摘要:
In a process for the synthesis of .sup.11 C-labeled methyl iodide which comprises producing .sup.11 CO.sub.2 by the irradiation of a proton beam, supplying .sup.11 CO.sub.2 gas to a collector of .sup.11 CO.sub.2 gas, bubbling .sup.11 CO.sub.2 gas into a reducing agent solution to reduce .sup.11 CO.sub.2, removing the reducing agent solution by evaporation, synthesizing .sup.11 CH.sub.3 I from the reduced product of .sup.11 CO.sub.2, and recovering .sup.11 CH.sub.3 I by distillation, the termination point of the .sup.11 CO.sub.2 gas supply, the termination point of the bubbling, the termination point of the evaporation of the reducing agent solution or the termination point of the distillation of .sup.11 CH.sub.3 I is decided by a radiation sensor provided in the vicinity of the reaction vessel or a transfer tube connecting the target box wherein .sup.11 CO.sub.2 gas is generated or a temperature sensor provided in an exhaust tube of the reaction vessel. The synthesizing time is shortened, and the yield of .sup.11 CH.sub.3 I is improved by improving the utilization of .sup.11 CO.sub.2 gas and the recovery of .sup.11 CH.sub.3 I of which the half-life is very short.
摘要:
In a process for the synthesis of .sup.11 C-labeled methyl iodide which comprises producing .sup.11 CO.sub.2 by the irradiation of a proton beam, supplying .sup.11 CO.sub.2 gas to a collector of .sup.11 CO.sub.2 gas, bubbling .sup.11 CO.sub.2 gas into a reducing agent solution to reduce .sup.11 CO.sub.2, removing the reducing agent solution by evaporation, synthesizing .sup.11 CH.sub.3 I from the reduced product of .sup.11 CO.sub.2, and recovering .sup.11 CH.sub.3 I by distillation, the termination point of the .sup.11 CO.sub.2 gas supply, the termination point of the bubbling, the termination point of the evaporation of the reducing agent solution or the termination point of the distillatin of .sup.11 CH.sub.3 I is decided by a radiation sensor provided in the vicinity of the reaction vessel or a transfer tube connecting the target box wherein .sup.11 CO.sub.2 gas is generated or a temperature sensor provide in an exhaust tube of the reaction vessel. The synthesizing time is shortened, and the yield of .sup.11 CH.sub.3 I is improved by improving the utilization of .sup.11 CO.sub.2 gas and the recovery of .sup.11 CH.sub.3 I of which the half-life is very short.
摘要:
A process for the synthesis of .sup.13 N-ammonia in target which comprises charging target water and hydrogen into a synthesis apparatus to make a pressurized condition at 0.1-5 kg/cm.sup.2 and irradiating proton beam to the target water which is circulated to produce .sup.13 N-ammonia, a process for the synthesis of .sup.13 N-ammonia in target which comprises bringing the target water containing .sup.13 N-ammonia thus produced into contact with a Na type cation-exchange resin to collect .sup.13 N-ammonia by the cation-exchange, and then bringing the cation-exchange resin into contact with a saline solution to elute the collected .sup.13 N-ammonia into the saline solution, and a process for the synthesis of a labeled compound, at the time of sucking a prescribed amount of the liquid of the target water, saline solution or the like into a syringe and injecting the liquid from the syringe into the above vessel, comprising depressing the piston of the syringe in the state that the pipe connecting the syringe and the vessel has been once closed to detect the displacement of the piston, and in the case that the displacement exceeds a prescribed value, judging that the sucked amount of the liquid into the syringe is short, on the other hand in the case that the displacement is not more than the prescribed value, opening said pipe to inject the liquid into the vessel.The method of the invention can synthesize high purity .sup.13 N-ammonia in a short time which is suitable for the PET (Positron Emission Tomography) system which is a kind of tomography utilized for the dragnosis of disease, etc.
摘要:
The present invention provides an optical disc apparatus that reduces access time while suppressing the emanation of heat from a beam expander. A microcomputer manages the operation time and pause time of a stepping motor constructed to move the movable lens of the beam expander, and in accordance with the duration of an immediately previous pause, limits the number of successive stepping-motor driving actions following the pause time, below a maximum permissible count. When the pause duration is shorter than a threshold value or when the number of successive stepping-motor driving actions reaches the maximum permissible count, the microcomputer starts next driving of the stepping motor after a required waiting time.
摘要:
Provided is a microchip capable of integrating liquid evaporation as an operation on the microchip. In the microchip 10 having a gas flow path 13 inside, liquid is dispersed by capillary action and pooled in a pool portion 12 at a bottom of the gas flow path 13, and at least a part of the liquid pooled in the pool portion 12 is evaporated. As the capillary action is used, the liquid can be dispersed and pooled in the pool portion 12 at the bottom of the gas flow path 13 inside the microchip 10. Besides, the liquid pooled in the pool portion 12 remains in the pool portion by a surface tension even if gas is made to flow in the gas flow path 13 or the gas flow path is evacuated for evaporation. This enables highly efficient evaporation inside the microchip 10.
摘要:
An FDG synthesizer, which comprises: a labeling reaction resin column comprising a column filled with a polymer-supported phase-transfer catalyst resin for trapping an �.sup.18 F! fluoride ion contained in a target water, and performing a labeling reaction between the thus trapped �.sup.18 F! fluoride ion and triflate, on the one hand, and a hydrolysis reaction vessel for receiving a reaction intermediate product obtained from the labeling reaction, and performing a hydrolysis reaction by adding a strong acidic aqueous solution or a strong alkaline aqueous solution thereto, on the other hand. The above-mentioned hydrolysis reaction vessel may be replaced with a cation-exchange resin column having a heating device and a flow rate control device of the reaction intermediate product.
摘要:
In a three-wavelength-compliant optical disk apparatus, the present invention enables to shorten time required for starting the apparatus such as discrimination of an optical disk and adjustment of a beam-expander. At the time of starting the apparatus, the operation of a tray driver which pulls a loaded optical disk within the apparatus is conducted in parallel with the operation of a beam-expander driver which allows a movable lens of the beam-expander to move to a predetermined position in accordance with the kind of optical disk. Further, at the time of discriminating the disk, the number of times an optical disk of a specific kind has continuously been loaded into the apparatus to date is stored in a memory, and a sequence of discriminating the kind of optical disk that is newly discriminated is switched by referring to the history information.
摘要:
An optical disc apparatus and method for recording and reproducing information to/from an optical disc, including discrimination of the optical disc, reading control information in an un-recordable area formed in an inner periphery of the optical disc, conducting focus control based on a focus error signal in a recordable area formed outside of the un-recordable area, and determining an optimum offset value of the focus error signal in the recordable area. Further, adjustment in amplitude of a reproduced signal from an inner periphery of the recordable area is conducted, test-writing in the inner periphery of the recordable area is conducted, test-writing in an outer periphery of the recordable area is conducted, and adjustment in amplitude of a reproduced signal from the outer periphery of the recordable area is conducted. The respective operations are conducted sequentially so as to make the optical disc in a reproducible and recordable condition.
摘要:
An optical disc apparatus having at least two optical condenser lens for recording and reproducing information of an optical disc, comprising: means for discriminating the optical disc; means for reading control information in a ROM area which is formed in an inner periphery of said optical disc; means for conducting focus control in a RAM area which is formed outside of said ROM area; means for conducting adjustment in amplitude of a reproduced signal from an inner periphery of said RAM area; means for conducting a pre-writing (a sample-writing); means for conducting test-writing in the inner periphery of said RAM area; means for conducting test-writing in an outer periphery of said RAM area; and means for conducting adjustment in amplitude of a reproduced signal from the outer periphery of said RAM area, wherein said means conducts the respective operations sequentially, thereby making said optical disc in reproducible and recorable condition, with a short time period and with a smooth confirmation operation.
摘要:
An image forming apparatus including an image holding member, an image forming section that forms an image on the image holding member, a main frame that houses at least the image holding member and the image forming section, a cover body that is mounted to the main frame so as to be able to tilt down and includes a side cover for opening and closing a side surface of the main frame and a top cover for opening and closing a top surface of the main frame; and a unit that is mounted to and dismounted from the side cover by moving in a vertical direction between the top cover and the main frame in a state where the cover body is tilted down, is provided.