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    Method for preparing organic/inorganic hybrid functionalized solids having a triazole ring
    2.
    发明授权
    Method for preparing organic/inorganic hybrid functionalized solids having a triazole ring 有权
    制备具有三唑环的有机/无机混合官能化固体的方法

    公开(公告)号：US08940905B2

    公开(公告)日：2015-01-27

    申请号：US13503292

    申请日：2010-10-06

    申请人： Marie Savonnet ,  David Farrusseng ,  Catherine Pinel ,  Delphine Bazer-Bachi ,  Nicolas Bats ,  Vincent Lecocq

    发明人： Marie Savonnet ,  David Farrusseng ,  Catherine Pinel ,  Delphine Bazer-Bachi ,  Nicolas Bats ,  Vincent Lecocq

    IPC分类号： C07F3/06 ,  C07F5/06 ,  C07F3/00 ,  C07F5/00

    CPC分类号： C07F5/069 ,  C07F3/003 ,  C07F5/003

    摘要： A process is described for the preparation of a functionalized hybrid solid with an organic-inorganic matrix, crystallized, bearing at least one reactive group based on a triazole ring, from a hybrid solid with an organic-inorganic matrix, MOF—NH2, comprising: i/ introduction, in a polar solvent S1, of said crystallized hybrid solid MOF—NH2, of at least one organic compound Q containing a nitride function N3 and at least one intermediate reagent R containing a nitrite function NO2, ii/ reaction of said reaction mixture, iii/ introduction in the reaction mixture of at least one reagent A bearing an alkyne function or an activated cyanide function, at least one Cu-based catalyst C and at least one polar solvent S2, iv/ reaction of said reaction mixture, v/ filtration and then washing and vi/ drying of said crystallized functionalized hybrid solid.

    摘要翻译： 描述了一种制备具有有机 - 无机基质的功能化混合固体的方法，该有机 - 无机基质结晶，具有至少一个基于三唑环的反应性基团，其与有机 - 无机基质MOF-NH 2的混合固体，包括： 在所述结晶的杂化固体MOF-NH 2的极性溶剂S1中引入至少一种含有氮化物官能N 3的有机化合物Q和至少一种含有亚硝酸盐功能NO 2的中间体试剂R，ii /所述反应的反应 混合物，iii /引入至少一种具有炔官能团或活性氰化物功能的试剂A的反应混合物，至少一种Cu基催化剂C和至少一种极性溶剂S2，iv /所述反应混合物的反应，v /过滤，然后洗涤和vi /干燥所述结晶的官能化混合固体。

    PROCESS FOR THE PREPARATION OF MAGADIITE OR KENYAITE FROM AN ORGANIC STRUCTURING AGENT COMPRISING TWO TERMINAL ALCOHOL FUNCTIONS
    4.
    发明申请
    PROCESS FOR THE PREPARATION OF MAGADIITE OR KENYAITE FROM AN ORGANIC STRUCTURING AGENT COMPRISING TWO TERMINAL ALCOHOL FUNCTIONS 失效
    从包含两种终端醇类功能的有机结构剂制备胶体或肯尼亚的方法

    公开(公告)号：US20110268640A1

    公开(公告)日：2011-11-03

    申请号：US13178044

    申请日：2011-07-07

    申请人： Emmanuelle GUILLON ,  Nicolas Bats ,  Antoine Fecant

    发明人： Emmanuelle GUILLON ,  Nicolas Bats ,  Antoine Fecant

    IPC分类号： C01B33/32 ,  C01B33/26

    CPC分类号： C01B33/38

    摘要： Described is a process for the preparation of a crystallised lamellar solid formed by magadiite consisting of implementing in a step (i) mixing of at least one silica source, at least one salt of N,N,N′,N′-tetramethyl-N,N′-dibenzyloctanediammonium, at least one alkali and/or alkaline earth metal M and water and then implementing in a step (ii) hydrothermal treatment of said mixture until said crystallised lamellar solid constituted by magadiite is formed.

    摘要翻译： 描述了制备由magadiite形成的结晶层状固体的方法，其包括在步骤（i）中混合至少一种二氧化硅源，至少一种N，N，N'，N'-四甲基-N ，N'-二苄基辛胺，至少一种碱金属和/或碱土金属M和水，然后在步骤（ii）中实施所述混合物的水热处理，直到形成由magadiite构成的所述结晶的层状固体。

    Process for the preparation of magadiite or kenyaite from an organic structuring agent comprising two terminal alcohol functions
    5.
    发明授权
    Process for the preparation of magadiite or kenyaite from an organic structuring agent comprising two terminal alcohol functions 失效
    用于由包含两个末端醇官能团的有机结构剂制备麦草碱或肯尼亚的方法

    公开(公告)号：US08021637B2

    公开(公告)日：2011-09-20

    申请号：US11956964

    申请日：2007-12-14

    申请人： Emmanuelle Guillon ,  Nicolas Bats ,  Antoine Fecant

    发明人： Emmanuelle Guillon ,  Nicolas Bats ,  Antoine Fecant

    IPC分类号： C01B33/32

    CPC分类号： C01B33/38

    摘要： Described is a process for the preparation of at least one crystallized lamellar solid formed by magadiite or kenyaite consisting of implementing in a step (i) mixing of at least one silica source, at least one organic structuring agent of the formula HO—(CH2)n—OH, with 2≦n≦5, at least one alkali and/or alkaline earth metal M and water and then implementing in a step (ii) hydrothermal treatment of said mixture until at least said crystallized lamellar solid is formed.

    摘要翻译： 描述了由制备由magadiite或kenyaite形成的至少一种结晶的层状固体的方法，其包括在步骤（i）中混合至少一种二氧化硅源，至少一种式HO-（CH 2）的有机结构剂， n-OH，2和nlE; n和nl; 5，至少一种碱金属和/或碱土金属M和水，然后在步骤（ii）中实施所述混合物的水热处理，直到形成至少所述结晶的层状固体。

    IM-13 CRYSTALLIZED SOLID AND ITS PROCESS FOR PREPARATION
    6.
    发明申请
    IM-13 CRYSTALLIZED SOLID AND ITS PROCESS FOR PREPARATION 失效
    IM-13结晶固体及其制备方法

    公开(公告)号：US20100324320A1

    公开(公告)日：2010-12-23

    申请号：US12301889

    申请日：2007-05-10

    申请人： Philippe Caullet ,  Jean-Louis Paillaud ,  Nicolas Bats ,  Yannick Lorgouilloux

    发明人： Philippe Caullet ,  Jean-Louis Paillaud ,  Nicolas Bats ,  Yannick Lorgouilloux

    IPC分类号： C07F7/02

    CPC分类号： C01B39/06 ,  C01B37/00 ,  C01B37/005

    摘要： The invention relates to a crystallized solid, referred to by the name IM-13, which has an X-ray diffraction diagram as provided below. Said solid has a chemical composition that is expressed according to the general formula mXO2: nYO2: pZ2O3: qR : sF : wH2O, where R represents one or more organic radical(s), X represents one or more tetravalent element(s) different from germanium, Y represents germanium, Z represents at least one trivalent element, and F is fluorine.

    摘要翻译： 本发明涉及名称为IM-13的结晶固体，其具有如下提供的X射线衍射图。 所述固体具有根据通式mXO 2：n YO 2：pZ 2 O 3：qR：sF：wH 2 O表示的化学组成，其中R表示一个或多个有机基团，X表示一个或多个与以下不同的四价元素： 锗，Y表示锗，Z表示至少一种三价元素，F表示氟。

    IZM-2 CRYSTALLINE SOLID AND PROCESS FOR ITS PREPARATION
    8.
    发明申请
    IZM-2 CRYSTALLINE SOLID AND PROCESS FOR ITS PREPARATION 有权
    IZM-2晶体固体及其制备方法

    公开(公告)号：US20100272624A1

    公开(公告)日：2010-10-28

    申请号：US12667111

    申请日：2008-05-14

    申请人： Antoine Fecant ,  Nicolas Bats

    发明人： Antoine Fecant ,  Nicolas Bats

    IPC分类号： C01B33/26

    CPC分类号： C01B39/48 ,  B01J20/10 ,  B01J20/18 ,  C01B37/02

    摘要： The invention concerns a crystalline solid designated IZM-2, which has the X ray diffraction diagram given below. Said solid has a chemical composition expressed as the anhydrous base in terms of moles of oxides by the formula XO2:aY2O3:bM2/nO, in which X represents at least one tetravalent element, Y represents at least one trivalent element and M is at least one alkali metal and/or an alkaline-earth metal with valency n, a and b respectively representing the number of moles of Y2O3 and M2/nO; a is in the range 0 to 0.5 and b is in the range 0 to 1.

    摘要翻译： 本发明涉及一种称为IZM-2的结晶固体，其具有下面给出的X射线衍射图。 所述固体具有通过式XO 2：a Y 2 O 3 :bM 2 / nO以氧化物的摩尔数表示为无水碱的化学组成，其中X表示至少一种四价元素，Y表示至少一种三价元素，M至少为 一种碱金属和/或碱土金属，其中n，a和b分别代表Y2O3和M2 / nO的摩尔数; a在0〜0.5的范围内，b在0〜1的范围内。

    PROCESS FOR THE PREPARATION OF MAGADIITE FROM AN ORGANIC STRUCTURING AGENT OF QUATERNARY DIAMMONIUM TYPE
    9.
    发明申请
    PROCESS FOR THE PREPARATION OF MAGADIITE FROM AN ORGANIC STRUCTURING AGENT OF QUATERNARY DIAMMONIUM TYPE 失效
    来自有机结构剂的季铵二氧化物类型的制备方法

    公开(公告)号：US20080152569A1

    公开(公告)日：2008-06-26

    申请号：US11956964

    申请日：2007-12-14

    申请人： Emmanuelle GUILLON ,  Nicolas BATS ,  Antoine FECANT

    发明人： Emmanuelle GUILLON ,  Nicolas BATS ,  Antoine FECANT

    IPC分类号： C01B33/32 ,  C01B33/26

    CPC分类号： C01B33/38

    摘要： Described is a process for the preparation of a crystallised lamellar solid formed by magadiite consisting of implementing in a step (i) mixing of at least one silica source, at least one salt of N,N,N′,N′-tetramethyl-N,N′-dibenzyloctanediammonium, at least one alkali and/or alkaline earth metal M and water and then implementing in a step (ii) hydrothermal treatment of said mixture until said crystallised lamellar solid constituted by magadiite is formed.

    摘要翻译： 描述了制备由magadiite形成的结晶层状固体的方法，其包括在步骤（i）中混合至少一种二氧化硅源，至少一种N，N，N'，N'-四甲基-N ，N'-二苄基辛烷基铵，至少一种碱金属和/或碱土金属M和水，然后在步骤（ii）中实施所述混合物的水热处理，直到形成由magadiite构成的所述结晶的层状固体。