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1.发明授权公开(公告)号：US10682634B2
公开(公告)日：2020-06-16
申请号：US14671258
申请日：2015-03-27
申请人： REACTION 35, LLC
发明人： Peter K. Stoimenov
摘要： A method of manufacturing a modified zeolite catalyst may include reacting a zeolite with a metal salt to form a zeolite/metal salt complex. The zeolite may be a ZSM-5 or ZSM-11. The method may include heating the zeolite/metal salt complex to form an intermediate modified zeolite, and reacting the intermediate modified zeolite with an acid. The method may include ion exchanging the intermediate modified zeolite following the reaction with the acid to form a modified zeolite catalyst.
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公开(公告)号：US10040734B2
公开(公告)日：2018-08-07
申请号：US15511969
申请日：2015-09-15
申请人： REACTION 35, LLC
摘要： A method includes brominating a butanes feed stream including i-butane in a bromination reactor to form a bromination effluent stream including t-butyl bromide. The method includes dehydrobrominating the t-butyl bromide to form isobutylene. Another method includes brominating a mixed pentanes feed stream including i-pentane and n-pentane in a bromination reactor to form a bromination effluent stream including t-pentyl bromide. The method includes dehydrobrominating the t-pentyl bromide to form isoamylene and HBr.
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公开(公告)号：US20140356269A1
公开(公告)日：2014-12-04
申请号：US14289177
申请日：2014-05-28
申请人： Reaction 35, LLC
发明人： Philip Grosso
CPC分类号： B01D19/0036 , B01D53/002 , B01D53/68 , B01D2257/2042 , B01D2257/2045 , B01D2257/2047 , C01B7/0706 , C01B7/0712 , C01B7/093 , C01B7/135
摘要： A method includes injecting a feed stream including a hydrogen halide and water into a vapor liquid separator. The feed stream has a liquid phase and a vapor phase. The method further includes separating the liquid phase and the vapor phase in the vapor liquid separator to form condensate and vapor, and discharging the condensate from the vapor liquid separator in a liquid stream. The method also includes discharging the vapor from the vapor liquid separator in a vapor stream.
摘要翻译： 一种方法包括将包括卤化氢和水的进料流注入蒸气分离器中。 进料流具有液相和气相。 该方法还包括分离汽相液体分离器中的液相和气相以形成冷凝物和蒸气，并将液体流中的蒸汽液分离器的冷凝物排出。 该方法还包括以蒸气流从蒸气分离器排出蒸汽。
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公开(公告)号：US20240359981A1
公开(公告)日：2024-10-31
申请号：US18762885
申请日：2024-07-03
申请人： REACTION 35, LLC
摘要： A process includes supplying a bromide brine and removing organic compounds from the bromide brine. The method also includes acidifying the bromide brine to form a stream containing hydrobromic acid and separating the hydrobromic acid from the stream containing hydrobromic acid.
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公开(公告)号：US20230234846A1
公开(公告)日：2023-07-27
申请号：US18100470
申请日：2023-01-23
申请人： REACTION 35, LLC
摘要： A process includes supplying a bromide brine and removing organic compounds from the bromide brine. The method also includes acidifying the bromide brine to form a stream containing hydrobromic acid and separating the hydrobromic acid from the stream containing hydrobromic acid.
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6.发明申请公开(公告)号：US20220009775A1
公开(公告)日：2022-01-13
申请号：US17367917
申请日：2021-07-06
申请人： REACTION 35, LLC
发明人： John WAYCUILIS
摘要： A hydrogen bromide (HBr) oxidation/quench system includes a heat exchanger reactor and an adiabatic catalytic reactor in fluid communication with the heat exchanger reactor. The system also includes a quench vessel, the quench vessel in fluid communication with the adiabatic catalytic reactor. The quench vessel has a flange. In addition, the system includes a joined three phase separator and absorber column, wherein both the three phase separator and the absorber column are in fluid communication with the quench vessel and an aqueous stripping column in fluid communication the heat exchanger reactor and the absorber column.
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公开(公告)号：US20170291864A1
公开(公告)日：2017-10-12
申请号：US15511969
申请日：2015-09-15
申请人： REACTION 35, LLC
CPC分类号： C07C17/23 , C07C1/30 , C07C5/2789 , C07C5/44 , C07C11/02 , C07C17/10 , C07C2527/08 , C07C2527/125 , C07C9/18 , C07C9/12 , C07C11/09 , C07C11/10 , C07C19/075
摘要： A method includes brominating a butanes feed stream including i-butane in a bromination reactor to form a bromination effluent stream including t-butyl bromide. The method includes dehydrobrominating the t-butyl bromide to form isobutylene. Another method includes brominating a mixed pentanes feed stream including i-pentane and n-pentane in a bromination reactor to form a bromination effluent stream including t-pentyl bromide. The method includes dehydrobrominating the t-pentyl bromide to form isoamylene and HBr.
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公开(公告)号：US20150361008A1
公开(公告)日：2015-12-17
申请号：US14734683
申请日：2015-06-09
申请人： REACTION 35, LLC
IPC分类号： C07C1/30 , C07C17/156 , C07C17/10
CPC分类号： C07C1/30 , C07C5/23 , C07C5/2512 , C07C5/2518 , C07C17/10 , C07C2521/06 , C07C2521/08 , C07C2521/10 , C07C2527/22 , C07C2527/224 , C07C2529/035 , C07C2529/04 , C07C11/167 , C07C19/075
摘要： Olefins and diolefins, such as 1,3-butiadiene, may be produced by a method utilizing a series of bromination and dehydrobromination reactions. Bromine may be reacted with n-butane to form dibromobutane. The dibromobutanes may be dehydrobrominating to form 1,3-butadiene. The method may include reacting butene with bromine to form bromobutenes, and dehydrobrominating the bromobutenes to form 1,3-butadiene. The method may include reacting butene with hydrogen bromide in the presence of oxygen to form bromobutenes, and dehydrobrominating the bromobutenes to form 1,3-butadiene. The method may include reacting butene with bromine to form dibromobutanes, and dehydrobrominating the dibromobutanes to form 1,3-butadiene.
摘要翻译： 烯烃和二烯烃如1,3-丁二烯可以通过使用一系列溴化和脱溴溴化反应的方法制备。 溴可以与正丁烷反应形成二溴丁烷。 二溴丁烷可以是脱氢溴化以形成1,3-丁二烯。 该方法可以包括使丁烯与溴反应形成溴丁烯，并将溴代丁烷脱溴形成1,3-丁二烯。 该方法可以包括在氧气存在下使丁烯与溴化氢反应形成溴代丁烷，并将溴代丁烷脱溴形成1,3-丁二烯。 该方法可以包括使丁烯与溴反应以形成二溴丁烷，并将二溴丁烷脱氢形成1,3-丁二烯。
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公开(公告)号：US10322987B2
公开(公告)日：2019-06-18
申请号：US16020545
申请日：2018-06-27
申请人： REACTION 35, LLC
摘要： A method includes brominating a butanes feed stream including i-butane in a bromination reactor to form a bromination effluent stream including t-butyl bromide. The method includes dehydrobrominating the t-butyl bromide to form isobutylene. Another method includes brominating a mixed pentanes feed stream including i-pentane and n-pentane in a bromination reactor to form a bromination effluent stream including t-pentyl bromide. The method includes dehydrobrominating the t-pentyl bromide to form isoamylene and HBr.
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公开(公告)号：US20180305279A1
公开(公告)日：2018-10-25
申请号：US16020545
申请日：2018-06-27
申请人： REACTION 35, LLC
IPC分类号： C07C17/23 , C07C5/44 , C07C17/10 , C07C5/27 , C07C11/02 , C07C1/30 , C07C9/18 , C07C9/12 , C07C11/09 , C07C11/10 , C07C19/075
CPC分类号： C07C17/23 , C07C1/30 , C07C5/2789 , C07C5/44 , C07C11/02 , C07C17/10 , C07C2527/08 , C07C2527/125 , C07C9/18 , C07C9/12 , C07C11/09 , C07C11/10 , C07C19/075
摘要： A method includes brominating a butanes feed stream including i-butane in a bromination reactor to form a bromination effluent stream including t-butyl bromide. The method includes dehydrobrominating the t-butyl bromide to form isobutylene. Another method includes brominating a mixed pentanes feed stream including i-pentane and n-pentane in a bromination reactor to form a bromination effluent stream including t-pentyl bromide. The method includes dehydrobrominating the t-pentyl bromide to form isoamylene and HBr.
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