies absorption properties of a water-absorbent resin as needed in the case where the ratio by weight of the water-absorbent resin to the total of the water-absorbent resin and the fibrous material is ".alpha.," and further the invention provides an absorbent article using a water-absorbent resin which is optimal to the ratio by weight ".alpha." of the water-absorbent resin. A water-absorbent resin, having a concentration absorption index of 35 or more as shown by the following equation (1):A(1-.alpha.)+B.alpha. (1)wherein A (g/g) is an absorption capacity of the resin under no load, andB (g/g) is an absorption capacity of the resin under a load, is used as the water-absorbent resin as used for the absorbent article of at least 0.4 in the ratio by weight ".alpha." of the water-absorbent resin to the total of the water-absorbent resin and the fibrous material.

    摘要翻译: 本发明根据吸水性树脂与吸水性树脂和纤维材料的总量的重量比为“α”的情况,根据需要明确了吸水性树脂的吸收特性,进一步本发明提供 使用吸水性树脂的吸收性物品,该吸水性树脂对于吸水性树脂的重量比“α”是最佳的。 浓度吸收指数为35以上的吸水性树脂,如下式(1)所示:A(1-α)+Bα(1)其中A(g / g)为 树脂在负载下的B(g / g)是树脂在负荷下的吸收能力,作为用于吸收性物品的吸水性树脂,以重量比“α”为至少0.4 吸水性树脂与吸水性树脂和纤维材料的总量相同。