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公开(公告)号：US20110300036A1
公开(公告)日：2011-12-08
申请号：US13205024
申请日：2011-08-08
IPC分类号： B01L3/14
CPC分类号： B65D51/1661 , B01J19/126 , B01L3/00 , B01L2300/042 , B65D79/005
摘要： A controlled release and self-resealing vessel assembly for high pressure, microwave assisted chemistry is disclosed. The vessel assembly includes a cylindrical reaction vessel formed of a material that is substantially transparent to microwave radiation. The vessel has angular walls, one closed end for retaining reactants in the lower portions of the vessel, and one open end that defines a mouth for the vessel. The mouth of the cylinder vessel has a lip that is beveled inwardly from the open end. A microwave-transparent solid floating plug closes the mouth of the reaction vessel; with the plug have a frustum portion for engaging the beveled lip when the plug is placed in the mouth of the vessel. A lid exerts a defined axial force against the plug for sealing the plug in the open end of the cylinder with the frustum engaging the lip.
摘要翻译： 公开了一种用于高压微波辅助化学的控释和自重密封容器组件。 容器组件包括由对微波辐射基本透明的材料形成的圆柱形反应容器。 容器具有角壁，一个封闭端用于将反应物保持在容器的下部，一个开口端限定容器的口。 气缸容器的口具有从开口端向内倾斜的唇缘。 微波透明固体浮动塞关闭反应容器的口; 当塞子被放置在容器的口中时，塞子具有用于接合斜面唇缘的截头锥体部分。 盖子对塞子施加限定的轴向力，用于将塞子密封在圆柱体的开口端中，其中截头锥体接合唇缘。
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公开(公告)号：US20110293491A1
公开(公告)日：2011-12-01
申请号：US13205045
申请日：2011-08-08
CPC分类号： B65D51/1661 , B01J19/126 , B01L3/00 , B01L2300/042 , B65D79/005
摘要： A controlled release and self-resealing pressure-maintaining lid for reaction vessels in microwave assisted chemistry is disclosed. The lid includes a rigid perimeter, a rigid center load-bearing portion, and a flexible portion connecting the rigid perimeter to the center load-bearing portion so that the center portion can move when said flexing portion flexes. The lid can be used in conjunction with a vessel assembly. The vessel assembly can include a microwave-transparent, heat expandable reaction vessel having at least two cylindrical portions axially adjacent one another with one of the portions having a diameter larger than the diameter of the other portion, a transition portion between the two cylindrical portions, a vessel mouth in the larger-diameter portion, and a cylindrical retaining sleeve around the vessel.
摘要翻译： 公开了一种用于微波辅助化学反应容器的控释和自重密封压力保持盖。 盖子包括刚性周边，刚性中心承载部分和将刚性周边连接到中心承载部分的柔性部分，使得当所述弯曲部分弯曲时中心部分可以移动。 盖可以与容器组件一起使用。 容器组件可以包括微波透明的热膨胀反应容器，其具有至少两个彼此轴向相邻的圆柱形部分，其中一个部分的直径大于另一部分的直径，两个圆柱形部分之间的过渡部分， 大直径部分中的容器口，以及围绕容器的圆柱形保持套。
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3.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 失效用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US07041947B2
公开(公告)日：2006-05-09
申请号：US10709060
申请日：2004-04-09
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis that includes heterogeneous or highly viscous materials. Includes a fluid reservoir for supplying or receiving fluids, a fluid pump in fluid communication with the reservoir for pumping fluids to or from the reservoir, a microwave transparent reaction vessel in fluid communication with the pump for supplying or receiving fluids to or from the pump and the reservoir, a pressure sensor in fluid communication with the reservoir and the vessel for measuring the pressure of fluids in the instrument at the sensor, and a processor in signal communication with the pressure sensor and the pump for controlling the pump and the flow of fluids in the instrument based at least in part on the pressure measured at the sensor.
摘要翻译： 用于化学合成的受控流微波仪器，包括异质或高粘度材料。 包括用于供应或接收流体的流体储存器，与储存器流体连通以将流体泵送到储存器的流体泵，与泵流体连通的微波透明反应容器，用于向或从泵供应或接收流体;以及 储存器，与储存器流体连通的压力传感器和用于测量传感器中仪器中的流体压力的容器，以及与压力传感器和泵信号通信的处理器，用于控制泵和流体流动 在仪器中至少部分地基于在传感器处测量的压力。
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4.发明授权Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures 有权用于微波辅助化学与高粘度液体和异种混合物的控制流量仪表公开(公告)号：US06989519B2
公开(公告)日：2006-01-24
申请号：US10605021
申请日：2003-09-02
申请人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
发明人： Michael John Collins, Jr. , Wyatt Price Hargett, Jr. , Edward Earl King , Joseph Joshua Lambert , James Edward Thomas
IPC分类号： H05B6/74
CPC分类号： B01J19/126 , B01J4/02 , B01J2219/00164 , B01J2219/1218 , B01J2219/1239 , B01J2219/126 , H05B6/6408 , H05B6/806
摘要： A controlled-flow microwave instrument for chemical synthesis using heterogeneous or highly viscous starting materials includes a microwave source for generating electromagnetic radiation in the microwave frequencies, a microwave cavity in wave communication with the source for exposing compositions placed therein to microwave radiation, a microwave-transparent pressure resistant reaction vessel in the cavity, a source reservoir for starting materials and related compositions, a pump in communication with the source reservoir for pumping heterogeneous or highly viscous materials from the source reservoir to the reaction vessel, and a pressure-resistant valve between the pump and the reaction vessel for isolating the reaction vessel from the pump and the source reservoir during application of microwave energy to compositions in the vessel and from any resulting high pressures generated therein.
摘要翻译： 用于使用异质或高粘度起始材料的化学合成的受控流微波仪器包括用于产生微波频率的电磁辐射的微波源，与所述源波浪连通的微波腔，用于将放置在其中的组合物暴露于微波辐射中; 在空腔中的透明耐压反应容器，用于起始材料和相关组合物的源储存器，与源储存器连通的泵，用于将来自源储器的非均质或高粘度物质泵送到反应容器，以及在源储存器之间的耐压阀， 泵和反应容器，用于在将微波能量应用于容器中的组合物和从其中产生的任何所得到的高压时将反应容器与泵和源储存器隔离。
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公开(公告)号：US06287526B1
公开(公告)日：2001-09-11
申请号：US09323198
申请日：1999-06-01
IPC分类号： B01J304
CPC分类号： H05B6/806 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/1209 , B01J2219/1218 , G01N1/44 , H05B6/763
摘要： A dynamic sealing structure for pressure vessels used in microwave assisted chemistry is disclosed. The structure includes a cylindrical vessel liner and a removable liner cap, each formed of a microwave transparent material. The liner has a circular mouth with a lip formed of respective first and second beveled edges, with the first beveled edge forming an interior edge of the circular mouth and the second beveled edge forming an exterior edge of the circular mouth. The cap includes respective interior and exterior faces, with a sleeve depending from the interior face and having a circumference that engages the interior surface of the vessel liner for being urged under pressure against the interior surface of the vessel liner. The interior face of the cap comprising a circular channel outward of the sleeve and having a circumference that engages the lip of the vessel liner, and with the channel comprising two beveled edges that respectively engage both beveled edges of the lip of the liner.
摘要翻译： 公开了用于微波辅助化学中的压力容器的动态密封结构。 该结构包括圆柱形容器衬里和可移除的衬套盖，每个由微波透明材料形成。 衬里具有圆形口，其具有由相应的第一和第二倾斜边缘形成的唇缘，其中第一倾斜边缘形成圆形口部的内部边缘，并且第二倾斜边缘形成圆形口部的外部边缘。 盖包括相应的内表面和外表面，套筒从内表面悬垂，并且具有接合容器衬里的内表面的圆周，用于在压力下被推压到容器衬里的内表面。 所述盖的内表面包括一个圆形通道，位于套筒的外部，并具有接合容器衬套的唇缘的圆周，并且该通道包括分别接合衬套的唇缘的两个倾斜边缘的两个斜边。
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公开(公告)号：US06246038B1
公开(公告)日：2001-06-12
申请号：US09516329
申请日：2000-03-01
IPC分类号： H05B650
CPC分类号： H05B6/806 , B01J19/126 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , G01L9/0051 , G01N1/44
摘要： A microwave vessel system for external and noninvasive pressure monitoring and control is disclosed. The system comprises a reaction vessel formed of a material that is transparent to microwave radiation, with the reaction vessel including a portion that is movable under pressure generated by a chemical reaction inside the vessel while maintaining the reaction sealed inside the vessel. A sensor is adjacent to the movable portion of the vessel for detecting the motion of the movable portion as the portion responds to pressure generated inside the vessel. The system includes means for maintaining the sensor against the movable portion while microwaves are applied to the vessel so that the movement of the movable portion under pressure is detected by the sensor.
摘要翻译： 公开了一种用于外部和无创压力监测和控制的微波容器系统。 该系统包括由对微波辐射透明的材料形成的反应容器，反应容器包括在容器内部通过化学反应产生的压力下可移动的部分，同时保持反应密封在容器内。 传感器邻近容器的可移动部分，用于检测可动部分的运动，因为该部分响应于容器内产生的压力。 该系统包括用于在将微波施加到容器的同时将传感器保持在可移动部分上的装置，使得在压力下的可移动部分的运动被传感器检测到。
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公开(公告)号：US06926939B2
公开(公告)日：2005-08-09
申请号：US10064718
申请日：2002-08-09
IPC分类号： B01J3/04 , B01J19/02 , B01J19/12 , F16J13/02 , G01N1/44 , G01N35/00 , H05B6/64 , H05B6/80 , B32B1/08 , A61L2/12 , B01L9/00 , B01L11/00
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymericcylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding is selected from the group consisting of filaments and yarns. A supporting frame extends along the cylinder and across the lid and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.
摘要翻译： 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆柱体的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面下边缘，当帽位于聚合圆筒上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个缠绕织物层，其中绕组选自长丝和纱线。 支撑框架沿着圆柱体延伸并且横过盖子并且横过气缸的封闭端延伸，并且当在容器内部产生压力时防止盖子从气缸移位。
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公开(公告)号：US06863871B2
公开(公告)日：2005-03-08
申请号：US09858614
申请日：2001-05-16
CPC分类号： H05B6/806 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/1209 , B01J2219/1218 , G01N1/44 , H05B6/763
摘要： A dynamic sealing structure for pressure vessels used in microwave assisted chemistry is disclosed. The structure includes a cylindrical vessel liner and a removable liner cap, each formed of a microwave transparent material. The liner has a circular mouth with a lip formed of respective first and second beveled edges, with the first beveled edge forming an interior edge of the circular mouth and the second beveled edge forming an exterior edge of the circular mouth. The cap includes respective interior and exterior faces, with a sleeve depending from the interior face and having a circumference that engages the interior surface of the vessel liner for being urged under pressure against the interior surface of the vessel liner. The interior face of the cap comprising a circular channel outward of the sleeve and having a circumference that engages the lip of the vessel liner, and with the channel comprising two beveled edges that respectively engage both beveled edges of the lip of the liner.
摘要翻译： 公开了用于微波辅助化学中的压力容器的动态密封结构。 该结构包括圆柱形容器衬里和可移除的衬套盖，每个由微波透明材料形成。 衬里具有圆形口，其具有由相应的第一和第二倾斜边缘形成的唇缘，其中第一斜边形成圆形口的内边缘，第二斜边形成圆形口的外边缘。 盖包括相应的内表面和外表面，套筒从内表面悬垂，并且具有接合容器衬里的内表面的圆周，用于在压力下被推压到容器衬里的内表面。 所述盖的内表面包括一个圆形通道，位于套筒的外部，并具有接合容器衬套的唇缘的圆周，并且该通道包括分别接合衬套的唇缘的两个倾斜边缘的两个斜边。
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公开(公告)号：US06534140B2
公开(公告)日：2003-03-18
申请号：US09260209
申请日：1999-03-01
IPC分类号： B29D2300
CPC分类号： H05B6/806 , B01J3/048 , B01J19/0073 , B01J19/02 , B01J19/126 , B01J2219/0245 , B01J2219/0295 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218 , F16J13/02 , G01N1/44 , G01N2035/00405 , H05B6/6408 , Y10T428/131 , Y10T428/1314 , Y10T428/1321 , Y10T428/1366 , Y10T428/1369 , Y10T428/139 , Y10T428/1393
摘要： A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder and a circular polymeric cap for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is beveled inwardly from the open end, and the circular polymeric cap has a beveled lower edge that engages the beveled lip when the cap is place upon the polymeric cylinder. For high pressure applications, a choke cylinder depends from the beveled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A composite sleeve surrounds the polymeric cylinder, and includes at least one wound fabric layer in which the winding is selected from the group consisting of filaments and yarns. A supporting frame extends along the cylinder and across the lid and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.
摘要翻译： 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括聚合物圆筒和用于圆柱体的圆形聚合物盖，所述圆筒在一端封闭并在另一端开口以接收盖。 圆筒的开口端具有从开口端向内倾斜的唇缘，并且圆形聚合物盖具有斜面的下边缘，当帽位于聚合物圆柱体上时，该下边缘接合倾斜的唇缘。 对于高压应用，阻塞气缸从盖的斜面下边缘取向，并且具有与聚合物圆筒的内径基本相同的外径，使得扼流圈为气缸提供自密封机构，作为来自 化学反应在气缸内增加。 复合套管围绕聚合物圆筒，并且包括至少一个缠绕织物层，其中绕组选自长丝和纱线。 支撑框架沿着圆柱体延伸并且横过盖子并且横过气缸的封闭端延伸，并且当在容器内部产生压力时防止盖子从气缸移位。
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公开(公告)号：US6124582A
公开(公告)日：2000-09-26
申请号：US265917
申请日：1999-03-10
CPC分类号： H05B6/806 , B01J19/126 , G01L9/0051 , G01N1/44 , B01J2219/1209 , B01J2219/1215 , B01J2219/1218
摘要： A microwave vessel system for external and noninvasive pressure monitoring and control is disclosed. The system comprises a reaction vessel formed of a material that is transparent to microwave radiation, with the reaction vessel including a portion that is movable under pressure generated by a chemical reaction inside the vessel while maintaining the reaction sealed inside the vessel. A sensor is adjacent to the movable portion of the vessel for detecting the motion of the movable portion as the portion responds to pressure generated inside the vessel. The system includes means for maintaining the sensor against the movable portion while microwaves are applied to the vessel so that the movement of the movable portion under pressure is detected by the sensor.
摘要翻译： 公开了一种用于外部和无创压力监测和控制的微波容器系统。 该系统包括由对微波辐射透明的材料形成的反应容器，反应容器包括在容器内部通过化学反应产生的压力下可移动的部分，同时保持反应密封在容器内。 传感器邻近容器的可移动部分，用于检测可动部分的运动，因为该部分响应于容器内产生的压力。 该系统包括用于在将微波施加到容器的同时将传感器保持在可移动部分上的装置，使得在压力下的可移动部分的运动被传感器检测到。
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