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公开(公告)号：US08889293B2
公开(公告)日：2014-11-18
申请号：US13652610
申请日：2012-10-16
申请人： Xiang-Ming He , Li Wang , Jian-Jun Li , Jian Gao , Wen-Ting Sun
发明人： Xiang-Ming He , Li Wang , Jian-Jun Li , Jian Gao , Wen-Ting Sun
IPC分类号： H01M4/60
CPC分类号： H01M4/137 , H01M4/131 , H01M4/136 , H01M4/5825 , H01M4/608 , H01M10/0525
摘要： A lithium ion battery includes a cathode electrode, an anode electrode, and an electrolyte. The anode electrode is spaced from the cathode electrode. The anode electrode includes an anode active material. The anode active material includes sulfur grafted poly(pyridinopyridine). The sulfur grafted poly(pyridinopyridine) includes a poly(pyridinopyridine) matrix and sulfur dispersed in the poly(pyridinopyridine) matrix. The electrolyte is located between the cathode electrode and the anode electrode.
摘要翻译： 锂离子电池包括阴极电极，阳极电极和电解质。 阳极与阴极隔开。 阳极电极包括阳极活性材料。 阳极活性材料包括硫接枝的聚（吡啶并吡啶）。 硫接枝的聚（吡啶并吡啶）包括分散在聚（吡啶并吡啶）基质中的聚（吡啶并吡啶）基质和硫。 电解质位于阴极和阳极之间。
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公开(公告)号：US20130302678A1
公开(公告)日：2013-11-14
申请号：US13652610
申请日：2012-10-16
申请人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN GAO , WEN-TING SUN
发明人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN GAO , WEN-TING SUN
IPC分类号： H01M4/60
CPC分类号： H01M4/137 , H01M4/131 , H01M4/136 , H01M4/5825 , H01M4/608 , H01M10/0525
摘要： A lithium ion battery includes a cathode electrode, an anode electrode, and an electrolyte. The anode electrode is spaced from the cathode electrode. The anode electrode includes an anode active material. The anode active material includes sulfur grafted poly(pyridinopyridine). The sulfur grafted poly(pyridinopyridine) includes a poly(pyridinopyridine) matrix and sulfur dispersed in the poly(pyridinopyridine) matrix. The electrolyte is located between the cathode electrode and the anode electrode.
摘要翻译： 锂离子电池包括阴极电极，阳极电极和电解质。 阳极与阴极隔开。 阳极电极包括阳极活性材料。 阳极活性材料包括硫接枝的聚（吡啶并吡啶）。 硫接枝的聚（吡啶并吡啶）包括分散在聚（吡啶并吡啶）基质中的聚（吡啶并吡啶）基质和硫。 电解质位于阴极和阳极之间。
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3.发明授权Lithium ion phosphate hierarchical structure, method for making the same, and lithium ion battery using the same 有权磷酸锂离子分层结构，制造方法和使用其的锂离子电池公开(公告)号：US08962186B2
公开(公告)日：2015-02-24
申请号：US13457554
申请日：2012-04-27
申请人： Li Wang , Xiang-Ming He , Wen-Ting Sun , Jian-Jun Li , Xian-Kun Huang , Jian Gao
发明人： Li Wang , Xiang-Ming He , Wen-Ting Sun , Jian-Jun Li , Xian-Kun Huang , Jian Gao
CPC分类号： H01M4/5825 , C01B25/45
摘要： A lithium iron phosphate hierarchical structure includes a plurality of lithium iron phosphate nano sheets and has an overall spherical-shaped structure. The overall spherical-shaped structure is constructed by a plurality of lithium iron phosphate nano sheets layered together. A method for making a lithium iron phosphate hierarchical structure includes several steps. In the method, a lithium ion contained liquid solution, a ferrous ion contained liquid solution, and a phosphate ion contained liquid solution are respectively provided. A concentration of lithium ions in the lithium ion contained liquid solution is equal to or larger than 1.8 mol/L. The lithium ion contained liquid solution, the ferrous ion contained liquid solution, and the phosphate ion contained liquid solution are mixed to form a liquid mixture. The liquid mixture is heated in a sealed reactor to form the lithium iron phosphate hierarchical structure.
摘要翻译： 磷酸铁锂层状结构包括多个磷酸铁锂纳米片，并且具有整体的球形结构。 整个球形结构由层叠在一起的多个磷酸铁锂纳米片构成。 制备磷酸铁锂层状结构的方法包括几个步骤。 在该方法中，分别设置锂离子液体溶液，含有亚铁离子的液体溶液和含有磷酸根离子的液体溶液。 锂离子含有的液体溶液中的锂离子浓度等于或大于1.8mol / L。 锂离子含有的液体溶液，含铁离子的液体溶液和含磷酸根离子的液体溶液混合形成液体混合物。 将液体混合物在密封的反应器中加热以形成磷酸铁锂分层结构。
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公开(公告)号：US20130307485A1
公开(公告)日：2013-11-21
申请号：US13652613
申请日：2012-10-16
申请人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN GAO , WEN-TING SUN
发明人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN GAO , WEN-TING SUN
IPC分类号： H02J7/00
CPC分类号： H01M4/364 , H01M4/38 , H01M4/604 , H01M4/608 , H01M10/052 , H01M10/0525 , H01M10/446 , Y02E60/122
摘要： A method for cycling a sulfur composite lithium ion battery includes a step of charging and discharging the sulfur composite lithium ion battery at a first voltage range between a predetermined highest voltage and a predetermined lowest voltage. The lithium ion battery includes an electrode active material. The electrode active material includes a sulfur composite. The step of charging and discharging satisfies at least one conditions of (1) and (2): (1) the predetermined lowest voltage of the first voltage range is larger than a discharge cutoff voltage of the sulfur composite; and (2) the predetermined highest voltage of the first voltage range is smaller than a charge cutoff voltage of the sulfur composite. A method for using a sulfur composite as an electrode active material of a lithium ion battery is also disclosed.
摘要翻译： 硫复合锂离子电池循环的方法包括在预定的最高电压和预定的最低电压之间的第一电压范围内对硫化合物锂离子电池进行充电和放电的步骤。 锂离子电池包括电极活性材料。 电极活性物质包括硫化合物。 充放电步骤满足（1）和（2）的至少一个条件：（1）第一电压范围的预定最低电压大于硫复合物的放电截止电压; 和（2）第一电压范围的预定最高电压小于硫复合材料的充电截止电压。 还公开了使用硫化合物作为锂离子电池的电极活性物质的方法。
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5.发明申请LITHIUM ION PHOSPHATE HIERARCHICAL STRUCTURE, METHOD FOR MAKING THE SAME, AND LITHIUM ION BATTERY USING THE SAME 有权锂离子磷酸盐分层结构，其制造方法和使用该锂离子电池的锂离子电池公开(公告)号：US20130136989A1
公开(公告)日：2013-05-30
申请号：US13457554
申请日：2012-04-27
申请人： LI WANG , XIANG-MING HE , WEN-TING SUN , JIAN-JUN LI , XIAN-KUN HUANG , JIAN GAO
发明人： LI WANG , XIANG-MING HE , WEN-TING SUN , JIAN-JUN LI , XIAN-KUN HUANG , JIAN GAO
CPC分类号： H01M4/5825 , C01B25/45
摘要： A lithium iron phosphate hierarchical structure includes a plurality of lithium iron phosphate nano sheets and has an overall spherical-shaped structure. The overall spherical-shaped structure is constructed by a plurality of lithium iron phosphate nano sheets layered together. A method for making a lithium iron phosphate hierarchical structure includes several steps. In the method, a lithium ion contained liquid solution, a ferrous ion contained liquid solution, and a phosphate ion contained liquid solution are respectively provided. A concentration of lithium ions in the lithium ion contained liquid solution is equal to or larger than 1.8 mol/L. The lithium ion contained liquid solution, the ferrous ion contained liquid solution, and the phosphate ion contained liquid solution are mixed to form a liquid mixture. The liquid mixture is heated in a sealed reactor to form the lithium iron phosphate hierarchical structure.
摘要翻译： 磷酸铁锂层状结构包括多个磷酸铁锂纳米片，并且具有整体的球形结构。 整个球形结构由层叠在一起的多个磷酸铁锂纳米片构成。 制备磷酸铁锂层状结构的方法包括几个步骤。 在该方法中，分别设置锂离子液体溶液，含有亚铁离子的液体溶液和含有磷酸根离子的液体溶液。 锂离子含有的液体溶液中的锂离子浓度等于或大于1.8mol / L。 锂离子含有的液体溶液，含铁离子的液体溶液和含磷酸根离子的液体溶液混合形成液体混合物。 将液体混合物在密封的反应器中加热以形成磷酸铁锂分层结构。
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公开(公告)号：US08372919B2
公开(公告)日：2013-02-12
申请号：US13051117
申请日：2011-03-18
申请人： Xiang-Ming He , Li Wang , Wei-Hua Pu , Wen-Ting Sun , Jian-Jun Li
发明人： Xiang-Ming He , Li Wang , Wei-Hua Pu , Wen-Ting Sun , Jian-Jun Li
CPC分类号： C08F8/34 , C08F8/48 , C08F120/44
摘要： In a method for making sulfurized polyacrylonitrile, polyacrylonitrile, a first solvent, a catalyst, and sulfur or sodium thiosulfate are provided. The polyacrylonitrile is dissolved in the first solvent to form a polyacrylonitrile solution. The catalyst is uniformly dispersed in the polyacrylonitrile solution. The polyacrylonitrile solution with the catalyst is heated to induce a cyclizing reaction of the polyacrylonitrile, thereby forming a first conjugated polymer solution with a conjugated polymer. The sulfur or sodium thiosulfate is uniformly mixed with the conjugated polymer to form a mixture. The mixture is heated to form sulfurized polyacrylonitrile.
摘要翻译： 在制备硫化聚丙烯腈的方法中，提供聚丙烯腈，第一溶剂，催化剂和硫代硫代硫酸钠。 将聚丙烯腈溶解在第一溶剂中以形成聚丙烯腈溶液。 催化剂均匀分散在聚丙烯腈溶液中。 加热具有催化剂的聚丙烯腈溶液引起聚丙烯腈的环化反应，由此与共轭聚合物形成第一共轭聚合物溶液。 将硫或硫代硫酸钠与共轭聚合物均匀混合以形成混合物。 将混合物加热以形成硫化聚丙烯腈。
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公开(公告)号：US20120097235A1
公开(公告)日：2012-04-26
申请号：US13051148
申请日：2011-03-18
申请人： XIANG-MING HE , LI WANG , WEI-HUA PU , WEN-TING SUN , JIAN-JUN LI
发明人： XIANG-MING HE , LI WANG , WEI-HUA PU , WEN-TING SUN , JIAN-JUN LI
CPC分类号： H01L51/004 , C08F8/48 , H01L51/424 , C08F120/44
摘要： The present disclosure relates to a method for making a conjugated polymer. In the method, polyacrylonitrile, a solvent, and a catalyst are provided. The polyacrylonitrile is dissolved in the solvent to form a polyacrylonitrile solution. The catalyst is uniformly dispersed into the polyacrylonitrile solution. The polyacrylonitrile solution with the catalyst is heated to induce a cyclizing reaction of the polyacrylonitrile, thereby forming a conjugated polymer solution with the conjugated polymer dissolved therein.
摘要翻译： 本发明涉及制备共轭聚合物的方法。 在该方法中，提供聚丙烯腈，溶剂和催化剂。 将聚丙烯腈溶解在溶剂中以形成聚丙烯腈溶液。 催化剂均匀分散在聚丙烯腈溶液中。 将具有催化剂的聚丙烯腈溶液加热以引起聚丙烯腈的环化反应，从而形成共轭聚合物溶液，其中共轭聚合物溶解在其中。
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公开(公告)号：US20120059085A1
公开(公告)日：2012-03-08
申请号：US13051123
申请日：2011-03-18
申请人： XIANG-MING HE , LI WANG , WEI-HUA PU , WEN-TING SUN , JIAN-JUN LI
发明人： XIANG-MING HE , LI WANG , WEI-HUA PU , WEN-TING SUN , JIAN-JUN LI
CPC分类号： H01M4/137 , C08F8/48 , H01M4/1399 , H01M4/604 , H01M10/052 , C08F120/44
摘要： The present disclosure relates to a method for making a conjugated polymer. In the method, polyacrylonitrile, a solvent, and a catalyst are provided. The polyacrylonitrile is dissolved in the solvent to form a polyacrylonitrile solution. The catalyst is uniformly dispersed into the polyacrylonitrile solution. The polyacrylonitrile solution with the catalyst is heated to induce a cyclizing reaction of the polyacrylonitrile, thereby forming a conjugated polymer solution with conjugated polymer.
摘要翻译： 本发明涉及制备共轭聚合物的方法。 在该方法中，提供聚丙烯腈，溶剂和催化剂。 将聚丙烯腈溶解在溶剂中以形成聚丙烯腈溶液。 催化剂均匀分散在聚丙烯腈溶液中。 将具有催化剂的聚丙烯腈溶液加热以引起聚丙烯腈的环化反应，从而与共轭聚合物形成共轭聚合物溶液。
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公开(公告)号：US08980367B2
公开(公告)日：2015-03-17
申请号：US13650300
申请日：2012-10-12
申请人： Li Wang , Xiang-Ming He , Wen-Ting Sun , Jian-Jun Li
发明人： Li Wang , Xiang-Ming He , Wen-Ting Sun , Jian-Jun Li
CPC分类号： H01M4/04 , B82Y30/00 , H01M4/13 , H01M4/139 , H01M4/38 , H01M4/663 , Y02E60/12 , Y02E60/122 , Y02P70/54
摘要： A method for making an anode active material is described. The anode active material includes a phosphorus composite material. In the method, a solid-state red phosphorus and a porous conductive carbon material are provided. The solid-state red phosphorus and the porous conductive carbon material are spaced disposed in a vessel and the vessel is sealed. The solid-state red phosphorus is sublimed by heating the vessel to make the sublimed red phosphorus diffused in the porous conductive carbon material. The sublimed red phosphorus is condensed. The condensed red phosphorus adsorbs in the porous conductive carbon material to form the phosphorus composite material.
摘要翻译： 对负极活性物质的制造方法进行说明。 阳极活性材料包括磷复合材料。 在该方法中，提供固态红磷和多孔导电碳材料。 固态红磷和多孔导电碳材料间隔开设置在容器中，容器被密封。 通过加热容器使固态红磷升华，使升华的红磷在多孔导电碳材料中扩散。 升华的红磷被浓缩。 浓缩的红磷吸附在多孔导电碳材料中以形成磷复合材料。
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公开(公告)号：US20130171055A1
公开(公告)日：2013-07-04
申请号：US13554127
申请日：2012-07-20
申请人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN-WEI GUO , WEN-TING SUN , JIAN-GUO REN
发明人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN-WEI GUO , WEN-TING SUN , JIAN-GUO REN
摘要： In the method for making graphene, an electrolyte solution is formed by dissolving an electrolyte lithium salt in an organic solvent. Lithium ions are separated out from the electrolyte lithium salt in the electrolyte solution. Metal lithium and graphite are disposed in the electrolyte solution, and the metal lithium and the graphite are in contact with each other. In the electrolyte solution, lithium ions and organic solvent molecules jointly insert between adjacent layers of the graphite to form a graphite intercalation compound. The graphene is peeled off from the graphite intercalation compound.
摘要翻译： 在制造石墨烯的方法中，通过将电解质锂盐溶解在有机溶剂中形成电解质溶液。 从电解液中的电解质锂盐中分离出锂离子。 金属锂和石墨配置在电解液中，金属锂和石墨彼此接触。 在电解液中，锂离子和有机溶剂分子在相邻的石墨层之间共同插入以形成石墨插层化合物。 石墨烯从石墨插层化合物上剥离出来。
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