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    Synthesis of .alpha.-fluorocarbonyl compounds
    6.
    发明授权
    Synthesis of .alpha.-fluorocarbonyl compounds 失效
    α-氟羰基化合物的合成

    公开(公告)号：US4215044A

    公开(公告)日：1980-07-29

    申请号：US32347

    申请日：1979-04-23

    申请人： William J. Middleton

    发明人： William J. Middleton

    IPC分类号： C07B39/00 ,  C07C45/30 ,  C07C45/51 ,  C07C51/363 ,  C07D243/24

    CPC分类号： C07D243/24 ,  C07B39/00 ,  C07C45/30 ,  C07C45/511 ,  C07C51/363

    摘要： Process for preparing an organic compound of the formula R.sup.2 R.sup.2 CFC(O)R.sup.3, which process comprises contacting and reacting in a reaction mixture which includes an inert solvent, at a temperature of -40.degree. C. to -100.degree. C., ROF and ##STR1## R is polyfluoroperhaloalkyl of 1-6 carbon atoms or FOCF.sub.2 ; R.sup.1 is hydrocarbyl of 1-6 carbon atoms;each R.sup.2 is selected from H, alkyl of 1-17 carbon atoms, cycloalkyl of 3-6 carbon atoms, aryl, heteroaryl and such alkyl, cycloalkyl, aryl and heteroaryl substituted by halogen or alkoxy of 1-6 carbon atoms;R.sup.3 is selected from H, alkyl and haloalkyl of 1-16 carbon atoms, cycloalkyl of 3-10 carbon atoms, aryl and haloaryl, OSi(R.sup.1).sub.3, OH, NH.sub.2, alkoxy of 1-6 carbon atoms, aryloxy, NHR.sup.1 and NR.sup.1.sub.2 wherein R.sup.1 is alkyl of 1-6 carbon atoms, N-arylamino and nitrogen or sulfur heterocyclic of 4-5 carbon atoms;R.sup.3 and one R.sup.2 taken together is a diradical which with the C.dbd.C group is carbocyclic, heterocyclic or haloheterocyclic, and recovering from the reaction mixture the compound of the formula R.sup.2 R.sup.2 CFC(O)R.sup.3.

    摘要翻译： 制备式R2R2CFC（O）R3的有机化合物的方法，该方法包括在-40℃至-100℃的温度下，在包含惰性溶剂的反应混合物中使ROF和 图像> R是1-6个碳原子的多氟卤代烷基或FOCF 2; R1是1-6个碳原子的烃基; 每个R 2选自H，1-17个碳原子的烷基，3-6个碳原子的环烷基，芳基，杂芳基和被1-6个碳原子的卤素或烷氧基取代的烷基，环烷基，芳基和杂芳基; R3选自H，烷基和1-16个碳原子的卤代烷基，3-10个碳原子的环烷基，芳基和卤代芳基，OSi（R1）3，OH，NH2，1-6个碳原子的烷氧基，芳氧基，NHR1和 NR12，其中R1是1-6个碳原子的烷基，具有4-5个碳原子的N-芳基氨基和氮或硫杂环; R 3和R 2一起是一个双基，其中C = C基团是碳环，杂环或卤素杂环，并从反应混合物中回收式R2R2CFC（O）R3的化合物。

    Electrical connector for spiral antenna and resistive/capacitive contact therefor
    8.
    发明授权
    Electrical connector for spiral antenna and resistive/capacitive contact therefor 失效
    用于螺旋天线和电阻/电容接触的电连接器

    公开(公告)号：US4636802A

    公开(公告)日：1987-01-13

    申请号：US665634

    申请日：1984-10-29

    申请人： William J. Middleton, Jr.

    发明人： William J. Middleton, Jr.

    IPC分类号： H01Q9/27 ,  H01Q1/36

    CPC分类号： H01Q9/27

    摘要： The problem of recurrent solder joint failure in spiral antennas is solved by the present invention through the use of resistive/capacitive contacts. Specifically, an electrical connector is provided for connecting opposed conductors disposed on a stripline, to a spiral antenna having a pair of dipole conductors disposed on a substrate. The connector includes a housing having a base, and a sidewall for supporting the substrate. A center post having first and second ends, and a cylindrical aperture, is mounted in the housing. The substrate is secured to the first end of the center post, the second end thereof secured to the base of the housing. A stripline contact snubber is supported in an end of the cylindrical aperture adjacent the substrate and receives the stripline. To ensure RF continuity between the stripline conductors and the dipole conductors, one or more mechanically compliant, leaf spring resistive/capacitive contacts are provided. Each of the resistive/capacitive contacts preferably includes a first portion soldered to an opposed conductor of the stripline, and a second portion extending from the first portion. Alternatively, each contact may be an integral extension of one of the stripline conductors. The second portion of each resistive/capacitive contact is compressed between the contact snubber and one of the dipole conductors, and thus placed in abutting relation therewith. Preferably, each resistive/capacitive contact is formed of a flexible metal material, or a metal-plated plastic material.

    摘要翻译： 本发明通过使用电阻/电容性触点来解决螺旋天线中反复焊接故障的问题。 具体地说，提供了一种电连接器，用于将布置在带状线上的相对导体连接到具有设置在基板上的一对偶极导体的螺旋天线。 连接器包括具有底座的壳体和用于支撑衬底的侧壁。 具有第一和第二端的中心柱和圆柱形孔安装在壳体中。 基板被固定到中心柱的第一端，其第二端固定到壳体的底部。 带状线接触缓冲器支撑在邻近衬底的圆柱形孔的端部并接收带状线。 为了确保带状线导体和偶极子导体之间的RF连续性，提供了一个或多个机械柔性的片簧电阻/电容触点。 每个电阻/电容触点优选地包括焊接到带状线的相对导体的第一部分和从第一部分延伸的第二部分。 或者，每个接触可以是带状线导体之一的整体延伸。 每个电阻/电容接触件的第二部分在接触缓冲器和一个偶极导体之间​​被压缩，并且因此与其邻接。 优选地，每个电阻/电容接触由柔性金属材料或金属镀覆的塑料材料形成。

    Fluoroxy compound solutions
    10.
    发明授权
    Fluoroxy compound solutions 失效
    氟氧化合物溶液

    公开(公告)号：US4568478A

    公开(公告)日：1986-02-04

    申请号：US601589

    申请日：1984-04-18

    申请人： William J. Middleton ,  Shlomo Rozen

    发明人： William J. Middleton ,  Shlomo Rozen

    IPC分类号： C01B9/08 ,  C07C69/62 ,  A62D3/00 ,  C01B7/00

    CPC分类号： C07C71/00 ,  C01B9/08 ,  C07C69/62

    摘要： There is disclosed a solution of at least one fluoroxy compound, wherein said solution has a fluoroxy compound concentration of at least 0.5 meq/liter; said concentration containing about 35 to 100% of an acyl hypofluorite, based on the total number of equivalents of fluoroxy compounds present. The acyl hypofluorite has the formula X(CF.sub.2).sub.n COOF wherein X is H or F and n is 5 to 16. The solution is prepared by treating a suspension of a corresponding specified alkali salt with excess F.sub.2, and is useful as a selective fluorinating agent.

    摘要翻译： 公开了至少一种氟氧化合物的溶液，其中所述溶液具有至少0.5meq / l的氟氧化合物浓度; 所述浓度含有约35至100％的酰基次氟酸盐，基于存在的氟氧化合物的总当量数。 酰基次氟酸盐具有式X（CF 2）n COOF，其中X为H或F，n为5至16.通过用相应的特定碱性盐与过量的F 2处理悬浮液制备该溶液，并且可用作选择性氟化剂 。