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公开(公告)号：US20140299819A1
公开(公告)日：2014-10-09
申请号：US12004671
申请日：2007-12-20
申请人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
CPC分类号： H01B1/04
摘要： A method for making a carbon nanotube film includes the steps of: (a) adding a plurality of carbon nanotubes into a solvent containing metallic ions, and flocculating the carbon nanotubes to get a floccule structure with the metallic ions therein; (b) reducing the metallic ions into metallic atoms, thereby the metallic atoms being attached onto outer surfaces of the carbon nanotubes to form a floccule structure of carbon nanotubes compounded with metal atoms; and (c) separating the floccule structure compounded with metal atoms from the solvent; and (d) shaping the floccule structure compounded with metal atoms to obtain/get the carbon nanotube film.
摘要翻译： 制造碳纳米管膜的方法包括以下步骤：（a）将多个碳纳米管加入含有金属离子的溶剂中，并使碳纳米管絮凝，得到其中的金属离子的絮状结构; （b）将金属离子还原为金属原子，由此将金属原子附着在碳纳米管的外表面上形成与金属原子复合的碳纳米管的絮凝结构; 和（c）将与金属原子配合的絮凝体结构与溶剂分离; 和（d）使与金属原子复合的絮凝结构成形以获得/获得碳纳米管膜。
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公开(公告)号：US08846144B1
公开(公告)日：2014-09-30
申请号：US12004671
申请日：2007-12-20
申请人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
CPC分类号： H01B1/04
摘要： A method for making a carbon nanotube film includes the steps of: (a) adding a plurality of carbon nanotubes into a solvent containing metallic ions, and flocculating the carbon nanotubes to get a floccule structure with the metallic ions therein; (b) reducing the metallic ions into metallic atoms, thereby the metallic atoms being attached onto outer surfaces of the carbon nanotubes to form a floccule structure of carbon nanotubes compounded with metal atoms; and (c) separating the floccule structure compounded with metal atoms from the solvent; and (d) shaping the floccule structure compounded with metal atoms to obtain/get the carbon nanotube film.
摘要翻译： 制造碳纳米管膜的方法包括以下步骤：（a）将多个碳纳米管加入含有金属离子的溶剂中，并使碳纳米管絮凝，得到其中的金属离子的絮状结构; （b）将金属离子还原为金属原子，由此将金属原子附着在碳纳米管的外表面上形成与金属原子复合的碳纳米管的絮凝结构; 和（c）将与金属原子配合的絮凝体结构与溶剂分离; 和（d）使与金属原子复合的絮凝结构成形以获得/获得碳纳米管膜。
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公开(公告)号：US07993750B2
公开(公告)日：2011-08-09
申请号：US11959144
申请日：2007-12-18
申请人： Ding Wang , Chang-Hong Liu , Peng-Cheng Song , Shou-Shan Fan
发明人： Ding Wang , Chang-Hong Liu , Peng-Cheng Song , Shou-Shan Fan
IPC分类号： B32B9/00
CPC分类号： C23C16/26 , C23C14/046 , H01L23/373 , H01L23/3733 , H01L2924/0002 , Y10T428/30 , H01L2924/00
摘要： A thermal interface material includes an array of carbon nanotubes with interspaces defined therebetween; and a low melting point metallic material filled in the interspaces. A method for fabricating a thermal interface material, the method includes (a) providing an array of carbon nanotubes with interspaces defined therebetween; and (b) depositing a low melting point metallic material on the carbon nanotubes in the interspaces therebetween to form a metallic layer with the array of carbon nanotubes embedded therein, and thereby, achieving the thermal interface material.
摘要翻译： 热界面材料包括其间限定有间隙的碳纳米管阵列; 和填充在间隙中的低熔点金属材料。 一种制造热界面材料的方法，所述方法包括（a）提供碳纳米管阵列，其间限定有间隙; 和（b）在其间的间隙中在碳纳米管上沉积低熔点金属材料以形成嵌入其中的碳纳米管阵列的金属层，从而实现热界面材料。
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公开(公告)号：US20080145570A1
公开(公告)日：2008-06-19
申请号：US11831907
申请日：2007-07-31
申请人： Qiu- Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Qiu- Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
摘要： A method of preparing a carbon nanotube/polymer composite material is provided. The method includes (a) providing a carbon nanotube-based film and a pre-polymer solution; (b) placing the carbon nanotube-based film at a bottom of a container, and pouring the pre-polymer solution in the container; and (c) polymerizing the pre-polymer solution and simultaneously integrating the pre-polymer solution with the carbon nanotube-based film. As such, a carbon nanotube/polymer composite material, including the polymer-impregnated nanotube layer and an upper polymer layer, is obtained. A multi-layer composite can be produced by essentially repeating this process, using the upper polymer layer as the base layer for the formation of the next layer set thereon.
摘要翻译： 提供了制备碳纳米管/聚合物复合材料的方法。 该方法包括（a）提供碳纳米管基膜和预聚物溶液; （b）将碳纳米管基膜放置在容器的底部，并将预聚物溶液倒入容器中; 和（c）使预聚物溶液聚合并同时将预聚物溶液与碳纳米管基膜一体化。 因此，得到包含聚合物浸渍的纳米管层和上层聚合物层的碳纳米管/聚合物复合材料。 可以通过基本上重复该方法来制备多层复合材料，其中使用上聚合物层作为形成其上设置的下一层的基层。
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公开(公告)号：US20080063860A1
公开(公告)日：2008-03-13
申请号：US11831904
申请日：2007-07-31
申请人： PENG-CHENG SONG , QIU-CEN ZHANG , CHANG-HONG LIU , SHOU-SHAN FAN
发明人： PENG-CHENG SONG , QIU-CEN ZHANG , CHANG-HONG LIU , SHOU-SHAN FAN
IPC分类号： B32B9/00
CPC分类号： B32B27/08 , Y10T428/265 , Y10T428/30
摘要： A carbon nanotube/polymer composite is described. The carbon nanotube/polymer composite includes at least one polymer material layer and at least one carbon nanotube/polymer composite layer. The carbon nanotube/polymer layer includes a polymer material and a plurality of carbon nanotubes embedded in the polymer material, wherein the carbon nanotube/polymer layer includes a top surface and a bottom surface opposite to the top surface, at least one of the top surface and bottom surface contacts with the adjacent polymer material layer, and the carbon nanotubes respectively contact at least one respective adjacent carbon nanotube to thereby yield a network of contacting carbon nanotubes.
摘要翻译： 描述了碳纳米管/聚合物复合材料。 碳纳米管/聚合物复合材料包括至少一个聚合物材料层和至少一个碳纳米管/聚合物复合层。 碳纳米管/聚合物层包括聚合物材料和嵌入聚合物材料中的多个碳纳米管，其中碳纳米管/聚合物层包括顶表面和与顶表面相对的底表面，至少一个顶表面 并且底表面与相邻的聚合物材料层接触，并且碳纳米管分别接触至少一个相应的相邻碳纳米管，从而产生接触碳纳米管的网络。
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公开(公告)号：US07988896B2
公开(公告)日：2011-08-02
申请号：US11831907
申请日：2007-07-31
申请人： Qiu-Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Qiu-Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
IPC分类号： B29C39/12
摘要： A method of preparing a carbon nanotube/polymer composite material is provided. The method includes (a) providing a carbon nanotube-based film and a pre-polymer solution; (b) placing the carbon nanotube-based film at a bottom of a container, and pouring the pre-polymer solution in the container; and (c) polymerizing the pre-polymer solution and simultaneously integrating the pre-polymer solution with the carbon nanotube-based film. As such, a carbon nanotube/polymer composite material, including the polymer-impregnated nanotube layer and an upper polymer layer, is obtained. A multi-layer composite can be produced by essentially repeating this process, using the upper polymer layer as the base layer for the formation of the next layer set thereon.
摘要翻译： 提供了制备碳纳米管/聚合物复合材料的方法。 该方法包括（a）提供碳纳米管基膜和预聚物溶液; （b）将碳纳米管基膜放置在容器的底部，并将预聚物溶液倒入容器中; 和（c）使预聚物溶液聚合并同时将预聚物溶液与碳纳米管基膜一体化。 因此，得到包含聚合物浸渍的纳米管层和上层聚合物层的碳纳米管/聚合物复合材料。 可以通过基本上重复该方法来制备多层复合材料，其中使用上聚合物层作为形成其上设置的下一层的基层。
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公开(公告)号：US08247024B2
公开(公告)日：2012-08-21
申请号：US11779244
申请日：2007-07-17
申请人： Qiu-Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Qiu-Cen Zhang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
CPC分类号： H01J9/025
摘要： A method for manufacturing a carbon nanotube/polymer composite includes the steps of: (a) providing a carbon nanotube array formed on a substrate in a container; (b) providing a prepolymer of polymethyl methacrylate (PMMA); (c) putting the prepolymer into the container for a period of over 30 minutes to fill in clearances of the carbon nanotube array; and (d) polymerizing the prepolymer film at a temperature of about 50° C. to 60° C. for a period of about 1 hour to 4 hours and then heating the prepolymer film to about 90° C. to 100° C. to form a polymer film, the carbon nanotube array thereby being embedded within the polymer film.
摘要翻译： 制造碳纳米管/聚合物复合体的方法包括以下步骤：（a）提供形成在容器中的基板上的碳纳米管阵列; （b）提供聚甲基丙烯酸甲酯（PMMA）的预聚物; （c）将预聚物放入容器中30分钟以上以填充碳纳米管阵列的间隙; 和（d）在约50℃至60℃的温度下将预聚物膜聚合约1小时至4小时，然后将预聚物膜加热至约90℃至100℃至 形成聚合物膜，由此将碳纳米管阵列嵌入聚合物膜内。
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公开(公告)号：US07785669B2
公开(公告)日：2010-08-31
申请号：US11967124
申请日：2007-12-29
申请人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
发明人： Ding Wang , Peng-Cheng Song , Chang-Hong Liu , Shou-Shan Fan
CPC分类号： B82Y30/00 , Y10S977/745 , Y10T428/1328 , Y10T428/1352 , Y10T428/24132 , Y10T428/30
摘要： A method for making a high-density carbon nanotube array includes the steps of: (a) providing a substrate having a carbon nanotube array formed thereon; (b) providing an elastic film; (c) stretching the elastic film uniformly, and covering the elastic film to the carbon nanotube array; (d) exerting a pressure uniformly on the elastic film, and shrinking the carbon nanotube array and the elastic film under the pressure; and (e) separating the nanotube array from the elastic film to acquire a high-density carbon nanotube array.
摘要翻译： 制造高密度碳纳米管阵列的方法包括以下步骤：（a）提供其上形成有碳纳米管阵列的基板; （b）提供弹性膜; （c）均匀地拉伸弹性膜，并将弹性膜覆盖到碳纳米管阵列上; （d）在弹性膜上施加均匀的压力，并在压力下收缩碳纳米管阵列和弹性膜; 和（e）从弹性膜分离纳米管阵列以获得高密度碳纳米管阵列。
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公开(公告)号：US20080241545A1
公开(公告)日：2008-10-02
申请号：US11959144
申请日：2007-12-18
申请人： DING WANG , CHANG-HONG LIU , PENG-CHENG SONG , SHOU-SHAN FAN
发明人： DING WANG , CHANG-HONG LIU , PENG-CHENG SONG , SHOU-SHAN FAN
CPC分类号： C23C16/26 , C23C14/046 , H01L23/373 , H01L23/3733 , H01L2924/0002 , Y10T428/30 , H01L2924/00
摘要： A thermal interface material includes an array of carbon nanotubes with interspaces defined therebetween; and a low melting point metallic material filled in the interspaces. A method for fabricating a thermal interface material, the method includes (a) providing an array of carbon nanotubes with interspaces defined therebetween; and (b) depositing a low melting point metallic material on the carbon nanotubes in the interspaces therebetween to form a metallic layer with the array of carbon nanotubes embedded therein, and thereby, achieving the thermal interface material.
摘要翻译： 热界面材料包括其间限定有间隙的碳纳米管阵列; 和填充在间隙中的低熔点金属材料。 一种制造热界面材料的方法，所述方法包括（a）提供碳纳米管阵列，其间限定有间隙; 和（b）在其间的间隙中在碳纳米管上沉积低熔点金属材料以形成嵌入其中的碳纳米管阵列的金属层，从而实现热界面材料。
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公开(公告)号：US20080160866A1
公开(公告)日：2008-07-03
申请号：US11779244
申请日：2007-07-17
申请人： QIU-CEN ZHANG , PENG-CHENG SONG , CHANG-HONG LIU , SHOU-SHAN FAN
发明人： QIU-CEN ZHANG , PENG-CHENG SONG , CHANG-HONG LIU , SHOU-SHAN FAN
IPC分类号： H01J9/02
CPC分类号： H01J9/025
摘要： A method for manufacturing a carbon nanotube/polymer composite includes the steps of: (a) providing a carbon nanotube array formed on a substrate in a container; (b) providing a prepolymer of polymethyl methacrylate (PMMA); (c) putting the prepolymer into the container for a period of over 30 minutes to fill in clearances of the carbon nanotube array; and (d) polymerizing the prepolymer film at a temperature of about 50° C. to 60° C. for a period of about 1 hour to 4 hours and then heating the prepolymer film to about 90° C. to 100° C. to form a polymer film, the carbon nanotube array thereby being embedded within the polymer film.
摘要翻译： 制造碳纳米管/聚合物复合体的方法包括以下步骤：（a）提供形成在容器中的基板上的碳纳米管阵列; （b）提供聚甲基丙烯酸甲酯（PMMA）的预聚物; （c）将预聚物放入容器中30分钟以上以填充碳纳米管阵列的间隙; 和（d）在约50℃至60℃的温度下将预聚物膜聚合约1小时至4小时，然后将预聚物膜加热至约90℃至100℃至 形成聚合物膜，由此将碳纳米管阵列嵌入聚合物膜内。
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